• Proceedings of the Korean Society of Precision Engineering Conference
• /
• 2008.06a
• /
• pp.621-622
• /
• 2008

• Proceedings of the Materials Research Society of Korea Conference
• /
• 1998.08a
• /
• pp.113.4-113
• /
• 1998

• Structural Engineering and Mechanics
• /
• v.35 no.3
• /
• pp.379-382
• /
• 2010

• Structural Engineering and Mechanics
• /
• v.17 no.6
• /
• pp.789-817
• /
• 2004

This paper deals with the modal analysis of rotational shell structures by means of the numerical solution technique known as the Generalized Differential Quadrature (G. D. Q.) method. The treatment is conducted within the Reissner first order shear deformation theory (F. S. D. T.) for linearly elastic isotropic shells. Starting from a non-linear formulation, the compatibility equations via Principle of Virtual Works are obtained, for the general shell structure, given the internal equilibrium equations in terms of stress resultants and couples. These equations are subsequently linearized and specialized for the rotational geometry, expanding all problem variables in a partial Fourier series, with respect to the longitudinal coordinate. The procedure leads to the fundamental system of dynamic equilibrium equations in terms of the reference surface kinematic harmonic components. Finally, a one-dimensional problem, by means of a set of five ordinary differential equations, in which the only spatial coordinate appearing is the one along meridians, is obtained. This can be conveniently solved using an appropriate G. D. Q. method in meridional direction, yielding accurate results with an extremely low computational cost and not using the so-called "delta-point" technique.

• Progress in Superconductivity
• /
• v.3 no.2
• /
• pp.213-217
• /
• 2002

We have fabricated successfully single-filament composite $MgB_2$/SUS tapes, as an ultrarobust conductor type. The fabrication of the $MgB_2$/SUS tapes was performed by power-in-tube (PIT) process such as swaging and cold rolling. The critical transition temperatures $T_{c}$~38.5 K and ~36 K were observed for the sintered and the nonsintered $MgB_2$/SUS tapes, respectively In addition, the isothermal magnetization M(H) of the sintered $MgB_2$/SUS tapes was measured at temperatures T (between 5 and 50 K) in fields up to 6 T, employing a PPMS-9 (Quantum Design). The persistent current density (J$T_{P}$) values were obtained from the M(H) data, using Bean model, fur the sintered $MgB_2$/SUS tapes. The estimated values were higher than ~ 6$\times$ $10^{5}$ $A/\textrm{cm}^2$ at T = 5 K, with H : 0 G. We also investigated the cross section of the sintered tapes, by using SEM and EDX. An evidence of weak reaction on boundary between $MgB_2$ and SUS tube is found in the SEM and EDX.X.X.X.

• Polymer(Korea)
• /
• v.30 no.6
• /
• pp.532-537
• /
• 2006

In order to successfully meet the environmental and recycling problems, natural polymer and their derivatives are recognized as a promising biodegradable material. In this study, the biodegradable composites of cellulose diacetate and starch were prepared, and their physical and thermal properties were investigated. For the melting processing, triacetine was added as a plasticizer into the composites. The processability of cellulose diacetate was further enhanced by increasing the amount of starch in the composites. The tensile stress and Young's modulus were decreased and elongation was increased with increasing the amount of starch in them. A $T_g$ value was decreased with increasing the amount of starch in the composites. Also, the morphology of the composites were observed with the SEM.

• Journal of the Korean Crystal Growth and Crystal Technology
• /
• v.16 no.2
• /
• pp.82-87
• /
• 2006

Glassy specimen was obtained by melting and quenching a borosilicate glass frit miked with $10{\sim}80wt%$ EAF dust. The glass transition temperature, $T_g$ of glassy specimen was measured around $550^{\circ}C$ from the DTA curve and the eat treatment condition to crystallize a glassy specimen was selected as $700^{\circ}C$/1 hr. The spinel crystal peaks were found in XRD analysis for the glass containing dust > 70 wt%. For the glass-ceramics, however, the spinel peaks in a specimen containing dust > 40 wt%, and the spinel and willemite peaks in dust > 80 wt%. The crystals of several tens of nanometer with aspect ratio of $0.7{\sim}1.0$ were observed at a glassy specimen containing dust > 40 wt% by SEM which was not found by XRD analysis. For the glass-ceramics, the crystals were found in a specimen containing dust of even 10 wt% by SEM. The feature and distribution of crystals observed through the specimen for a glass-ceramics were diverse and not uniform. The crystals found in the glass-ceramics containing 70 wt% dust were hexahedral with an aspect ratio of around unity.

