• Title/Summary/Keyword: Room temperatures

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Improvement on the Formability of Magnesium Alloy Sheet by Heating and Cooling Method (가열냉각방법에 의한 마그네슘합금의 판재성형성 개선)

  • Kang, Dae-Min;Manabe, Ken-ich
    • Transactions of Materials Processing
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    • v.14 no.7 s.79
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    • pp.607-612
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    • 2005
  • In this paper, warm deep drawing process with local heating and cooling technique was attempted to improve the formability of AZ31 magnesium alloy which is impossibly to form by conventional methods at room temperature by finite element method and experiment. For FE analysis, in first model with considering heat transfer, both die and blankholder were heated to 573K while the punch was kept at room temperature by cooling water. Also distribution of thickness and von Mises stress at room temperature and 498k for warm deep drawing were compared by FEM. Uniaxial tension tests at elevated temperature were done in order to obtain the temperature dependence of material constant under temperature of $293K\~573K$ and cross head velocity of $5\~500mm/min$. The phenomenological model for warm deep drawing process in this work was based on the hardening law and power law strain rate dependency. Deep drawing experiment were conducted at temperatures of room temperature, 373K, 423K, 473K, 498K, 523K, and 573K for the blank and deep drawing tools(holder and die) and at a punch speed of 10mm/min.

Room Temperature Polymerization of N-vinylcarbazole in Tetrahydrofuran

  • Lyoo, Won-Seok;Kwak, Jin-Woo;Noh, Seok-Kyun;Kim, Dae-Heum;Lee, Jinwon;Kim, Nakjoong;Park, Ki-Hong;Lee, Chul-Joo
    • Fibers and Polymers
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    • v.5 no.2
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    • pp.89-94
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    • 2004
  • N-Vinylcarbazole (VCZ) was solution-polymerized in tetrahydrofuran (THF) at 25, 35, and $45^{\circ}C$ using a room temperature initiator, 2,2'-azobis(2,4-dimethylvaleronitrile) (ADMVN); the effects of amount of solvent, polymerization temperature, and initiator concentration were investigated. On the whole, the experimental results corresponded to predicted ones. Room polymerization temperature using ADMVN proved to be successful in obtaining poly(N-vinylcarbazole) (PVCZ) of high molecular weight with small temperature rise during polymerization, nevertheless of free radical polymerization by azoinitiator. The polymerization rate of VCZ in THF was proportional to the 0.47 power of ADMVN concentration. The molecular weight was higher and the molecular weight distribution was narrower with PVCZ polymerized at lower temperatures. For PVCZ prepared in THF at $25^{\circ}C$ using ADMVN concentration of 0.00005 mol/mol of VCZ, weight-average molecular weight of 221,000 was obtained, with polydispersity index of 2.05, and degree of lightness converged to about 99%.

Effect of Thermal Cycling on Shape Memory Effect and Stabilization of Parent Phase in Fe-21%Mn Alloy (Fe-21%Mn 합금의 형상기억효과와 모상의 안정화에 미치는 반복열처리의 영향)

  • Jin, W.;Choi, C.S.
    • Journal of the Korean Society for Heat Treatment
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    • v.4 no.3
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    • pp.31-38
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    • 1991
  • Effect of thermal cycling on shape memory effect and stabilization of austenite was investigated in Fe-21%Mn alloy. The thermal cyclic treatment was carried out with two types, room temperature${\leftrightarrow}215^{\circ}C$ and room temperature${\leftrightarrow}260^{\circ}C$. In case of the room temperature${\leftrightarrow}215^{\circ}C$, the SME was rapidly increased up to 3 cycles and maintained nearly constant value regardless of further cycles. In case of the room temperature${\leftrightarrow}260^{\circ}C$, however, the SME was increased with increasing the thermal cycle up to 5 cycles and decreased gradually with further cycle. The variation of the ${\varepsilon}$ martensite volume pet with the thermal cycle was in good agreement with the variation of the SME. Therefore, the change of the SME due to the cyclic treatment was explained with the change of the ${\varepsilon}$ martensite content. As the thermal cycle was increased, the $M_s$ temperature was decreased, and the $A_s$ and $A_f$ temperatures were increased, respectively.

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A Study on the Characteristics of Fire Resistance of Window Material in Compartment Fire (건물화재시 창문재료에 따른 내화특성 연구)

  • Hur, Man-Sung;Jang, Moon-Seok;Cho, Soo
    • Fire Science and Engineering
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    • v.17 no.1
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    • pp.62-67
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    • 2003
  • The full-scale compartment fire tests were carried out to evaluate the characteristics of fire resistance of window material under actual fire conditions. The room size used for full-scale room fire tests was 4 by 3.8 m with 2.4 m high ceiling. The windows with PVC, Aluminum and AL+Wood frame materials were established, sofa and mattress were used as fire sources. The window contained pair glasses with the air between 6 mm glasses. Temperatures at total 32 points in the room were measured to find the temperature distribution in the room fire. It is examined that thermal effects on window frame materials such as charring, distortion, melting, structural collapse, and other effects.

