• Title/Summary/Keyword: SEM $T_g

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Optimization of FSW of Nano-silica-reinforced ABS T-Joint using a Box-Behnken Design (BBD)

  • Mahyar Motamedi Kouchaksarai ;Yasser Rostamiyan
    • Advances in nano research
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    • v.14 no.2
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    • pp.117-126
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    • 2023
  • This experimental study investigated friction stir welding (FSW) of the acrylonitrile-butadiene-styrene (ABS) T-joint in the presence of various nano-silica levels. This study aim to handle the drawbacks of the friction stir welding (FSW) of an ABS T-joint with various quantity of nanoparticles and assess the performance of nanoparticles in the welded joint. Moreover, the relationship between the nanoparticle quantity and FSW was analyzed using response surface methodology (RSM) Box-Behnken design. The input parameters were the tool rotation speed (400, 600, 800 rpm), the transverse speed (20, 30, 40 mm/min), and the nano-silica level (0.8, 1.6, 2.4 g). The tensile strength of the prepared specimens was determined by the universal testing machine. Silica nanoparticles were used to improve the mechanical properties (the tensile strength) of ABS and investigate the effect of various FSW parameters on the ABS T-joint. The results of Box-Behnken RSM revealed that sound joints with desired characteristics and efficiency are fabricated at tool rotation speed 755 rpm, transverse speed 20 mm/min, and nano-silica level 2.4 g. The scanning electron microscope (SEM) images revealed the crucial role of silica nanoparticles in reinforcing the ABS T-joint. The SEM images also indicated a decrease in the nanoparticle size by the tool rotation, leading to the filling and improvement of seams formed during FSW of the ABS T-joint.

Adsorption and Antibacterial Properties of Metal Ion Treated Activated Carbon Fiber (금속이온이 처리된 활성탄소섬유의 흡착과 항균성)

  • Oh, Won-Chun;Bang, Seong-Ho
    • Analytical Science and Technology
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    • v.13 no.2
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    • pp.131-135
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    • 2000
  • We studied adsorption isotherm, surface properties and antibacterial activity of Cu treated activated carbon fiber (ACF). The BET surface area of Cu treated ACF are distributed to $688.2-887.8m^2/g$. The adsorption results show that BET surface areas move gradually to lower value with increasing treated Cu mole concentration. Using t-method, the specific micropore volumes and average pore size were obtained. From the SEM study, it is also observed that many of micropores in activated carbon fiber are blocked surface after the treatment. And we also observed that the activity of E. coli in kind of colon bacillus increases gradually to larger range with increasing Cu mole ratio. From these results, we suggest the antibacterial mechanism for metal treated ACF.

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Effect Of $Al_2O_3$on the Crystallization Of MgO-CaO-${SiO_2}-{P_2O_5}$ Bioglass-Ceramic System (I) (MgO-CaO-${SiO_2}-{P_2O_5}$계 Bioglass-Ceramic의 결정화에 미치는 $Al_2O_3$ 첨가의 영향(I))

  • 이민호;배태성
    • Journal of Biomedical Engineering Research
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    • v.15 no.2
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    • pp.189-194
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    • 1994
  • Effects of ${AI_2O_3}/{P_2O_5}$ ratio on the crystallization of a series of glasses with the nominal composition of 41.4wt % $SiO_2$, 35.0wt % CaO, 20.6wt % (${P_2O_5}$+${AI_2O_3}$) and 3.0wt% MgO were investigated with DTA, XRD and SEM. The major crystalline phases are apatite and anorthite. The glass transition temperature ($T_g$) and the softening point ($T_s$) are shifted to the upper temperature by increasing $AI_2O_3$ content. The temperature of apatite crystallization ($T_{p1}$) is increased by $AI_2O_3$ content, but the tempera¬ture of anorthite crystallization ($T_{p2}$) is not affected significantly. With increased of $AI_2O_3$, the apatite crystallization is decreased, but anorthite crystallization is increased.

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The physicochemical properties and the antibacterial effects of Ag-treated activated carbon (은이 처리된 활성탄의 물리화학적 특성과 항균 특성)

  • 오원춘;김범수;오한준;김면건
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.9 no.3
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    • pp.339-346
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    • 1999
  • We studied th physicochemical properties and the antibacterial effects of the Ag-treated activated carbon. The adsorption isotherms for the series of Ag-impregnated activated carbons represented typical Type-I. The surface area of the impregnated carbon was in the range of $740~1110\;m^{2}/g$, while the surface area of starting materials was $1440\;m^{2}/g$. Using t-plot, ${\alpha}_{s}$}-plot as well as DR-plot, and the volume of micropore was obtained. From the SEM study, the highly developed porous structure and the homogeneous distribution of Ag on the surface of activated carbon were confirmed. Finally, antibacterial effects of Ag-treated carbon aginst E. coli was discussed.

