• Nuclear Engineering and Technology
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• 제27권6호
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• pp.825-832
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• 1995

SA508 Cl.3 원자로 압력용기강에서 하중변수와 온도가 공기 중에서 피로 균열성장률에 미치는 영향에 대하여 조사하였다. 피로 균열성장률 시험은 12.7mm 두께의 CT(compact tension) 시편을 이용하였으며, 균열길이 추정은 컴플라이언스 방법을 사용하였다. 시험은 0.1, 0.5 하중비와 1, 10Hz의 하중주파수로 상온에서 40$0^{\circ}C$ 까지 온도를 변화시키면서 수행하였다. 12$0^{\circ}C$ 이하의 비교적 낮은 온도에서는 피로균열전파속도는 하중주파수와 온도에 영향을 받지 않았지만, 12$0^{\circ}C$이상의 경우 피로 균열성장률은 온도가 높을수록, 하중주파수가 낮을수록 증가하였다. 이러한 피로균열진전속도의 빨라짐은 균열선단에서의 산화속도의 증가로 인한것으로 생각된다. 또한 하중비의 영향으로 균열닫힘과 산화의 상호작용으로 피로 균열성장률은 상온에서 두드러졌다.

• 한국진공학회지
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• 제6권S1호
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• pp.96-109
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• 1997

In order to simulate the corrosion behavior of Zr-4 alloy in pressurized water reactors it was implanted (or bombarded) with 190ke V $Zr^+\; and \;Ar^+$ ions at liquid nitrogen temperature and room temperature respectively up to a dose of $5times10^{15} \sim 8\times10^{16} \textrm{ions/cm}^2$ The oxidation behavior and electrochemical vehavior were studied on implanted and unimplanted samples. The oxidation kinetics of the experimental samples were measured in pure oxygen at 923K and 133.3Pa. The corrosion parameters were measured by anodic polarization methods using a princeton Applied Research Model 350 corrosion measurement system. Auger Electron Spectroscopy (AES) and X-ray Photoelectric Spectroscopy (XPS) were employed to investigate the distribution and the ion valence of oxygen and zirconium ions inside the oxide films before and after implantation. it was found tat: 1) the $Zr^+$ ion implantation (or bombardment) enhanced the oxidation of Zircaloy-4 and resulted in that the oxidation weight gain of the samples at a dose of $8times10^{16}\textrm{ions/cm}^2$ was 4 times greater than that of the unimplantation ones;2) the valence of zirconium ion in the oxide films was classified as $Zr^0,Zr^+,Zr^{2+},Zr^{3+}\; and \;Zr^{4+}$ and the higher vlence of zirconium ion increased after the bombardment ; 3) the anodic passivation current density is about 2 ~ 3 times that of the unimplanted samples; 4) the implantation damage function of the effect of ion implantation on corrosion resistance of Zr-4 alloy was established.

• 대한기계학회논문집A
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• 제39권11호
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• pp.1091-1097
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• 2015

흑연은 우수한 열특성을 지니기 때문에 로켓 노즐목 재료로 많이 이용된다. 하지만 흑연은 소성영역을 동반하지 않으며 파괴되는 준취성 특성을 보이므로 일반구조재료와 비교해 보았을 때, 강도 관점에서 상대적으로 취약하며, $450^{\circ}C$ 이상에서 산화가 발생한다. 따라서 흑연 재료의 실구조체 적용을 위하여 이 재료에 대한 기계적 열적 특성 평가가 요구된다. 본 논문에서는 ATJ 계열 흑연의 고온파단특성에 대한 실험적인 연구를 수행하였다. 특히, 온도와 하중, 그리고 산화조건을 변수로 두어 강도 및 파단특성에 대한 상관관계를 연구하였다. 이를 위하여 ASTM 규정을 준수하여 상온, 500, $1,000^{\circ}C$에서 일축 압축 및 인장시험을 수행하였으며, 파단면은 SEM 촬영을 통하여 분석하였다.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2016년도 추계학술대회 논문집
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• pp.195-195
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• 2016