Effect of Room-temperature, Calcined Eggshell Reactants on Synthesis of Hydroxyapatite

  • Kang, Tea-Sung;Pantilimon, Cristian M.;Lee, Sang-Jin
    • Journal of the Korean Ceramic Society
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    • v.52 no.3
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    • pp.204-208
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    • 2015
  • Synthesis of hydroxyapatite (HA) was attempted through a room-temperature reaction of calcined eggshell with phosphoric acid. Ball-milled, calcined eggshell powder, which has a specific surface area of $31.6m^2/g$, was mixed with various concentrations of phosphoric acid at room temperature. The mixtures showed high reactivity and a vigorous exothermic reaction ; the reacted samples showed both $Ca(OH)_2$ and $CaHPO_4$ crystal phases. After heating at temperatures above $400^{\circ}C$, an HA crystal phase was observed in all samples. The calcined eggshell showed a pure CaO single phase, while the $Ca(OH)_2$ phase was only observed in the wet, ball-milled calcined powder. The degree of formation of the HA crystal phase increased as the phosphoric acid concentration and the heating temperature were increased. A mixture with 50 wt% phosphoric acid concentration showed a well-developed HA crystal phase after heat treatment at $800^{\circ}C$, while the formation of a more intensive amorphous phase was observed in the products of the room-temperature reaction.

Validation of Sanitation Management Standards for Vegetable Preparation with No-Cook Step Based on Microbiological Analysis (미생물 분석에 의한 채소류 비가열 조리공정의 위생관리 기준 유효성 평가)

  • Kim, Won-Kyeong;Ryu, Kyung
    • Journal of the Korean Dietetic Association
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    • v.27 no.1
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    • pp.45-58
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    • 2021
  • This study evaluated the sanitation management standards for vegetable preparation processes without a cooking stage. The aerobic plate counts (APC), coliform counts, and Escherichia coli of the samples at each production step were analyzed, and microbial growth of the samples stored at different temperatures was measured. The validation was judged in accordance with the microbial criteria stipulated by the British PHLS. After washing and disinfection, the APCs of the two samples decreased to 3~4 log CFU/g in both seasons. Compared to the purchasing stage, the decrease in coliform counts was approximately 0~3 log CFU/g in both seasons; E. coli was not detected. The initial APC and coliform levels of two vegetable samples were 4~5 log CFU/g in both seasons, with an increase of 1 log CFU/g taking more than 6 h at 25℃ and 2 h at 35℃. More than 10 h at 25℃ and 6 h at 35℃ were required to increase the E. coli O157:H7 count by 1~2 log CFU/g for two seasoned samples. In conclusion, washing and disinfection effects and changes in microbial growth during room temperature storage were similar in the two vegetables. Despite the low sanitizing effect of the two vegetables, when cut vegetables were stored under the critical limit within 2 h at two different room temperatures, seasoned lettuce and chicory were at the 'satisfactory' or 'acceptable' levels of PHLS regardless of the storage temperatures. The validation of sanitation management standards applied to vegetable preparation with the no-cook step was approved.

Low-velocity impact performance of the carbon/epoxy plates exposed to the cyclic temperature

  • Fathollah Taheri-Behrooz;Mahdi Torabi
    • Steel and Composite Structures
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    • v.48 no.3
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    • pp.305-320
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    • 2023
  • The mechanical properties of polymeric composites are degraded under elevated temperatures due to the effect of temperature on the mechanical behavior of the resin and resin fiber interfaces. In this study, the effect of temperature on the impact response of the carbon fiber reinforced plastics (CFRP) was investigated at low-velocity impact (LVI) using a drop-weight impact tester machine. All the composite plates were fabricated using a vacuum infusion process with a stacking sequence of [45/0_2/-45/90_2]s, and a thickness of 2.9 mm. A group of the specimens was exposed to an environment with a temperature cycling at the range of -30 ℃ to 65 ℃. In addition, three other groups of the specimens were aged at ambient (28 ℃), -30 ℃, and 65 ℃ for ten days. Then all the conditioned specimens were subjected to LVI at three energy levels of 10, 15, and 20 J. To assess the behavior of the damaged composite plates, the force-time, force-displacement, and energy-time diagrams were analyzed at all temperatures. Finally, radiography, optical microscopy, and scanning electron microscopy (SEM) were used to evaluate the effect of the temperature and damages at various impact levels. Based on the results, different energy levels have a similar effect on the LVI behavior of the samples at various temperatures. Delamination, matrix cracking, and fiber failure were the main damage modes. Compared to the samples tested at room temperature, the reduction of temperature to -30 ℃ enhanced the maximum impact force and flexural stiffness while decreasing the absorbed energy and the failure surface area. The temperature increasing to 65 ℃ increased the maximum impact force and flexural stiffness while decreasing the absorbed energy and the failure surface area. Applying 200 thermal cycles at the range of -30 ℃ to 65 ℃ led to the formation of fine cracks in the matrix while decreasing the absorbed energy. The maximum contact force is recorded under cyclic temperature as 5.95, 6.51 and 7.14 kN, under impact energy of 10, 15 and 20 J, respectively. As well as, the minimum contact force belongs to the room temperature condition and is reported as 3.93, 4.94 and 5.71 kN, under impact energy of 10, 15 and 20 J, respectively.

