• Nano
• /
• v.13 no.12
• /
• pp.1850142.1-1850142.9
• /
• 2018

Modified titanate nanotubes (TNT) were tested for their adsorption of methylene blue (MB) from water solutions. They were obtained from the $TiO_2$ nanopowder using a standard alkaline hydrothermal method but in the stage of acid washing, when the titanate flakes begin to roll into nanotubes, magnetite nanoparticles were added. The $Fe_3O_4$ magnetic nanoparticles with diameter of around 2 nm and 12 nm were used in the tests. Significantly stronger adsorption of MB was observed when smaller nanoparticles were used compared to using larger nanoparticles and compared to the case of unmodified nanotubes. It was shown that the increased adsorption of MB is associated with a more negative value of ${\zeta}$-potential for titanates modified by the ultra-small nanoparticles. In the adsorption experiment, pH 7 was selected. These results may prove to be of great importance in the case of potential applications corresponding to the use of such material for wastewater purification.

• Korean Journal of Metals and Materials
• /
• v.49 no.11
• /
• pp.893-899
• /
• 2011

Fabrication of a complex aluminum alloy by the ARB process using dissimilar aluminum alloys has been carried out. Two-layer stack ARB was performed for up to six cycles at ambient temperature without a lubricant according to the conventional procedure. Dissimilar aluminum sheets of AA1050 and AA5052 with thickness of 1 mm were degreased and wire-brushed for the ARB process. The sheets were then stacked together and rolled to 50% reduction such that the thickness became 1 mm again. The sheet was then cut into two pieces of identical length and the same procedure was repeated for up to six cycles. A sound complex aluminum alloy sheet was successfully fabricated by the ARB process. The tensile strength increased as the number of ARB cycles was increased, reaching 298 MPa after 5 cycles, which is about 2.2 times that of the initial material. The average grain size was $24{\mu}m$ after 1 cycle, and became $1.8{\mu}m$ after 6 cycles.

• Korean Journal of Materials Research
• /
• v.32 no.10
• /
• pp.414-418
• /
• 2022

Magnesium alloy is the lightest practical metal. It has excellent specific strength and recyclability as well as abundant reserves, and is expected to be a next-generation structural metal material following aluminum alloy. This paper investigated the possibility of thin plate fabrication by applying a overheating treatment to the melt drag method, and investigating the surface shape of the thin plate, grain size, grain size distribution, and Vickers hardness. When the overheating treatment was applied to magnesium alloy, the grains were refined, so it is expected that further refinement of grains can be realized if the overheating treatment is applied to the melt drag method. By applying overheating treatment, it was possible to fabricate a thin plate of magnesium alloy using the melt drag method, and a microstructure with a minimum grain size of around 12 ㎛ was obtained. As the overheating treatment temperature increased, void defects increased on the roll surface of the thin plate, and holding time had no effect on the surface shape of the thin plate. The fabricated thin plate showed uniform grain size distribution. When the holding times were 0 and 30 min, the grain size was refined, and the effect of the holding time became smaller as the overheating treatment temperature increased. As the overheating temperature becomes higher, the grain size becomes finer, and the finer the grain size is, the higher the Vickers hardness.

• Journal of the Korean Society of Food Culture
• /
• v.24 no.3
• /
• pp.308-314
• /
• 2009

In this study, we examined the composition of catechins, theaflavins and alkaloids in leaves during processing to fermented black tea, which is produced by withering, roll breaking, and fermentation of Korean Yabukida tea plant. In addition, we determined the optimal conditions for the production of fermented black tea. The average moisture content in fresh leaves was 70.85%, which dropped to 3.07% in fermented black tea at the last stage of production. When the leaves were analyzed by HPLC, seven types of catechins, four types of theaflavins and three types of alkaloids were identified. The levels of catechins, theaflavins, and alkaloids were then evaluated after being processed into fermented tea. From these experiments, we found that the level of theaflavins, which determines the property of the tea, increased during fermentation. This effect resulted from the change in EGCG, ECG, EGC, EC during the process of fermentation. We also found that the maximal amount of theaflavins was created after 1-2 hours of fermentation. Thus, our results imply that the best condition for producing fermented black tea would be to ferment for 1-2 hours.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.27 no.11
• /
• pp.712-717
• /
• 2014

Glass ceramic has a high mechanical strength and low sintering temperature. So, it can be used as a thick film substrate or a high strength insulator. A series of glass ceramic samples based on MgO-$Al_2O_3-SiO_2-ZrO_2$ (MASZ) were prepared by melting at $1,600^{\circ}C$, roll-quenching and heat treatment at various temperatures from $900^{\circ}C$ to $1,400^{\circ}C$. Dependent on the heat treatment temperature used, glass ceramics with different crystal phases were obtained. Their nucleation behavior, microstructure and mechanical properties were investigated with differential thermal analysis (DTA), X-ray diffraction (XRD), scanning electron microscopy (SEM), and Vicker's hardness testing machine. With increasing the heat treatment temperature of MASZ samples, their hardness and toughness initially increase and then reach the maximum points at $1,300^{\circ}C$, and begin to decrease at above this temperature, which is likely to be due to the softening of glass ceramics. As the content of $ZrO_2$ in MAS glass ceramics increases from 7.0 wt.% to 13 wt.%, Vicker's hardness and fracture toughness increase from $853Kg/mm^2$ to $878Kg/mm^2$ and $1.6MPa{\cdot}m^{1/2}$ to $2.4MPa{\cdot}m^{1/2}$ respectively, which seems to be related with the nucleation of elongated phases like fiber.

