• Journal of Powder Materials
• /
• v.25 no.2
• /
• pp.126-131
• /
• 2018

In the present study, we investigate the effects of milling time and the addition of a process control agent (PCA) on the austenite stability of a nanocrystalline Fe-7%Mn alloy by XRD analysis and micrograph observation. Nanocrystalline Fe-7%Mn alloys samples are successfully fabricated by spark plasma sintering. The crystallite size of ball-milled powder and the volume fraction of austenite in the sintered sample are calculated using XRD analysis. Changes in the shape and structure of alloyed powder according to milling conditions are observed through FE-SEM. It is found that the crystallite size is reduced with increasing milling time and amount of PCA addition due to the variation in the balance between the cold-welding and fracturing processes. As a result, the austenite stability increased, resulting in an exceptionally high volume fraction of austenite retained at room temperature.

• Applied Microscopy
• /
• v.52
• /
• pp.5.1-5.10
• /
• 2022

The use of Pipelines for long-distance transportation of crude oil, natural gas and similar applications is increasing and has pivotal importance in recent times. High specific strength plays a crucial role in improving transport efficiency through increased pressure and improved laying efficiency through reduced diameter and weight of line pipes. TRIP-based high-strength and high-ductility alloys comprise a mixture of ferrite, bainite, and retained austenite that provide excellent mechanical properties such as dimensional stability, fatigue strength, and impact toughness. This study performs microstructure analysis using both Nital etching and LePera etching methods. At the time of Nital etching, it is difficult to distinctly observe second phase. However, using LePera etching conditions it is possible to distinctly measure the M/A phase and ferrite matrix. The fraction measurement was done using OM and SEM images which give similar results for the average volume fraction of the phases. Although it is possible to distinguish the M/A phase from the SEM image of the sample subjected to LePera etching. However, using Nital etching is nearly impossible. Nital etching is good at specific phase analysis than LePera etching when using SEM images.

• Transactions of the Korean Society of Automotive Engineers
• /
• v.8 no.4
• /
• pp.141-148
• /
• 2000

As the steel plates used for automobile safety the TRIP-assisted multiphase steels are being introduced to automobile industry with respect to their remarkable mechanical properties for the combination of high strength and large elongation. This multiphase structure is generated by two stage heat treatment (intercritical annealing & isothermal treatment) The metastable retained austenite can be transformed to martensite when plastically deformed which results in TRIP effect. Actually the microstructure of TRIP-assisted steels consist of a fine dispersite. There present discussion deals with bainite reaction kinetics of austenite in the process o f two stage heat treatment. In relation to bainite transformation the characteristics of bainite reaction is found to be influenced by the bainite tempering temperature and also by the relative rate in which carbides precipitate within residual austenite.

• Journal of Korea Foundry Society
• /
• v.15 no.2
• /
• pp.146-155
• /
• 1995

This study was performed to investigate the effect of austempering temperature on the mechanical properties and fracture characteristics of the ductile cast iron with Cu, Mo and Cu, Mo, Ni. The results obtained from this study are summarized as follows; Microstructures of Cu-Mo and Cu-Mo-Ni ductile cast iron by austempering were obtained low bainite with some martensite at $250^{\circ}C$, mixture structure of upper and low bainite obtained at $300^{\circ}C$ and upper bainite obtained at $350^{\circ}C$. Tensile, impact and fracture toughness properties were remarkably controlled by retained austenite. With increasing austempering temperature, tensile and yield strength, hardness decreased, while the elongation and impact absorption energy, fracture toughness increased. With adding Ni, tensile and yield strength increased and elongation, facture toughness and impact absorption energy decreased. Retained austenite increased with increasing austempering temperature and the fracture surface were shown mixture structure of fibrous and dimple.

• Journal of Powder Materials
• /
• v.25 no.3
• /
• pp.220-225
• /
• 2018

The microstructure and mechanical characteristics of SUS630 specimens fabricated using the direct energy deposition (DED) process are investigated. In DED, several process parameters such as laser scan speed, chamber gas flow, powder carrier gas flow, and powder feed rate are kept fixed; the laser power is changed as 150 W, 180 W, and 210 W. As the laser power increases, the surface becomes smooth, the thickness uniformity improves, and the size and number of pores decreases. With the increase in laser power, the hardness deviation decreases and the average hardness increases. The microstructure of the material is columnar; pores are formed preferentially along the columnar interface. The lath-martensite phase governs the overall microstructure. The volumetric fraction of the retained austenite phase is measured to increase with the increase of laser input power.

