• 제목/요약/키워드: SEM $T_g

검색결과 161건 처리시간 0.028초

A New Method for Cultivation of Sclerotium of Grifola umbellata

  • Choi, Kyung-Dal;Lee, Kyung-Tae;Shim, Jae-Ouk;Lee, Youn-Su;Lee, Tae-Soo;Lee, Sang-Sun;Guo, Shun-Xing;Lee, Min-Woong
    • Mycobiology
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    • 제31권2호
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    • pp.105-112
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    • 2003
  • Sclerotia of Grifola umbellata were cultivated by two methods such as burying and root inoculation methods. The sclerotia of G. umbellata produced by the burying method were $6.0{\sim}6.8{\times}3.4{\sim}4.6{\times}1.8{\sim}1.9cm$(Width$\times$Length$\times$Thickness) in size and $17.3{\sim}19.6g$ in weight, respectively. Their increase rate was $1.10{\times}1.12$ times. On the other hand, the sclerotia cultivated by the root inoculation method were $18.3{\sim}31.5{\times}12.5{\sim}26.4{\times}3.1{\sim}3.7cm(W{\times}L{\times}T)$ in size and $219.1{\sim}576.6g$ in weight, respectively. Their growth increment was $11.18{\sim}39.77$ times. The rhizomorphs of Armillaria mellea were developed with a high density under fallen leaves layer covering cultivation site, and distributed mainly between soil surface and soil depth of about 10 cm as well as colonized prominently on the inoculated wood logs. Fungal interaction between G. umbellata and A. mellea were observed mainly in the stage of white sclerotium of G. umbellata. The sclerotia of G. umbellata which were developed newly and harvested in the root inoculation method were twined with root hairs of host tree and rhizomorphs of A. mellea. The sclerotia of G. umbellata decomposing root hairs of host tree were confirmed through SEM examination. Physiochemical characteristics of soil in all cultivation sites had no significant differences. Soil pH were in the range of pH $3.98{\sim}4.40$. Organic matters were the range of $17.97{\sim}23.86%$ and moisture contents of soil were $12.00{\sim}18.20%$. Soil temperatures showed $12.9{\sim}13.8^{\circ}C$ in November and $22.0{\sim}23.9^{\circ}C$ in August, respectively. In conclusion, the root inoculation method seems to be a practical method for cultivating sclerotia of G. umbellata due to its many advantages such as simplicity of inoculation process, shortening of cultivation periods and facility of harvest.

Influences of the Irradiation of Intense Pulsed ion Beam (IPIB) on the Surface of Ni$_3$Al Base Alloy IC6

  • Le, X.Y.;Yan, S.;Zhao, W.J.;Han, B.H.;Wang, Y.G.;Xue, J.M.;Zhang, H.T.
    • Journal of Korean Vacuum Science & Technology
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    • 제6권2호
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    • pp.92-96
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    • 2002
  • In this paper, we treated the Ni$_3$Al based alloy samples with intense pulsed ion beams (IPIB) at the beam parameters of 250KV acceleration voltage, 100 - 200 A/cm$^2$ current density and 60 u pulse duration. We simulated the thermal-mechanical process near the surface of Ni$_3$Al based alloy with our STEIPIB codes. The surface morphology and the cross-section microstructures of samples were observed with SEM, the composition of the sample surface layer was determined by X-ray Energy Dispersive Spectrometry (XEDS) and the microstructure on the surface was observed by Transmission Electron Microscope (TEM). The results show that heating rate increases with the current density of IPIB and cooling rate reached highest value less than 150 A/cm$^2$. The irradiation of IPIB induced the segregation of Mo and adequate beam parameter can improve anti-oxidation properly of IC6 alloy. Some craters come from extraneous debris and liquid droplets, and some maybe due to the melting of the intersection region of interphase. Increasing the pulse number enlarges average size of craters and decreases number density of craters.

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SnO2센서의 ZnO 첨가량에 따른 di(propylene glycol) methylether (DPGME)에 대한 반응 특성 (Di(propylene glycol) Methylether (DPGME) Sensing Characteristics of SnO2-ZnO Sensor)

  • 차건영;백원우;윤기열;이상태;최낙진;이덕동;허증수
    • 한국재료학회지
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    • 제14권3호
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    • pp.224-228
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    • 2004
  • Respectively the powder made of ZnO added $SnO_2$ was prepared by coprecipitation method and the thick film gas sensor was fabricated by screen-printing technique, The morphology and phase of the powder and film was investigated by SEM and XRD. The specific area of the particle was linearly increased with ZnO contents. Target gas was di(propylene glycol) methylether ($CH_3$($OC_3$$H_{6}$ )$_2$OH, DPGME), which is simulant gas of blister gas. The gas sensing characteristics for DPGME were examined with flow type measurement system and the concentrations of target gas were controlled from 500 ppb to 1500 ppb. ZnO (2 wt%) added $SnO_2$ showed maximum sensitivity to DPGME at $300^{\circ}C$.

