• Textile Coloration and Finishing
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• v.22 no.4
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• pp.341-348
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• 2010

Sodium sulfate is commonly added in reactive dyebath in order to increase substantivity of the reactive dye to cellulose fiber by reducing repulsion between anionic dye and fiber. While sodium sulfate is mostly used in solid form, it is inconvenient to dissolve a large amount of powder sodium sulfate. Furthermore, if there is undissolved salt in dyebath it might cause unlevel dyeing. In this study, sodium sulfate in liquid or solid form was used in dyeing of cellulose fabric with reactive dyes of three primary color and the effect of type or amount of sodium sulfate on dyeing and fastness properties was investigated. When the amount of sodium sulfate rose to 30-50 g/l, K/S value of the dyed fabric markedly increased; further rise in sodium sulfate concentration resulted in slow increase in K/S value. For light color, optimum amount was about 30 g/l in solid form and 50-100 g/l in liquid form while, for medium to deep color, it was 50 g/l and 100-150 g/l in solid and liquid form, respectively. When using each optimum amount of salt in solid or liquid form for medium color, shape of dyeing curve as well as exhaustion was similar to each other. On the whole, similar color fastness results were obtained regardless of type or amount of sodium sulfate.

• Journal of Fashion Business
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• v.18 no.5
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• pp.69-81
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• 2014

Fabric made of 100% silk was dyed with Undaria pinnatifida extracts under different conditions such as varing colorant concentration, temperature, time and dyebath pH. The dye uptake (K/S, value), CIE L*,a*,b* and Munsell values of the dyed samples and mordanted samples were measured. Colorfastness, antibacterial property and UV protection property were also evaluated. As colorants concentration increased, the dye uptake increased progressively and maximum color strength was obtained at 100% V/V. Dye uptake also increased with increasing temperature and time, and the maximum color strength was obtained at $80^{\circ}C$ and 60min. With pre-mordanting, the color of the Al and Fe mordanted silk fabrics was yellow on the Munsell color system, while the Cu mordanted fabric was a greenish color. Al and Fe post-mordanted fabrics had a yellow tone, and the Cu post-mordanted fabric had a yellow greenish tone. The light fastness property of the Cu mordanted silk fabric was relatively good, The effect of Al and Fe mordanting on fastness was insignificant. The antibacterial activity of dyed and unmordanted silk fabric was excellent, whereas fabric dyed and mordanted with Undaria pinnatifida extract demonstrated superior ultraviolet protection.

• Journal of Chest Surgery
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• v.30 no.5
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• pp.540-543
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• 1997

In this paper, we present an extremely rare case of a primary intrapulmonary neurogenic tumor, in which localization of S-100 protein was investigated using immunohistochemical staining. The patient, who was a 47 year old man, experienced no symptoms, however, a routine chest X-ray revealed a round tumor like shadow in the hilar area of left lung. To confirm and cure the mass, surgery was performed. Histopathological examination of the excised tumor revealed it to be a primary intrapulmonary neurilemmoma. Immunohistochemical staining demonstrated the presen e of S-100 protein in the tumor cells.

• Textile Coloration and Finishing
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• v.32 no.2
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• pp.89-95
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• 2020

In this study, the efficacy of Amaranth(Amaranthus spp. L.) as a natural dye resource was investigated for wool fabrics. It is known that a large amount of flavonoid and anthocyanin colorant are contained in leaves and stems, as well as red flowers. The optimum condition of dyeing was 1.3% of dye concentration(o.w.b.) at 100℃ for 60 minutes, resulting the K/S value, 23.43 and R Munsell color on the wool fabrics. Al, Fe, Zinc and Titanium were used as a mordant. The mordant improved the dye uptake, regardless of the mordant type and mordant method. The pre-mordanting method was more effective than the post-mordanting method. Al pre-mordanted fabric showed the highest K/S, 30.02. Light fastness and washing fastness were high in grades 4-5 and 5, and rubbing fastness was good in grades 4 and 4-5 in dry condition, but low in grades 2-3 and 3 in wet condition. The dry cleaning fastness was excellent in all 5 grades. However, the alkaline perspiration fastness ratings were low in grades 2-3 and 3. The results show Amaranthus spp. L. colorant can be used as a functional natural dye for wool fabrics.

