• 제목/요약/키워드: SEM : scanning electron microscope

검색결과 1,887건 처리시간 0.031초

Chemical bath deposition(CBD)에 의해 성장된 CdS 박막의 annealing 효과 (Annealing effects of CdS thin films grown by Chemical bath deposition(CBD))

  • 김미정;정원호;오동훈;채영안;차덕준;조승곤;정양준;;이기진
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 추계학술대회 논문집
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    • pp.358-360
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    • 2007
  • For large scaled solar cells and photosensors CdS thin films of $2{\mu}m$ thickness have deposited on ITO glass substrate by chemical bath deposition methode in $300^{\circ}C$ electric furnace. The surface roughness and resistance of cadmium sulphide(CdS) thin films with different microstructures and morphologies was investigated by using a x-ray diffraction (XRD), a scanning electron microscope (SEM), an atomic force microscope (AFM), and a near-field scanning microwave microscope (NFMM). As the different substrate heat temperatures, the microwave reflection coefficient $S_{11}$ and intensity of the (002) diffraction peak was changed, and the surface morphology also has shown differently.

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불소 표면 개질 고분자 분리막의 제조와 노블가스 분리특성 (Fabrication of Fluorinated Polymeric Membranes and Their Noble Gas Separation Properties)

  • 김기범;윤국로
    • 공업화학
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    • 제21권4호
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    • pp.475-478
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    • 2010
  • 불소화 반응을 통하여 PDMS을 질소 분위기 하에서 $50{\sim}2000\;{\mu}mol/mol$ 농도의 불소 가스($F_2$)를 사용하여 직접적인 방법으로 복합막 표면개질을 하였고 이를 OM (Optical Microscope), AFM (Atomic Force Microscope), SEM (Scanning electron microscope), FT-IR (Fourier transform infrared spectroscopy)을 측정하여 막 표면을 연구하였고 GC (Gas chromatography)로 혼합 노블가스의 기체 거동을 조사하였다. 다양한 노블 혼합 가스를 사용하여 표면 개질된 PDMS 멤브레인의 선택도가 50% 향상 되었다.

A study on the fine structure of marine diatoms in Korean coastal waters: Genus Thalassiosira 5

  • Park, Joon-Sang;Lee, Jin-Hwan
    • ALGAE
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    • 제25권3호
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    • pp.121-131
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    • 2010
  • Thalassiosira species were collected from October 2007 to January 2009 in an attempt to better understand species diversity of the genus Thalassiosira in Korean coastal waters. A total of 5 Thalassiosira species (T. concaviuscula, T. oceanica, T. partheneia, T. simonsenii and T. nanolineata) were identified here. Most species in this study were of small size, and 5 species were recorded for the first time in Korean coastal waters. Using a scanning electron microscope (SEM), we described distinctive characteristics of fine structure that proved to be important diagnostic characteristics for the identification of each species. The most important diagnostic characteristics for Thalassiosira species identification were the marginal strutted processes, the position of labiate processes, and the areolation. The differential characteristics of the species studied were: T. concaviuscula has a double layered external tubes on the marginal strutted processes; T. oceanica shows marginal ridges that are interlinked between the marginal strutted processes; the valve face of T. partheneia is fairly convex and its labiate process is positioned midway between two strutted processes; T. simonsenii is characterized by two labiate processes and somewhat coarse areolae; and, T. nanolineata has several central strutted processes and linear areolation.