Titanium and its alloys are widely used as implants in orthopedics, dentistry and cardiology due to their outstanding properties, such as high strength, high level of hemocompatibility and enhanced biocompatibility. Hence, recent works showed that the synthesis of new Ti-based alloys for implant application involves more biocompatible metallic alloying element, such as, Nb, Hf, Zr and Mo. In particular, Nb and Hf are one of the most effective Ti ${\beta}-stabilizer$ and reducing the elastic modulus. Plasma electrolyte oxidation (PEO) is known as excellent method in the biocompatibility of biomaterial due to quickly coating time and controlled coating condition. The anodized oxide layer and diameter modulation of Ti alloys can be obtained function of improvement of cell adhesion. Silicon (Si) and magnesium (Mg) has a beneficial effect on bone. Si in particular has been found to be essential for normal bone and cartilage growth and development. In vitro studies have shown that Mg plays very important roles in essential for normal growth and metabolism of skeletal tissue in vertebrates and can be detected as minor constituents in teeth and bone. The aim of this study is to research Si and Mg doped hydroxyapatite film formation by plasma electrolytic oxidation. Ti-29Nb-xHf (x= 0, 3, 7 and 15wt%, mass fraction) alloys were prepared Ti-29Nb-xHf alloys of containing Hf up from 0 wt% to 15 wt% were melted by using a vacuum furnace. Ti-29Nb-xHf alloys were homogenized for 2 hr at $1050^{\circ}C$. Each alloy was anodized in solution containing typically 0.15 M calcium acetate monohydrate + 0.02 M calcium glycerophosphate at room temperature. A direct current power source was used for the process of anodization. Anodized alloys was prepared using 270V~300V anodization voltage at room. A Si and Mg coating was produced by RF-magnetron sputtering system. RF power of 100W was applied to the target for 1h at room temperature. The microstructure, phase and composition of Si and Mg coated oxide surface of Ti-29Nb-xHf alloys were examined by FE-SEM, EDS, and XRD.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2001년도 추계학술대회논문집A
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• pp.349-354
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• 2001

The split Hopkinson pressure bar has been used for a high strain rate impact test. Also it has been developed and modified for compression, shear, tension, elevated temperature and subzero tests. In this paper, SHPB compression tests have been performed with pure titanium at elevated temperatures. The range of temperature is from room temperature to $1000^{\circ}C$ with interval of $200^{\circ}C$. To raise temperature of the specimen, a radiant heater which is composed of a pair of ellipsoidal cavities and halogen lamps is developed at high temperature SHPB test. There are some difficulties in a high temperature test such as temperature gradient, lubrication and prevention of oxidation of specimen. The temperature gradient of specimen is affected by the variation of temperature. Barreling occurred at not properly lubricated specimen. Stress-strain relations of pure titanium have been obtained in the range of strain rate at $1900/sec{\sim}2000/sec$ and temperature at $25^{\circ}C{\sim}1000^{\circ}C$.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 2002년도 proceedings of the second asia international conference on tribology
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• pp.347-348
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• 2002

The numbers of synthetic greases have been developed with synthetic oils because of their excellent performance factors including thermal/oxidation stability, low-temperature fluidity and plastic compatibility. Long life under high-temperature condition and excellent low-temperature fluidity are required to serve as grease for bearings of engine room electrical component. As many plastics are used in place of metals for the purpose of weight saving, synthetic hydrocarbon grease is in use to avoid adverse effect on plastics. Other various special synthetic greases are also in use depending on specific requirements like conductivity and vacuum condition.

