• 제목/요약/키워드: SBN

검색결과 80건 처리시간 0.029초

Crystallization and Electrical Properties of SBN60 Thin Films Prepared by Ion Beam Sputter Deposition

  • Jang, Jae-Hoon;Jeong, Seong-Won;Lee, Hee-Young
    • Transactions on Electrical and Electronic Materials
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    • 제6권1호
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    • pp.10-13
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    • 2005
  • $Sr_{0.6}Ba_{0.4}Nb_{2}O_{6}$, hereafter SBN60, thin films of 300 nm thickness were deposited using ion beam sputtering technique, in which sintered ceramic target of the same composition was utilized and the $Ar:O_{2}$ gas ratio was controlled during deposition onto $Pt(100)/TiO_{2}/SiO_{2}/Si$ substrate. Crystallization and orientation behavior as well as electrical properties of the films were examined after annealing treatment at $650{\sim}800{\cric}C$. It was found that the film orientation was dependent upon $Ar:O_{2}$ratio, in which strong (00l) orientation was developed when the gas ratio was about 1:4 at $4.3{\times}10^{-4}$ torr. Typical remanent polarization (2Pr), the coercive field (Ec) and the dielectric constant of Pt/SBN60/Pt thin film capacitor were approximately $10{\mu}C/cm^{2}$, 60 kV/cm, and 615, respectively.

혼합하중 조건하에서 갈색산화물이 입혀진 구리계 리드프레임/EMC 계면의 파손경로 (Failure Path of the Brown-oxide-coated Copper-based Leadframe/EMC Interface under Mixed-Mode Loading)

  • 이호영
    • 한국표면공학회지
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    • 제36권6호
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    • pp.491-499
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    • 2003
  • Copper-based leadframe sheets were oxidized in a hot alkaline solution to form brown-oxide layer on the surface and molded with epoxy molding compound (EMC). The brown-oxide-coated leadframe/EMC joints were machined to form sandwiched double-cantilever beam (SDCB) specimens and sandwiched Brazil-nut (SBN) specimens for the purpose of measuring the fracture toughness of leadframe/EMC interfaces. The SDCB and the SBN specimens were designed to measure the fracture toughness of the leadframe/EMC interfaces under nearly mode-I loading and mixed-mode (mode I + mode II) loading conditions, respectively. Fracture surfaces were analyzed by various equipment such as glancing-angle XRD, SEM, AES, EDS and AFM to elucidate failure path. Results showed that failure occurred irregularly in the SDCB specimens, and oxidation time of 2 minutes divided the types of irregular failures into two classes. The failure in the SBN specimens was quite different from that in the SDCB specimens. The failure path in the SBN specimens was not dependent on the phase angle as well as the distance from tips of pre-cracks.

구리계 리드프레임/EMC 접합체의 파괴거동 (Fracture Behavior of Cu-based leadframe/EMC joints)

  • 이호영;유진
    • 한국재료학회지
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    • 제10권8호
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    • pp.551-557
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    • 2000
  • 구리계 리드페임의 표면에 흑생산화물을 형성시키기 위하여 알칼리 용액에 담궈 산화시킨후 EMC(epoxy molding compound)로 몰딩하였고 기계적 가공을 하여 SDCB(sandwiched double-cantilever beam) 및 SBN(sandwiched Brazil-nut)시편을 만들었다. SDCB와 SBN 시편은 리드프레임/EMC 계면의 접착력을 각각 준 mode I 하중 및 혼합모드 하중 하에서 파괴인성치로 측정하기 위하여 고안되었다. 파괴경로를 밝혀내기 위하여 접착력 츨정 후에 얻어진 파면에 대하여 glancing-angle XRD, SEM, AFM, EDS 및 AES를 이용하여 분석하였다. SDCB 실험 후의 파면은 파괴되는 양상에 따라 세 가지 형태로 나눌 수 있었으며, 각 형태는 리드프레임의 접착전 표면 산화물 형성 상태와 밀접한 관계가 있었다. SBN 실험 후의 파면은 균열에서 가까운 부분과 먼 부분으로 나누어지는 특징을 보였는데, 이는 동적 파괴 효과(dynamic fracture effect)에 기인하는 것이라 생각된다. 또한 위상각에 따라 확실히 다른 파괴 양상을 보였는데, 이는 위상각에 따라 mode II 성분이 변하기 때문으로 생각된다.

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Aerosol deposition을 이용한 $SrBi_2Nb_2O_9$의 고정화에 의한 광촉매 특성에 관한 연구 (Phtocatalytic Activity of the $SrBi_2Nb_2O_9$ Thick Film by Aerosol Deposition)

  • 김지호;최덕균;황광택;고상민;조우석;김진호
    • 한국수소및신에너지학회논문집
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    • 제21권5호
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    • pp.375-382
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    • 2010
  • A layered perovskite photocatalysts, $SrBi_2Nb_2O_9$ (SBN), was synthesized by the conventional solid-state reaction method and characterized by X-ray diffraction (XRD) and UV-visble spectrophotometry. The results showed that the structure of $SrBi_2Nb_2O_9$ is orthorhombic. Diffuse reflectance spectra for calcined and attrition-milled SBN showed the main absorption edges were less 400 nm, that is ultraviolet region. SBN under micron-sized powder was deposited on the $Al_2O_3$ by room temperature powder spray in vacuum process, so called aerosol deposition (AD), and nano-grained $SrBi_2Nb_2O_9$ photocatalytic thick film was fabricated. AD-deposited SBN thick films were characterized by XRD, scanning electron microscopy (SEM) and UV-visable spectrophotometry, Moreover, it was found that several nano-sized SBN film by AD process can improve the photocatalytic activity under visable reflectance.

RF 스퍼터링법에 의한 세라믹 박막의 표면형상 및 구조 (Suface Morphology and Structure of Ceramic Thin Film by RF Sputtering Method)

  • 김진사;조춘남;최운식;송민종;소병문;김충혁
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2009년도 제40회 하계학술대회
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    • pp.1248_1249
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    • 2009
  • The $Sr_{0.7}Bi_{2.3}Nb_2O_9$(SBN) thin films are deposited on Pt-coated electrode(Pt/Ti/$SiO_2$/Si) using RF sputtering method with RF power and Ar/$O_2$ ratio. The size of grain of SBN thin films were increased with the increase of Ar/$O_2$ ratio and RF power respectively. Also, the crystallinity of SBN thin films were increased remarkably at RF power and Ar/$O_2$ ratio were 80[W] and 80/20, respectively.

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