• Transactions of Materials Processing
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• v.26 no.5
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• pp.286-292
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• 2017

Magnesium alloy shows strong anisotropy and asymmetric behavior in tension and compression curve, especially at room temperature. These characteristics limit the application of finite element method (FEM) which is based on conventional continuum mechanics. To accurately predict the material behavior of magnesium alloy at microstructural level, a methodology of fully coupled multiscale simulation is presented and a crystal plasticity model as a constitutive equation in the simulation of metal forming process is introduced in this study. The existing constitutive equation for rigid plastic FEM is modified to accommodate deviatoric stress component and its derivatives with respect to strain rate components. Viscoplastic self-consistent (VPSC) polycrystal model was selected as a constitutive model because it was regarded as the most robust model compared to Taylor model or Sachs model. Stiffness matrix and load vector were derived based on the new approach and implemented into $DEFORM^{TM}-3D$ via a user subroutine handling stiffness matrix at an elemental level. The application to extrusion and rolling process of pure magnesium is presented in this study to assess the validity of the proposed multiscale process.

• Journal of the Korean Society for Heat Treatment
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• v.14 no.4
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• pp.212-219
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• 2001

The fatigue test was carried out to evaluate the fatigue characteristics of fire resistance steel for frame structure and heat affected zone (HAZ) by the one side Gas Metal Arc Welding (GMAW). In this paper, the fatigue crack growth behavior was investigated with the compact tension specimen of base metal and the HAZ according to chemical composition and rolling end temperature, respectively. And the acoustic emission signals obtained from the fatigue test were analyzed by the time-frequency analysis method as a nondestructive evaluation. Main results obtained are summarized as follows; The hardness was appeared softening phenomenon that weld metal and HAZ are lower than that of base metal. Fatigue life of welded specimen was longer than that of base metal. m was 3~4.5 in base metal and 3.8~5.8 in HAZ. The main frequency range of acoustic emission signal analyzed from time-frequency method is different with the range by noise and crack. Also, it could be classified that it was also generated by fracture mechanics of dimple, inclusion etc.

• Applied Microscopy
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• v.7 no.1
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• pp.45-49
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• 1977

For obtaining high manganese steel plates, the study has been made on the optimum conditions in melting, forging, rolling and water toughning treatment practices. The optimum water toughning temperature and time was found to be $1030^{\circ}C$ and 30 min. respectively for the plates of 1 mm thickness. The argon atmosphere is very effective for the prevention of decarburization which can be easily occured in open air. There is a close relation between the degree of c 이 d working and the hardess. The greater the cold reduction ratio is, the smaller the grain size is and it results in the increase of hardness. The improvement of tensile and bending properties can be made by the addition of small amount of nickel, chromium and vanadium.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2007.04a
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• pp.185-188
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• 2007

The main objective of this research effort was to develope the performance of C/SiC composites manufactured by LSI (Liquid Silicon Infiltration) method for solid and liquid rocket propulsion system and ensure the performance analysis technique. The various carbon preform were manufactured by filament winding, tape rolling, involute layup and stack molding process. For the best performance of thermal and mechanical properties, many process conditions were tested and selected by varying preform, the content of SiC, temperature, impregnation resin and chemical vapour reaction. In conclusion, the high performance and reliability of C/SiC composite were proved for solid and liquid rocket propulsion system. And the performance analysis technique related to mathematical ablation model was originated.

• Korean Journal of Materials Research
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• v.19 no.8
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• pp.432-436
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• 2009

A Cu-Fe-P copper alloy was processed by accumulative roll-bonding (ARB) for ultra grain refinement and high strengthening. Two 1mm thick copper sheets, 30 mm wide and 300 mm long, were first degreased and wire-brushed for sound bonding. The sheets were then stacked on top of each other and roll-bonded by about 50% reduction rolling without lubrication at ambient temperature. The bonded sheet was then cut into two pieces of the same dimensions and the same procedure was repeated for the sheets up to eight cycles. Microstructural evolution of the copper alloy with the number of the ARB cycles was investigated by optical microscopy (OM), transmission electron microscopy(TEM), and electron back scatter diffraction(EBSD). The grain size decreased gradually with the number of ARB cycles, and was reduced to 290 nm after eight cycles. The boundaries above 60% of ultrafine grains formed exhibited high angle boundaries above 15 degrees. In addition, the average misorientation angle of ultrafine grains was 30 degrees.

• Korean Journal of Materials Research
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• v.27 no.1
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• pp.53-61
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• 2017

Magnesium alloys are of emerging interest in the automotive, aerospace and electronic industries due to their light weight, high specific strength, damping capacity, etc. However, practical applications are limited because magnesium alloys have poor formability at room temperature due to the lack of slip systems and the formation of basal texture, both of which characteristics are attributed to the hcp crystal structure. Fortunately, many magnesium alloys, even commercialized AZ or ZK series alloys, exhibit superplastic behavior and show very large tensile ductility, which means that these materials have potential application to superplastic forming (SPF) of magnesium alloy sheets. The SPF technique offers many advantages such as near net shaping, design flexibility, simple process and low die cost. Superplasticity occurs in materials having very small grain sizes of less than $10{\mu}m$ and these small grains in magnesium alloys can be achieved by thermomechanical treatment in conventional rolling or extrusion processes. Moreover, some coarse-grained magnesium alloys are reported to have superplasticity when grain refinement occurs through recrystallization during deformation in the initial stage. This report reviews the characteristics of superplastic magnesium alloys with high-strain rate and coarse grains. Finally, some examples of SPF application are suggested.