• 한국해양공학회지
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• 제16권2호
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• pp.60-66
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• 2002

The remote measurement system(RMS) as a new experimental method is limited in its application to crack measurement at elevated temperatures because of the oxide layer on the specimen surface. Since TiAIN and Cr coating layers have a high resistance to oxidation and wear, this paper proposed a TiAIN and Cr coating technique for specimens to facilitate the measurement of crack growth behavior using RMS. To investigate the effects of the coating layer, tension and fatigue tests were carried out at room temperature and at $538^{\circ}C$. The test material was 1Cr-1Mo-0.25V steel which is widely used as a turbine rotor material. From the experimental results, it was found that the mechanical properties of the TiAIN and Cr coated specimens were similar to those of the substrate. Accordingly, the TiAIN and Cr coated layer had hardly any influence on the fatigue crack propagation.

• 대한전기학회:학술대회논문집
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• 대한전기학회 1993년도 하계학술대회 논문집 B
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• pp.1177-1179
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• 1993

A study has been carried out on the characteristics of dielectric consent and the dissipation factor of Eicosamethyl Eneasiloxane as a function of frequency($30{\sim}10^5$[Hz]) and temperature(-70[$^{\circ}C$] to 65[$^{\circ}C$]). The result shows that a well-defined maxima of the absorption curves characterized by a dipole loss mechanism at a low temperature range. For temperatures in the vicinity of room temperature and higher, the loss in the range of power frequencies are predominantly of ionic nature. The increase of ionic conduction is attributed to the presence of ionizable oxidation products and their increased dissocation feature. The effect of viscosity upon the dipole loss intensity appeared to be considerably less pronounced than that upon ionic conduction loss.

• 한국세라믹학회지
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• 제34권5호
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• pp.467-472
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• 1997

Porous silicon was prepared by an anodic etching. The pore size was about 10 nm at an etching time of 20 sec and a current density of 20 mA/$\textrm{cm}^2$. The porous layer was composed of an micro-porous layer (0.6 ${\mu}{\textrm}{m}$) and a macro-porous layer (10 ${\mu}{\textrm}{m}$). Room temperature PL with maximum peak 6700$\AA$ appeared. The peak disappeared by an oxidation reaction when the porous silicon was heated to 100~20$0^{\circ}C$ in atmosphere. In order to avoid the oxidation a heat treatment was done in H2 atmosphere. The micro-pore and Si column, which formed quantum well, were collapsed by the high temperature. The PL maximum peak of heated sample was gradually red-shifted and showed about 300$\AA$ red-shift at 50$0^{\circ}C$. The intensity of PL was maintained to high temperatures in lower pressures. The porous Si was carbonized in C2H2+H2 gas in order to increase thermal stability. The carbonization of the porous Si prevented red-shift of the maximum PL peak caused by sintering effect at high temperatures, and the carbonized porous Si showed Pl signal at higher temperatures by above 20$0^{\circ}C$ than the sample in H2 atmosphere.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2006년도 춘계학술대회 논문집
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• pp.149-152
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• 2006

Dry sliding wear behavior of low carbon dual phase steel, of which microstructure consists of hard martensite in a ductile ferrite matrix, has been investigated. The wear characteristics of the dual phase steel was compared with that of a plain carbon steel which was normalized at $950^{\circ}C$ for 30min and then air-cooled. Dry sliding wear tests were carried out using a pin-on-disk type tester at various loads of 1N to 10N under a constant sliding speed condition of 0.2m/sec against an AISI 52100 bearing steel ball at room temperature. The sliding distance was fixed as 1000m for all wear tests. The wear rate was calculated by dividing the weight loss measured to the accuracy of $10^{-5}g$ by the specific gravity and sliding distance. The worn surfaces and wear debris were analyzed by SEM, EDS and a profilomter. Micro vickers hardness values of the cross section of worn surface were measured to analyze strain hardening behavior underneath the wearing surfaces. The were rate of the dual phase steel was lower than the plain carbon steel. Oxidation on the sliding surface and strain hardening were attributed for the higher wear resistance of the dual phase steel.