FIT OF FIXTURE/ABUTMENT/SCREW INTERFACES OF INTERNAL CONNECTION IMPLANT SYSTEM

  • Kim, Jin-Sup;Kim, Hee-Jung;Chung, Chae-Heon;Baek, Dae-Hwa
    • 대한치과보철학회지
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    • 제43권3호
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    • pp.338-351
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    • 2005
  • Statement of problem. Accurate fit between the implant components is important because the misfit of the implant components results in frequent screw loosening, irreversible screw fracture, plaque accumulation, poor soft tissue reaction, and destruction of osseointegration. Purpose. This study is to evaluate the machining accuracy and consistency of the implant fixture/ abutment/screw interfaces of the internal connection system by using a Stereoscopic Zoom microscope and FE-SEM(field emission scanning electron microscope) Materials and methods. The implant systems selected in this study were internal connection type implants from AVANA(Osstem^{\circledR}), Bioplant(Cowell-Medi^{\circledR}), Dio(DIO^{\circledR}), Neoplant(Neobiotech 􀋓), Implantium(Dentium􀋓)systems. Each group was acquired 2 fixtures at random. Two piece type abutment and one piece type abutment for use with each implant system were acquired. Screw were respectively used to hold a two piece type abutment to a implant fixture. The implant fixtures were perpendiculary mounted in acrylic resin block. Each two piece abutment was secured to the implant fixture by screw and one piece abutment also secured to the implant fixture. Abutment/fixture assembly were mounted in liquid unsaturated polyester. All samples were cross-sectioned with grinder-polisher unit. Finally all specimens were analysed the fit between implant fixture/abutment/screw interfaces Results and conclusions. 1. Implant fixture/abutment/screw connection interfaces of internal connection systems made in Korea were in good condition. 2. The results of the above study showed that materials and mechanical properties and quality of milling differed depending on their manufacturing companies.

초고진공 분자선 에피성장 시스템의 제작과 에피성장된 ZnSe/GaAs(001)의 광학특성 (Construction of an Ultra High Vacuum Molecular Beam Epitaxy System and Optical Property of ZnSe/GaAs(001) Epitaxial films)

  • 김은도;손영호;엄기석;조성진;황도원
    • 한국진공학회지
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    • 제15권5호
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    • pp.458-464
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    • 2006
  • 본 연구에서는 초고진공 (UHV; ultra high vacuum) 분자선 에피성장 (MBE; molecular beam epitaxy) 시스템의 제작과 성능연구가 성공적으로 이루어졌다. 초고진공 용 분자선 에피성장 시스템을 국산화개발 및 제작하여, 장비에 관한 성능 테스트를 하게 되었다. 본 장비의 진공도가 $2X10^{10}$ Torr에 도달함을 확인하였고, 시편 가열모듈(substrate heating module)이 $1,100^{\circ}C$까지 가열됨을 확인할 수 있었으며, ZnSe/GaAs(001)의 증착특성을 SEM (scanning electron microscope), AFM (atomic force microscope), XRD (x-ray diffraction), PL (photoluminescence) 등으로 조사하였다.

전해액 조성이 전기도금으로 제작된 구리박막의 특성에 미치는 영향 (Effect of electrolyte composition on Cu thin film by electroplating)

  • 송유진;서정혜;이연승;염기수;류영호;홍기민
    • 한국정보통신학회:학술대회논문집
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    • 한국해양정보통신학회 2008년도 추계종합학술대회 B
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    • pp.95-99
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    • 2008
  • 반도체 소자의 소형화에 따라 낮은 비저항을 가진 구리가 ULSI의 금속배선으로 사용되고 있다. 구리선의 비저항은 RC delay와 집적회로의 신호전달에 영향을 미치게 된다. 본 논문에서는 전기도금 된 구리박막의 비저항에 대해 전해액이 미치는 영향을 조사하였다. 4탐침 표면저항측정기로 비저항을 평가하였고, XRD (X-ray Diffraction), AFM (Atomic Force Microscope), FE-SEM (Field Emission Scanning Electron Microscope), XPS (X-ray Photoelectron Spectroscopy)로 박막의 특성을 조사하였다. 실험한 결과, 전해액의 조건이 전기도금으로 증착된 낮은 비저항을 갖는 구리박막의 형성에 있어 중요한 역할을 하는 것을 확인하였다.

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초소수성 전기 분무 마이크로 추진 장치 및 마이크로 추력 측정 (Study on super-hydrophobic electro-spray micro thruster and measurement of micro scale thrust)