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Static analysis of shear-deformable shells of revolution via G.D.Q. method

  • Artioli, Edoardo;Viola, Erasmo
    • Structural Engineering and Mechanics
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    • v.19 no.4
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    • pp.459-475
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    • 2005
  • This paper deals with a novel application of the Generalized Differential Quadrature (G.D.Q.) method to the linear elastic static analysis of isotropic rotational shells. The governing equations of equilibrium, in terms of stress resultants and couples, are those from Reissner-Mindlin shear deformation shell theory. These equations, written in terms of internal-resultants circular harmonic amplitudes, are first put into generalized displacements form, by use of the strain-displacements relationships and the constitutive equations. The resulting systems are solved by means of the G.D.Q. technique with favourable precision, leading to accurate stress patterns.

Piezothermoelastic solution for angle-ply laminated plate in cylindrical bending

  • Dube, G.P.;Upadhyay, M.M.;Dumir, P.C.;Kumar, S.
    • Structural Engineering and Mechanics
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    • v.6 no.5
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    • pp.529-542
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    • 1998
  • Generalised plane strain solution is presented for simply supported, angle-ply laminated hybrid plate under cylindrical bending. The arbitrary constants in the general solution of the governing differential equations are obtained from the boundary and interface conditions. The response of hybrid plates to sinusoidal loads is obtained to illustrate the effect of the thickness parameter and the ply-angle. The classical lamination theory and the first order shear deformation theory are also assessed.

Effect of Zeolite Filler on the Thermal and Mechanical Properties of Cellulose Diacetate (Cellulose Diacetate의 열적 및 기계적 물성에 미치는 Zeolite 충전효과)

  • Lee, Chang-Kyu;Cho, Mi-Suk;Kim, In-Hoi;Nam, Jae-Do;Lee, Young-Kwan
    • Polymer(Korea)
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    • v.33 no.3
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    • pp.243-247
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    • 2009
  • Cellulose diacetate (CDA) was plasticized with triacetine (TA) and epoxidized soybean oil (ESO) in a high speed mixer. Composites of plasticized CDA and zeolite were prepared by a melting process. The $T_g$ value, $106^{\circ}C$ of the plasticized CDA was confirmed by DMA analysis. The $T_g$ value of the CDA with 50% zeolite was $125^{\circ}C$. As the content of zeolite was increased from 10 to 50% the modulus of the composite was increased from 1.7to 3.6 GPa by two times over the plasticized CDA, and its tensile strength was increased to 62 MPa and then decreased down 51 MPa, and its elongation was increased to 10% and then decreased down 3.2%. In the SEM image, the compatibility between CDA and zeolite was observed. Increasing the amount of zeolite in the composites resulted in further enhancement of the $CH_3COOH$ absorption effects.

A Study on the Structure Properties of Amorphous $As_{40}Se_{50-x}S_{x}Ge_{10}$ Thin Film (비정질 $As_{40}Se_{50-x}S_{x}Ge_{10}$ 박막의 구조특성에 관한 연구)

  • 김종빈;정홍배
    • Journal of the Korean Institute of Telematics and Electronics A
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    • v.29A no.11
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    • pp.106-112
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    • 1992
  • In this paper, we analyze the structure characteristics of $As_{40}Se_{50-x}S_{x}Ge_{10}$ system bulk and thin films. As the results of XRD patterns, it identified amorphous state. In order to find the glass transition temperature($T_g$), crystallization($T_c$) and melting point ($T_m$)of bulk sample, it ascertained that TS1gT is 238$^{\circ}C$ in $As_{40}Se_{15}S_{35}Ge_{10}$, and 231$^{\circ}C$ in $As_{40}Se_{25}S_{25}Ge_{10}$ & $As_{40}Se_{50}Ge_{10}$ following the thernal analysis by DSC, DTA, & TGA method. Also it was confirmed the phase seperation of continuous phase and dispertion phase by the optical texture of polarizing microscope and $T_g$ near 20$0^{\circ}C$ in thin film. Therefore, it was found that it occurs the phase seperation of Ge-rich dontinuous phase and Se-rich dispersion phase following the EDS analysis of thin film and the surface SEM photograph.

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