Zr/Ti 몰비에 따른 PZT-PCNS 압전 세라믹의 압전 및 유전 특성 (The Dielertric and Piezoelectric Properties of PZT-PCNS Piezoelectric Ceramics with Zr/Ti Mole Ratio)

  • 이시용;이용회;이문주;이종섭;임기조
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2001년도 추계학술대회 논문집 전기물성,응용부문
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    • pp.100-102
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    • 2001
  • In this paper, the piezoelectric and dielectric properties of $Pb(Zr_xTi_{1-x)O_3$ - $Pb(Co_{1/3}Nb_{1/3})O_3)$ piezoelectric ceramics have been investigated as a function of Zr/Ti mole ratio. From the results, when Zr/Ti mole ratio is 49/51, electromechanical coupling coefficient($k_p$), piezoelectric strain constant($d_{33}$) mechanical quality factor($Q_m$), and Permittivity(${{\varepsilon}_{33}}^T/{\varepsilon}_0$) is 64[%], 469[PC/N], 360 and 2000, respectively. Morphotropic Phase Boundary is Zr/Ti mole ratio(49/51) from XRD analysis. Also. From SEM observation, when sintering temperature is 1150[$^{\circ}C$], grain size is about $1{\sim}2[{\mu}m]$ and maximum sintering density is 7.85[$g/cm^3$].

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A direct damage detection method using Multiple Damage Localization Index Based on Mode Shapes criterion

  • Homaei, F.;Shojaee, S.;Amiri, G. Ghodrati
    • Structural Engineering and Mechanics
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    • 제49권2호
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    • pp.183-202
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    • 2014
  • A new method of multiple damage detection in beam like structures is introduced. The mode shapes of both healthy and damaged structures are used in damage detection process (DDP). Multiple Damage Localization Index Based on Mode Shapes (MDLIBMS) is presented as a criterion in detecting damaged elements. A finite element modeling of structures is used to calculate the mode shapes parameters. The main advantages of the proposed method are its simplicity, flexibility on the number of elements and so the accuracy of the damage(s) position(s), sensitivity to small damage extend, capability in prediction of required number of mode shapes and low sensitivity to noisy data. In fact, because of differential and comparative form of MDLIBMS, using noise polluted data doesn't have major effect on the results. This makes the proposed method a powerful one in damage detection according to measured mode shape data. Because of its flexibility, damage detection process in multi span bridge girders with non-prismatic sections can be done by this method. Numerical simulations used to demonstrate these advantages.

Employee Performance Optimization Through Transformational Leadership, Procedural Justice, and Training: The Role of Self-Efficacy

  • KUSUMANINGRUM, G.;HARYONO, Siswoyo;HANDARI, Rr. Sri
    • The Journal of Asian Finance, Economics and Business
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    • 제7권12호
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    • pp.995-1004
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    • 2020
  • This study aims to analyze the effect of transformational leadership (TL), procedural justice (PJ), and training (T) on employee performance (EP) mediated by self-efficacy (SE). The object of this research is Rumah Sakit Umum Daerah (RSUD) M.Th. Djaman, a hospital in Sanggau Regency, while the subjects are the institution's staff. Data collection search uses purposive sampling with a total of 120 samples. Data are obtained through questionnaires distributed directly to respondents using the Google Form application. Data analysis techniques used in this study include standard error of mean (SEM) with AMOS software version 24.00. Methods use to test validity and reliability of data include Confirmatory Factor Analysis (CFA), Construct Reliability (CR) and VE. The results of the analysis show that only training has a significant effect on self-efficacy, and self-efficacy has a significant effect on employee performance. Also, self-efficacy is proven to mediate the role of training on employee performance; the other hypotheses are not significant. Training is the most prominent positive factor affecting self-efficacy and self-efficacy has a significant effect on employee performance at RSUD M.Th. Djaman. The results of this study can be used as a reference by management in determining what policy priorities should take precedence.

Self-assembly and Mechanism of L-Alanine-based Dihydrazide Derivative as Excellent Gelator of Organic Solvents

  • Wang, Chuan-Sheng;Wang, Xiao-Hong;Li, Zhi-Yuan;Wei, Wei;Shi, Zhong-Liang;Sui, Zhi-Tong
    • Bulletin of the Korean Chemical Society
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    • 제32권4호
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    • pp.1258-1262
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    • 2011
  • A new organogelator, L-Alanine dihydrazide derivative can self-assemble in various organic solvents and turned them into thermally reversible physical supramolecular organogels at extremely low concentrations (< 2 wt %). The gel-sol phase transition temperatures ($T_{GS}$) were determined as a function of gelator concentration and the corresponding enthalpies (${\Delta}H_g$) were extracted. Scanning electron microscopy (SEM) measurements revealed that the interspaces of fiber-like network structures were diminished with the increasing of the LMOG concentration. FT-IR spectroscopy studies revealed that hydrogen-bonding and hydrophobic interaction were the driving forces for the formation of the gels. Based on the data of XRD and molecular modeling, the possible packing modes for the formation of organogelator aggregates were proposed.