  • 이영종;유용훈;;김상훈;박배호;변도영
    • 한국항공우주학회지
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    • 제37권2호
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    • pp.175-180
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    • 2009
  • 이 논문은 폴리머 기반의 전기 분무 장치를 만들기 위하여 이온빔 장치를 통하여 초소수성으로 가공 된 polytetrafluoroethylene(PTFE) 노즐을 사용하였다. 초소수성 표면을 만들기 위하여, PTFE 표면은 Ar과 $O_2$를 이용한 이온빔 공정 장치를 사용하였다. 최적의 표면 공정 조건은 Ar과 $O_2$ 유량 및 에너지 단위를 변화 시켜 얻을 수 있었다. 공정된 노즐의 표면 특성을 분석하기 위하여 접촉각 측정을 수행하였고, 표면의 형태적 분석을 위해 scanning electron microscope(SEM) 그리고 atomic force microscope(AFM) 측정을 하였다. 초소수성으로 공정된 노즐을 사용함으로써 보다 안정적이고 반복적인 전기 분무가 가능함을 확인 하였으며, 공정 된 노즐의 성능을 평가하기 위하여 외팔보와 이온빔으로 표면 처리 된 노즐 그리고 레이져 변위센서를 이용하여 마이크로 스케일의 추력을 측정하였다.

레이저 유도 광열 효과를 이용하여 제작된 오목한 광섬유 팁의 곡률 반경에 관한 연구 (A Study on the Radius of Curvature of Concave Optical Fiber Tips fabricated by Laser-Induced Photothermal Effect)

  • 최지원;손경호;유경식
    • 한국전자통신학회논문지
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    • 제14권5호
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    • pp.871-876
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    • 2019
  • 본 논문에서는 플루오린화 수소산(Hydrofluoric acid: HF) 수용액과 광섬유에 인가된 $1.55{\mu}m$ 파장의 레이저를 통해 유도된 광열 효과를 이용하여 오목한 광섬유 팁을 제작하였다. 제작 과정에서 인가한 레이저의 세기, 식각 시간, HF 수용액의 농도에 따른 광섬유 팁 오목 면의 곡률 반경을 광학 현미경을 이용하여 측정하였으며 곡률 반경이 세 변인에 대하여 어떻게 변화하는지 분석하였다. 또한, Free Spectral Range(FSR)와 Scanning electron microscope(SEM) 촬영을 통해 현미경을 이용한 측정 방법의 신뢰성을 검증하였다. 본 논문을 통해 광섬유 팁의 오목 면 제작 과정에서 변인에 따라 곡률 반경을 조절할 수 있게 됨으로써 기존의 HF 수용액을 이용한 광섬유 식각 방법의 한계점을 극복할 수 있었다.

Scanning Electron Microscopic Observation of Human Skin Replica

  • Rhyu, Yeon-Seung;Chung, Ye-Ji;Uhm, Chang-Sub
    • Applied Microscopy
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    • 제40권4호
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    • pp.267-270
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    • 2010
  • The skin is the largest organ of the integument system whose surface is closely related with many physiological and pathological conditions. Various methods are used to understand the structural and functional status of human skin. We would like to present usefulness of scanning electron microscopic (SEM) observation of skin replica and its significance of training module for a novice. The silicon replicas from several regions of the body (hand, finger, forearm, lip, and face) were casted by applying Exafine$^{(R)}$ mixture. The positive replicas were prepared by applying EPON 812 mixture on negative silicon replicas. Some of the negative silicon replicas were cut with a razor blade and surface profiles were observed. The negative and positive replicas were coated with platinum and were observed under the scanning electron microscope. We could investigate the detailed structures of the human skin surface without any physical damage to the subject. The positive replicas depicted real surface structure of the human skin vividly. The cross sectional view of the negative silicon replicas provided surface profile clearly. The scanning electron microscopic observation of the human skin replicas would be useful to study skin surface structures and to evaluate medical and esthetical applications.

후경화 조건에 따른 에폭시 수지의 물성에 관한 연구 (A Study on the Physical Property of Epoxy Resin Due to After-Curing Condition)

  • 한정영;김명훈;강성수
    • 한국생산제조학회지
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    • 제21권6호
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    • pp.976-981
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    • 2012
  • In this study, hardness, microstructure and temperature of glass transition are measured respectively by using SEM (Scanning electron microscope) and DSC (Differential scanning calorimeter) to analyze the effects on material properties by after-curing in the epoxy resin. As the result of hardness test according to the after-curing conditions, the higher the temperature of after-curing, hardness and heat resistance are, the higher hardness is. As a result of microstructure for each specimen by SEM, it could be confirmed that the specimen with after-curing has more dense fracture surface. It is also found that temperatures of glass transitions by DSC are comparatively higher in the specimens with after-curing, and the differences between after-curing conditions are negligible.