Effects of Storage Time and Temperature on the Hygienic Quality of Shell Eggs (계란의 저장·보관 조건에 따른 위생적 품질 변화)

  • Kim, Jong-Gyu;Park, Jeong-Yeong;Kim, Joong-Soon
    • Journal of Environmental Health Sciences
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    • v.41 no.6
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    • pp.438-448
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    • 2015
  • Objectives: This study was performed to examine the effects of storage time and temperature and their interaction on the hygienic quality parameters of shell eggs. Methods: Eggs from 40-week-old Hy-Line Brown hens were sampled immediately after being laid and subjected to storage periods of four weeks at a refrigerated temperature ($4-5^{\circ}C$) or room temperature ($13.0-19.7^{\circ}C$). Interior/exterior qualities were examined every one week. Results: Weight loss was 2.4-3.1%. The initial specific gravity of the eggs was maintained until one week at both temperatures. Air cell size exceeded 4 mm when stored for one week at room temperature, and two weeks at refrigerated temperature. Albumen index and Haugh unit were significantly decreased at both temperatures after one week (p<0.001). Rapidly increased pH of the albumen with one week of storage was observed, regardless of temperature (p<0.001). Extension of the storage for up to four weeks at room temperature resulted in remarkable deterioration of eggshell quality and instrumental color as redness (a). Air cell size, albumen and yolk indices, Haugh unit, pH of albumen and yolk were found to be influenced by storage time and temperature (p<0.001). Interaction effects between storage time and temperature were also significant for air cell size, pH of albumen and yolk (p<0.001). Conclusion: The results suggest that air cell size and pH of albumen and yolk were important parameters influenced by storage time and temperature in shell eggs. Storage time was more influential for air cell size, and temperature for the pH of yolk. Both variables almost equally influenced the pH of albumen.

Pressure fluctuations of the hot cathode ionization gauges at the stainless steel high vacuum chamber according to room temperature variations (스테인레스 스틸 고진공용기에 부착된 열음극 전리진공게이지의 주변 온도변화에 따른 압력요동)

  • ;;;;Ichiro Arakawa
    • Journal of the Korean Vacuum Society
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    • v.13 no.2
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    • pp.54-58
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    • 2004
  • Three hot cathode ionization gauges (HCIG) were used to study their responses of pressure measurements at the stainless steel high vacuum (HV) chamber around room temperatures. The pressure variations of HV measured by the three HCIGs between $20 ^{\circ}C$ and $26 ^{\circ}C$ were 5.0 %, 5.3 %, and 10.3 %, respectively. However, pressure differences between $21.5 ^{\circ}C$ and $22.5^{\circ}C$ were lower than the gauges uncertainty limits. The pressure variations of the HCIGs at the HV chamber was not directly affected by gauge characteristics, but pressure changes due to room temperatures.

Thermophysical Properties of $UO_2$ Fuel Materials

  • Lee, Hung-Joo;Kim, Chul-Whan
    • Nuclear Engineering and Technology
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    • v.8 no.2
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    • pp.81-88
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    • 1976
  • A flash method for measuring the unknown thermal property (the density, specific heat, or thermal diffusivity could be chosen as unknown) is described. The thermal diffusivity of UO$_2$ fuel samples is obtained from room temperature (300 K) to high temperature (1400 K). The specific heat is measured using a commercially available differential scanning calorimeter from room temperature to 500 K. The thermal conductivity of UO$_2$ fuel samples is calculated from the density, thermal diffusivity, and specific heat at constant pressure. The present results are in complete agreement with the usual trends for the thermal conductivity of dielectric materials, in which impurity levels are very important at low temperatures but become relatively unimportant at high temperatures. In addition, the thermal diffusivity values at room temperature are reexamined by measuring the thermal diffusivity of several UO$_2$ fuel samples with same level of doped Gd$_2$O$_3$.

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