• Journal of Welding and Joining
• /
• v.13 no.2
• /
• pp.122-131
• /
• 1995

The effects of cooling rate on the microstructures, precipitation of Cu-cluster, .epsilon.-Cu and impact toughness of high strength low alloy(HSLA) steel were studied using hardness tester, impact tester, DSC(differential scanning calorimetry), AES(auger electron spectroscopy) and TEM(transmission electron microscopy). Not only the Cu-precipitates but also the segregation of Cu, As, Sb, P, S, N, Sn along grain boundary were not observed at the specimens heat treated from 800.deg. C to 300.deg. C with the cooling time of 12-125 sec. The Cu-cluster, .epsilon.-Cu are formed by introducing ageing after cooling and the effect of precipitates on hardening increase after cooling was the same in all cooling rate. The peak hardness was obtained at an ageing of 500.deg. C in all cooling conditions. The impact energy become higher as the cooling time increases. This fact can be explained to be due to the tempering effect applied on the cooling stage since the present alloy has a relatively high Ms temperature and the local high concentration of the retained austenite.

• Journal of the Korean Society of Manufacturing Technology Engineers
• /
• v.8 no.1
• /
• pp.81-88
• /
• 1999

This paper was carried out to know the influence of advanced austempered ductile cast iron (ADI) on the tool life and mechanical properties of drilling machinability. For manufactured method of ADI, the spheroidal graphite cast iron were austenized at 90$0^{\circ}C$ for 1 hour and then austempered for 2 hour at 37$0^{\circ}C$ in the salt bath. And interrelationship has been investigated between tool life and mechanical characteristics of specimen material on drilling condition when the ordinary and step-feed drilling are carried out to drill holes of specimens. Tensile strength and hardness of ADI decrease and elongation of ADI increases with the increase austempered temperature. It is known that about 2 times of tool life in the case of step-feed decreases compared with ordinary feed due to the high hardness of ADI and hardness ascribed to the fact that retained austenite became to martensite state due to cutting heat in drilling. Under the constant feed rate 0.1mm/rev relation between hardness and length of end tip after drilling can be formularized to Hv=$788.46L^{-0.096}$ for the cutting speed 6.1m/min.

• Journal of the Korean Society for Heat Treatment
• /
• v.15 no.6
• /
• pp.255-259
• /
• 2002

Effect of martensite on the mechanical properties of austempered ductile cast iron was investigated after obtained the martensite by subzero treatment. Retained austenite was transformed to martensite by subzero treatment, and with decreasing subzero treatment temperature, volume fraction of martensite was increased. With increasing of the volume fraction of martensite, tensile strength was increased and elongation was decreased, ratio of increasing of strength and decreasing of elongation was higher in case of specimens with lot's of Cu contents. With increasing of the volume fraction of martensite, hardness slowly increased until only about 5% and it rapidly increased in a straight proportion when it is above 5%, while impact value was rapidly decreased until about 7% but it had a little change when it is above 7%.

• Journal of Korea Foundry Society
• /
• v.16 no.2
• /
• pp.109-115
• /
• 1996

Effect of various austempered structures on fracture characteristics of C/V graphite cast iron has studied. The tensile strength and hardness reached the maximum value of 971.4MPa and HB302 at the austempering temperature of $250^{\circ}C$, respectively. As the austempering temperature increased, the amount of retained austenite increased from 18% to 22, 29%, while $K_{IC}$ values ranged from the value of $65MPa{\cdot}m^{12} to 70MPa{\cdot}m^{1/2}, 66MPa{\cdot}m^{1/2}. This fact that $K_{IC}$ value was not sensitive to the increase of the amount of the retained austenite was that $K_{IC}$ was dependent on the matrix structure in lower bainitic matrix, while dependent on the notch effect from C/V graphite shape in upper bainitic matrix. Fractured surfaces showed a ductile fracture pattern at $300^{\circ}C$. Very large coalescence by C/V graphite and relatively small voids by spheroidal graphite were observed.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 2001.05a
• /
• pp.156-160
• /
• 2001

The effects of TRansformation Induced Plasticity(TRIP) phenomena on the plastic deformation of 0.2C-1.5Si-1.5Mn multiphase steels have been investigated at various heat treatment and stress conditions. In order to estimate the formability, the hole expansion(HE) tests and the tensile tests were carried out. The formability evaluated from the uni-axial tensile tests was quite different from the formability measured from multi-axial HE-tests. Consequently, the formability in the multi-axial stress state decreased due to the extinction of the retained austenite relatively at earlier deformation stage and the production of irregular α' martensite. However, the defects of TRIP-steels were initiated exactly at the boundary between transformed martensite and ferrite matrix regardless of stress state. In addition, new experimental formula is proposed in order to predict the multi-axial formability of the TRIP steels from the results of uniaxial tensile test.