• Nuclear Engineering and Technology
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• v.33 no.4
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• pp.397-408
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• 2001

A marine reactor shows very different thermal-hydraulic characteristics compared to a land- based reactor. Especially, study on the variation of flow field due to ship motions such as inclination, heaving and rolling is essential since the flow variation has great influence on the reactor cooling capability. In this study, the natural circulation characteristics of integral type marine reactor with modular steam generators were analyzed using computational fluid dynamics code, CFX-4, for inclined conditions. The numerical analyses are performed using the results of natural circulation experiments for integral reactor which are already conducted at Seoul National University. From the results, it was found that the flow rate in the ascending steam generator cassettes increases due to buoyancy effect. Due to this flow variation, temperature difference occurs at the outlets of the each steam generator cassettes. which is mitigated through downcomer by thermal mixing. Also, around the upper pressure header the flow from descending hot leg goes up to the ascending steam generator cassettes due to large natural circulation driving force in ascending steam generator cassettes. From this result, the increase of How rate in the ascending steam generator cassettes could be understood qualitatively.

• Transactions of Materials Processing
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• v.18 no.1
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• pp.45-51
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• 2009

Shape memory alloy has been used to improve the tensile strength of composite by the occurrence of compressive residual stress in matrix using its shape memory effect. In order to fabricate shape memory alloy composite, TiNi alloy fiber and Al2024 sheets were used as reinforcing material and matrix, respectively. In this study, TiNi/Al2024 shape memory alloy composite was made by using hot press method. In order to investigate bonding condition between TiNi reinforcement and Al matrix, the micro-structure of interface was observed by using optical microscope and diffusion layer of interface was measured by using Electron Probe Micro Analyser. And the mechanical properties of composite with three parameters(volume fraction of fiber, cold rolling amount and test temperature) were obtained by tensile test. The most optimum bonding condition for fabrication the TiNi/Al2024 composite material was obtained as holding for 30min. under the pressure of 60MPa at 793K. The strength of composite material increased considerably with the volume fraction of fiber up to 7.0%. And the tensile strength of this composite increased with the reduction ratio and it also depends on the volume fraction of fiber.

• Membrane and Water Treatment
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• v.6 no.3
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• pp.251-262
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• 2015

In this work the preparation and characterization of a membrane containing a uniform mesoporous Titanium oxide top layer on a porous stainless steel substrate has been studied. The 316 L stainless steel substrate was prepared by powder metallurgy technique and modified by soaking-rolling and fast drying method. The mesoporous titania membrane was fabricated via the sol-gel method. Morphological studies were performed on both supported and unsupported membranes using scanning electron microscope (SEM) and field emission scanning microscope (FESEM). The membranes were also characterized using X-ray diffraction (XRD) and $N_2$-adsorption / desorption measurement (BET analyses). It was revealed that a defect-free anatase membrane with a thickness of $1.6{\mu}m$ and 4.3 nm average pore size can be produced. In order to evaluate the performance of the supported membrane, single-gas permeation experiments were carried out at room temperature with nitrogen gas. The permeability coefficient of the fabricated membrane was $4{\times}10^{-8}\;lit\;s^{-1}\;Pa^{-1}\;cm^{-1}$.

• Proceedings of the Materials Research Society of Korea Conference
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• 2009.05a
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• pp.43.2-43.2
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• 2009

니켈기 초내열합금 Inconel 617은 Cr, Mo 등의 첨가물이 함유된 고용 강화된 합금으로써, 우수한 고온 강도, 크립 저항성, 내부식성 및 내산화성을 가지고 있는 것으로 알려져 있다. 또한 Inconel 617의 주된 carbide은 $M_{23}C_6$와 미량의 $M_6C$ carbide로 형성되어있다. 본 연구에서는 냉간 압연 및 고온열화가 carbide의 크기, 분율 그리고 상 변화에 미치는 영향을 평가하였다. 냉간 압연은 50%까지 수행하였으며, 50% 냉간 압연한 시편을 $1050^{\circ}C$에서 1시간 동안 재결정을 수행하였다. 이로 인해 미세한 결정립과 carbide을 가지는 시편을 확보할 수 있었으며, as-received 시편 보다 균일하게 carbide을 분산 시킬 수 있었다. 또한 재결정 후 $950^{\circ}C$에서 고온열화에 의한 carbide의 변화를 평가함으로써, 냉간 압연 및 고온열화에 의한 carbide의 크기, 분율 그리고 상 변화에 미치는 영향을 평가할 수 있었다. Carbide의 분율을 평가하기 위하여 BSE image을 관찰하였으며, Image analyzer을 이용하여 계산되었다. 그리고 carbide의 성분 분석을 통한 $M_{23}C_6$와 $M_6C$의 상을 평가하기 위하여 EPMA 분석을 수행하였으며, carbide의 분산에 의한 균질도를 평가하기 위하여 비커스 경도를 측정하였다.