• Fashion & Textile Research Journal
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• v.10 no.5
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• pp.771-778
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• 2008

The natural dyeing of cotton fabric with Perilla frutescens var. acuta extract was investigated. The proper extraction temperature and time were $100^{\circ}C$ and 120 minutes. The proper temperature, time and colorant powder concentration for the dyeing of cotton fabric with Perilla frutescens var. acuta powder were $90^{\circ}C$, 60 minutes and 15%(o.w.b.), respectively. In various mordanted methods, the K/S values of simultaneous-mordanted methods were higher than those of pre-and post-mordanted methods. And the Cu-and Fe mordant showed higher K/S values than those of other mordants. Light colorfasness of mordanted cotton fabric was poor, but the other colorfasnesses were shown to be good. The cotton fabric mordanted with Cu mordant was showed effective bacterial reduction.

• Textile Coloration and Finishing
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• v.10 no.3
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• pp.50-56
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• 1998

Nonwoven fabric was treated with chitosan solution to impart antimicrobial activities by pad-dry method. Antimicrobial activity was measured by Shake Flask Method. Two chitosans of different molecular weight(Mw) with similar degree of deacetylation(DDA) were used : ca. 1,800(chitosan oligomer : DDA 84%) and 180,000(DDA 86%). Chitosan oligomer displayed high antimicrobial activity against P. vulgaris at 0.01%, S. aureus and E. coli at 0.05% treatment concentration, shelving above 90% of reduction rate. Chitosan of Mw 180,000 was effective against S. aureus, E. coil and P. vulgaris at 0.05% treatment concentration, showing almost 100% reduction rate. While chitosan of Mw 180,000 shelved reduction rate above 75% against K. pneumoniae and P. aeruginosa at 0.5% treatment concentration, chitosan oligomer was not effective against them. Fabrics become stiffer and less air permeable as treatment concentration increases. Liquid strike-through time of the sample treated with 0.5% chitosan oligomer solution (3.0 sec) was comparable with a hydrophilic finished sample commercially available(2.6 sec).

• Textile Coloration and Finishing
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• v.11 no.3
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• pp.32-40
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• 1999

Chitosan fiber was prepared by wet spinning with various draw ratio. Chitosan fiber was coated with f-carboxymethyl keratein(SCMK) by extruding chitosan solution into 1 M NaOH solution containing 1% SCMK. Among three chitosan used in this study(chitosans of 5 cps, 50 cps, 100 cps), 50 cps chitosan gave the best tenacity and optimum concentration was 5%. SCMK coating increased the tenacity of chitosan fiber. Regardless of SCMK coating, tenacity and elongation of both chitosan fibers were increased with the increase of draw ratio. Chitosan fiber showed antimicrobial activity against Staphyloccus aureus showing 66∼72% of bacteria reduction rates. On the other hand, chitosan fiber coated with SCMK didn't show any antimicrobial activity.

• Proceedings of the Korean Society of Dyers and Finishers Conference
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• 2011.03a
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• pp.52-52
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• 2011