폴리케톤 섬유의 UV 및 산처리에 의한 표면개질 (Surface Modification of Polyketone Fibers by UV irradiation and Acid treatment)

  • 최혜영;이태상;이종;이승구
    • 한국염색가공학회:학술대회논문집
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    • 한국염색가공학회 2011년도 제44차 학술발표회
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    • pp.69-69
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    • 2011
  • 폴리케톤 섬유는 제조 원료로 에틸렌과 일산화탄소를 사용하여 합성한 공중합체 물질로 생산에 필요한 비용을 크게 절약할 수 있다. 폴리케톤 섬유는 p-아라미드 섬유에 근접하는 고강도 고탄성을 가진 섬유로 우수한 내화학성을 가지며, 고무와의 계면접착이 우수하다는 특성을 가지고 있어 MRG(Mechanical Rubber Goods)용 보강재 및 타이어코드로의 사용에 대한 관심이 증대하고 있다. 그러나 폴리케톤 섬유의 생산 및 산업현장에서의 활용은 아직 적은 상태로 그 특성에 대한 연구가 미흡한 상태이다. 따라서 본 연구에서는 폴리케톤 섬유의 기본적인 특성 분석을 하고, 폴리케톤 소재의 표면을 UV 조사와 인산을 이용한 산처리 방법을 이용하여 처리하고 표면처리에 따른 폴리케톤 섬유의 표면특성 및 물성특성을 분석하였다. UV 조사 처리시 에너지 변화와 산처리시의 pH조건 및 처리시간의 변화에 따른 표면의 미세구조를 SEM과 AFM 등을 이용하여 관찰한 결과, UV 에너지와 산처리 조건의 증가에 따라 표면요철이 증가를 보이다가 과도한 처리에 의하여 표면에 degradation이 발생하였다. 또한 UV 에너지 및 산처리 조건에 따른 열적, 화학적 그리고 물리적 특성의 변화를 분석하였다.

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Effect of laser shock peening and cold expansion on fatigue performance of open hole samples

  • Rubio-Gonzalez, Carlos;Gomez-Rosas, G.;Ruiz, R.;Nait, M.;Amrouche, A.
    • Structural Engineering and Mechanics
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    • 제53권5호
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    • pp.867-880
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    • 2015
  • Mechanical fastening is still one of the main methods used for joining components. Different techniques have been applied to reduce the effect of stress concentration of notches like fastener holes. In this work we evaluate the feasibility of combining laser shock peening (LSP) and cold expansion to improve fatigue crack initiation and propagation of open hole specimens made of 6061-T6 aluminum alloy. LSP is a new and competitive technique for strengthening metals, and like cold expansion, induces a compressive residual stress field that improves fatigue, wear and corrosion resistance. For LSP treatment, a Q-switched Nd:YAG laser with infrared radiation was used. Residual stress distribution as a function of depth was determined by the contour method. Compact tension specimens with a hole at the notch tip were subjected to LSP process and cold expansion and then tested under cyclic loading with R=0.1 generating fatigue cracks on the hole surface. Fatigue crack initiation and growth is analyzed and associated with the residual stress distribution generated by both treatments. It is observed that both methods are complementary; cold expansion increases fatigue crack initiation life, while LSP reduces fatigue crack growth rate.

Piezoelectric friction dampers for earthquake mitigation of buildings: design, fabrication, and characterization

  • Chen, Genda;Garrett, Gabriel T.;Chen, Chaoqiang;Cheng, Franklin Y.
    • Structural Engineering and Mechanics
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    • 제17권3_4호
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    • pp.539-556
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    • 2004
  • In this paper, the design, fabrication and characterization of a piezoelectric friction damper are presented. It was sized with the proposed practical procedure to minimize the story drift and floor acceleration of an existing 1/4-scale, three-story frame structure under both near-fault and far-field earthquakes. The design operation friction force in kip was numerically determined to range from 2.2 to 3.3 times the value of the peak ground acceleration in g (gravitational acceleration). Experimental results indicated that the load-displacement loop of the damper is nearly rectangular in shape and independent of the excitation frequency. The coefficient of friction of the damper is approximately 0.85 when the clamping force on the damper is above 400 lbs. It was found that the friction force variation of the damper generated by piezoelectric actuators with 1000 Volts is approximately 90% of the expected value. The properties of the damper are insensitive to its ambient temperature and remain almost the same after being tested for more than 12,000 cycles.