• Journal of the Korea Convergence Society
• /
• v.8 no.5
• /
• pp.179-184
• /
• 2017

The cage of a tapered roller bearing keeps the gap between the rollers, which prevents friction, wear and suppresses heating. The material of the cage is changing from metal to plastic for lightening the weight. If the cage is severely deformed due to resonance, the roller may not be able to roll and even get off the cage. In this paper, the dynamic characteristics of the cage is analyzed according to the cage material. Under the assumption that a train runs at the highest speed, frequency harmonics of that speed is calculated, and the comparative analysis is carried out in order to select the optimum thickness of the cage, which is easy to change among the cage design variables for avoiding the resonance.

• Journal of Animal Environmental Science
• /
• v.5 no.2
• /
• pp.79-86
• /
• 1999

Recently more dairy farmers are interested in the utilization of stretch film for wrapping silage material. Most of stretch film are imported from abroad and one domestic product was developed, but its quality has not yet been tested. Therefore this study was executed to offer basic data on this material to the farmers. Measured items were tensile load, extension ratio, and tear propagation strength of stretch films. Comparisons were made among the white color of domestic product(Kw), and white(Fw), black (Fb) and green color(Fg) of foreign products. The result were summarized as follows: 1. Tensile loads of lengthwise direction in stretch films were 557.4, 377.4, 282.6 and 398.4kgf/$\textrm{cm}^2$ in Kw, Fw, Fb and Fg, respectively, and tensile loads of width direction were 415.9, 418.1, 360.2 and 433.0kgf/$\textrm{cm}^2$ in Kw, Fw, Fb and Fg, respectively. 2. Extension ratios of lengthwise direction were 650, 462.5, 512.5% and 537.5% in Kw, Fw, Fb and Fg, respectively, Extension ratios of width direction were 930, 962.5, 950 and 1,000% in Kw, Fw, Fb and Fg, respectively. 3 Tear propagation strength of lengthwise direction 187.9, 148.9, 157.3 and 142.8kgf/cm, and tear propagation strength of width direction were 141.4, 129.8, 140.4 and 106.6kgf/cm in Kw, Fw, Fb and Fg, respectively. 4. In the light transmittance, there was no difference between white and green color stretch film, but it was very low in black one. Therefore, it is thought that research on quality of roll bale silage treated with each stretch film would be needed.

• Polymer(Korea)
• /
• v.27 no.5
• /
• pp.436-442
• /
• 2003

Thermosetting elastomer such as EPDM (Ethylene Propylene Dien Rubber) has been applied to the sponge weatherstrip of a vehicle as a main material. However, the thermosetting elastomers have limited recycling and have brought about the environmental problems. Furthermore, many steps of the manufacturing process such as formulation, mastication and vulcanization make difficult to control uniformity of the endproducts. These problems of current EPDM weatherstrip necessitated development of a new recyclable material, Thermoplastic Vulcanizates (TPV). In this study the influence of the water contents, and the processing conditions. On the foam density and structure in water blowing process was carried out. We found that TPV also can be foamed with water, maintaining the uniformity form this study. Therefore, many inevitable problems of EPDM weatherstrip can be solved, and this new technique is expected to take a roll of making a breakthrough in the rubber industry.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 1996.05a
• /
• pp.59-62
• /
• 1996

Plasma displays (PDP) as a large area wall-hanging display device are rabidly developed with flat CRT, TPT LCD and etc. Especially, AC Plasma Display Panels(AC PDPs) have the inherent memory function which is effective for large area displays. The memory function in AC PDPs is caused by the accumulation of the electrical charge on the protecting layer formed on the dielectric layer. This MgO protective layer prevents the dielectric layer from sputtering by ion in discharge plasma and also has the additional important roll in lowering the firing voltage due to the large secondary electron emission coefficient). Until now, the MgO Protective layer is mainly formed by E-Beam evaporation. With increasing the panel size, this process is difficult to attain cost reduction, and are not suitable for large quantity of production. To the contrary, the methode of shuttering are easy to apply on mass production and to enlarge the size of the panel and shows the superior adhesion and uniformity of thin film. In this study, we have prepared MgO protective layer on AC PDP Cell by reactive magnetron sputtering and studied the effect of MgO layer on the surface discharge characteristics of ac PDP.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.36 no.12
• /
• pp.1619-1625
• /
• 2012

An electrical steel strip is commonly used as a core material in all types of electric transformers and motors. It is produced by a cold rolling process. In this paper, a damage-mechanics-based approach that predicts the edge fracture of an electrical steel strip during cold rolling is presented. We adopted the normal tensile stress criterion and the fracture energy method as a damage initiation criterion and a damage evolution scheme, respectively. We employed finite element analysis (FEA) to simulate crack initiation and propagation at the initial notch located at the edges of the strip. The material constants required in FEA were experimentally obtained by tensile tests using a standard and a notched sheet-type specimen. The results reveal that the edge crack was initiated at the entrance of the roll bite and that it rapidly evolved at the exit. The evolution length of the edge crack increased as the length of the initial notch as well as the front tension reel force of the strip increased.