나노필라멘트는 단면직경이 수백 나노미터에서 수십 나노미터 수준인 초극세 장섬유를 말하며, 해도형 복합방사로 얻어진 섬유를 알칼리 감량을 통해 해성분을 용출하여 도성분에 해당하는 나노필라멘트를 얻는다. 이러한 나노필라멘트사는 초극세와 마찬가지로 단위중량당 표면적이 크고, 작은 굴곡반경 및 낮은 굴곡 반발성으로 인하여 일반 합성섬유에 비하여 고가성 및 새로운 기능성을 부여하는 제품에 응용 될 수 있다. 특히 나노필라멘트를 이용한 편물제품으로 경편물은 wiping cloth 등 산업용도에 적용되며, 환편물은 인조피혁 등 의류용으로 사용된다. 나노필라멘트 편물은 원사섬도, 편물의 조직, 밀도 및 중량 등에 따라 분할율과 용출 특성이 상이하므로 후가공 공정에 있어서 감량공정은 매우 중요하다. 또한 나노필라멘트와 같은 세사의 경우 일반사보다 비표면적이 증가하여 동일한 염색조건에서 옅은 색상을 나타낸다. 이로 인해 같은 색상을 위하여 보다 많은 염료를 투입해야 하며, 결과적으로 견뢰도 문제가 발생할 우려가 있다. 이 연구에서는 해도형 나노필라멘트 PET 원사와 일반 PET사를 복합한 2종의 편물을 이용하여 알칼리감량특성 및 3가지 분산염료에 대한 염색성과 견뢰도를 조사하였다. 알칼리 처리조건에 따른 감량률을 측정함으로써 각 편물의 이론 감량률에 도달하는 지점을 확인하고, SEM사진 분석을 통하여 해도사의 감량정도 및 분할특성을 확인하였다. 나노필라멘트 편성물은 염료농도가 증가함에 따라 지속적으로 K/S 값이 증가하였으나, 전체적으로 낮은 K/S값을 얻었다. 또한 염색온도가 110에서 $100^{\circ}C$로 증가함에 따라 K/S값이 감소하였는데, 이는 고온에서 분산염료가 나노필라멘트로부터 일반 PET사로 이염이 더 많이 발생하였기 때문이라고 생각된다. 세탁견뢰도의 경우 양호 또는 우수하였으나, 일광견뢰도의 경우 1등급으로 매우 낮아 이를 개선하기 위한 노력이 향후 진행되어야 할 것이다.

• Fashion & Textile Research Journal
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• v.19 no.5
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• pp.620-625
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• 2017

In this study, the dyeing conditions(temperature, time, concentration) are changed from various conditions on wool fabrics by using corydalis tuber extract in order to develop new natural dyes. The purpose of this study is to improve the dyeability, color fastness, and functionality and to derive optimal dyeing conditions by comparing and analyzing the changes of K/S values and surface color by dyeing pH changes, mordant method, and mordant type. As a result of the experiment, the optimum dyeing condition of the wool fabrics is shown dyeing temperature:$80^{\circ}C$, dyeing time:90min, dyeing concentration:100%. The dyeability by pH variants of corydalis tuber extract indicates that K/S values is higher alkaline than acidic. The mordant method of corydalis tuber extract showed pre-mordant has high K/S values. In terms of color fastness, marked improvement has not been shown despite of mordant treatment on wool fabrics. In particular, color change of color fastness to washing, color fastness to light indicates the low fastness. In addition, the functionality such as antibacterial activities and deodorization can be given at dyeing with corydalis tuber extract thus it is expected to be applied to underwear or apparel products for the elderly and infirm and children with weak skin that required high functionality.

• Korean Journal of Food Science and Technology
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• v.31 no.3
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• pp.720-726
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• 1999

High voltage pulsed electric fields (PEF) technology is a non-thermal technique which is applicable to extract useful components froms biological materials. This research suggested the possibility for extracting carotenoid pigments from Phaffia rhodozyma by PEF treatments. The yeast cell suspensions were treated with high voltage pulses in a recycled PEF treatment chamber which consists a pair of thin plates of stainless steel adhering to a small chamber with approximately $1{\sim}4\;mm$ gap. A 2.5 log reduction in survivability and more than 98% of electropermeabilization of the yeast cells could be achieved by PEF treatment for $300\;{\mu}s$ with an electric field of 30 kV/cm and pulse duration of $1\;{\mu}s$. When the yeast cell suspended in 0.01% NaCl solution were treated with PEF under various conditions, carotenoid pigments were not extracted. However, the PEF treatment of the yeast cell suspensions in 0.01% $CaCl_2$ solution, have positive effects on the extraction of carotenoid pigments ($27.3\;{\mu}g/g$ of dried yeast).