• Analytical Science and Technology
• /
• v.13 no.2
• /
• pp.194-199
• /
• 2000

The study on the adsorption, the surface properties and the antibacterial effects of the Ni-treated PAN based activated carbon fibers was carried out. In the adsorption study on the Ni-treated PAN based ACFs, Type I isotherms for N1-N3 and Type II-Type III isotherms for N4-N6 were obtained, respectively. Futhermore, their adsorbed volumes slowly were decreased with the increase in the mole concentration of Ni on the treated PAN based ACFs. From the BET equation, the specific surface areas of the Ni-treated PAN based ACFs were in the range of $692.58-895.24m^2/g$. The micropore volumes obtained from ${\alpha}_s$-method using common-t value were $0.19-0.56cm^3/g$. The surfaces of PAN based ACFs partially blocked by metal after the treatment were observed from the SEM micrographs. Finally, from the antibacterial effects using Shake flask method against E. coli, the percentage of the effects was 92.5-100% and the antibacterial effect was increased with the increase in mole concentration of Ni treated.

• Journal of the Korean Ceramic Society
• /
• v.38 no.12
• /
• pp.1104-1109
• /
• 2001

Samples with the nominal composition, B $i_{1.84}$P $b_{0.34}$S $r_{1.91}$C $a_{2.03}$C $u_{3.06}$ $O_{10+}$$\delta$/ high $T_{c}$ superconductors containing As as an additive were fabricated by a solid-state reaction method. Samples with Ag of 10wt%, 30 wt% and 50 wt% each were sintered at 86$0^{\circ}C$~875$^{\circ}C$ for 24 hours. The structural characteristics, critical temperature and grain size with respect to Ag contents were analyzed by XRD(X-ray Diffraction) and SEM(Scanning Electron Microscope), respectively. As Ag contents increased, XRD peaks of g in Bi-2223 phase superconductors intensified and the proportion of the phase transition from Bi-2223 to Bi-2212 was increased.increased.

• Journal of the Korean Chemical Society
• /
• v.63 no.6
• /
• pp.453-458
• /
• 2019

Synthesis of ZnCo₂O₃ oxide is performed by sol-gel method via nitrate-citrate route. Powder X-ray diffraction (XRD) study shows monoclinic unit cell having lattice parameters: a = 5.721(1) Å, b = 8.073(2) Å, c = 5.670(1) Å, β = 93.221(8)°, space group P_2/m and Z = 4. Average crystallite sizes determined by Scherrer equation are the range ~14-32 nm, whereas SEM micrographs show nano-micro meter size particles formed in ZnCo₂O₃. Endothermic peak at ~798 K in the Differential scanning calorimetric (DSC) trace without weight loss could be due to structural transformation and the endothermic peak ~1143 K with weight loss is due to reversible loss of O₂ in air atmosphere. Energy Dispersive X-ray (EDX) analysis profile shows the presence of elements Zn, Co and O which indicates the purity of the sample. Magnetic measurements in the range of +12 kOe to -12 kOe at 10 K, 77 K, 120 K and at 300 K by PPMS-II Physical Property Measurement System (PPMS) shows hysteresis loops having very low values of the coercivity and retentivity which indicates the weakly ferromagnetic nature of the oxide. Observed X-band EPR isotropic lineshapes at 300 K and 77 K show positive g-shift at g_iso ~2.230 and g_iso ~2.217, respectively which is in agreement with the presence of paramagnetic site Co²⁺(3d⁷) in the oxide. DC conductivity value of 2.875 ×10^-8 S/cm indicates very weakly semiconducting nature of ZnCo₂O₃ at 300 K. DRS absorption bands ~357 nm, ~572 nm, ~619 nm and ~654 nm are due to the d-d transitions ⁴T_1g(⁴F)→²E_g(²G), ⁴T_1g(⁴F)→⁴T_1g(⁴P), ⁴T_1g(⁴F)→⁴A_2g(⁴F), ⁴T_1g(⁴F)→⁴T_2g(⁴F), respectively in octahedral ligand field around Co²⁺ ions. Direct band gap energy, E_g~ 1.5 eV in the oxide is obtained by extrapolating the linear part of the Tauc plot to the energy axis indicates fairly strong semiconducting nature of ZnCo₂O₃.