• Title/Summary/Keyword: Resin thickness

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IN VITRO EVALUATION OF FRACTURE RESISTANCE OF VARIOUS THICKNESS FIBER- REINFORCED COMPOSITE INLAY FPD

  • Yi Yang-Jin;Yoon Dong-Jin;Park Chan-Jin;Cho Lee-Ra
    • The Journal of Korean Academy of Prosthodontics
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    • v.41 no.6
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    • pp.762-771
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    • 2003
  • Statement of problem. In dentistry, the minimally prepared inlay resin-bonded fixed partial denture (FPD) made of new ceromer / fiber-reinforced composite (FRC) was recently introduced. However, the appropriate dimensions for the long-term success and subsequent failure strength are still unknown. Purpose. The aim of this study was to investigate the most fracture-resistible thickness combination of the ceromer / FRC using a universal testing machine and an AE analyzer. Material and Methods. A metal jig considering the dimensions of premolars and molars was milled and 56-epoxy resin dies, which had a similar elastic modulus to that of dentin, were duplicated. According to manufacturer's instructions, the FRC beams with various thicknesses (2 to 4 mm) were constructed and veneered with the 1 or 2 mm-thick ceromers. The fabricated FPDs were luted with resin cement on the resin dies and stored at room temperature for 72 hours. AE (acoustic emission) sensors were attached to both ends, the specimens were subjected to a compressive load until fracture at a crosshead speed of 0.5 mm/min. The AE and failure loads were recorded and analyzed statistically. Results. The results showed that the failure strength of the ceromer/FRC inlay FPDs was affected by the total thickness of the connectors rather than the ceromer to FRC ratio or the depth of the pulpal wall. Fracture was initiated from the interface and propagated into the ceromer layer regardless of the change in the ceromer / FRC ratio. Conclusion. Within the limitations of this study, the failure loads showed significant differences only in the case of different connector thicknesses, and no significant differences were found between the same connector thickness groups. The application of AE analysis method in a fiber-reinforced inlay FPD can be used to evaluate the fracture behavior and to analyze the precise fracture point.

Color evaluation by thickness of interim restorative resin produced by digital light processing 3D printer (디지털 광학기술인 3D 프린터로 제작된 임시수복용 레진의 두께별 색 평가)

  • Kang, Wol;Kim, Won-Gi
    • Journal of Technologic Dentistry
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    • v.43 no.3
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    • pp.77-83
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    • 2021
  • Purpose: The purpose of this in vitro study was to measure and compare the thickness-dependent color dimensions of digital light processing (DLP) three-dimensional (3D) printer and conventional interim restorative resin. Methods: Specimens (N=60) were fabricated using either subtractive manufacturing (S group) or DLP 3D printing (D group) material. All milled and 3D-printed specimens were allocated into three different groups (n=10) according to different thicknesses as follows: 1.0, 1.5, and 2.0 mm. Color measurements in the CIELab coordinates were made using a spectrophotometer under room light conditions (1,003 lux). The color differences (𝚫E*) between the specimen and control target data were calculated. Data were analyzed using the oneway analysis of variance (ANOVA). Post hoc comparisons were conducted using Tukey's honestly significant difference method (α=0.05 for all tests). Results: The 𝚫L*, 𝚫a*, 𝚫b*, and 𝚫E* values of interim restorative resin produced by DLP 3D printing were obtained in terms of the specimen's thickness increased compared with the increases by subtractive manufacturing. When the thickness was similar, the color difference between subtractive manufacturing and DLP 3D printing was ≥5.5, which is a value required by the dentist for remanufacturing. Conclusion: Color was influenced by the thickness of the interim restorative resin produced by DLP 3D printing.

COLOR DIFFERNCE OF IN-CERAM BY THE VARIOUS POSTCORE MATERIALS AND COPING THICKNESS (지대치 코어 재료와 In-Ceram coping의 두께가 In-Ceram의 색에 미치는 영향)

  • Shim, Jig-Hyeon;Vang, Mong-Sook
    • The Journal of Korean Academy of Prosthodontics
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    • v.33 no.4
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    • pp.634-644
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    • 1995
  • The purpose of this study is to evaluate the color differences in the In-Ceram according to coping thickness and various abutment core materials ; amalgam, precious alloy, composite resin, non-precious alloy. After the porcelain was built up on the In-Ceram coping at the thicknes of 0.3mm and 0.5mm then it was cemented with glass ionomer cement to the post & core materials. The following results were obtained. 1. There were significant differences in the $L^*$ values $a^*$ and $b^*$ values in the cementation of different cores, to the In-Ceram(P<0.01). $L^*$ values were not significantly different between the composite resin to the In-Ceram and the $a^*\;b^*$ values were not significantly different between the amalgam and the non-precious alloy. 2. All of cementations of In-Ceram to the core materisal had color difference(${\Delta}E^*ab$) compared to the In-Ceram. In the 0.3mm thickness of the In-Ceram copping non-precious alloy indicated the greatest value, while the composite resin core showed the lowest value with a thickness of 0.5mm In-Ceram copping. 3. By controlloing the In-Ceram coping thickness $L^*$ value was significatly different(P<0.01), but not in $a^*$ and $b^*$ values. 4. In an amalgam, precious & non-prcious alloys there was a 1,74 to 3.06 range color difference in the controlled thickness of In-Ceram coping at the thickness of 0.3mm and 0.5mm. The above results suggest that the requirement of the sufficient thickness of In-Ceram coping and the suitable core material in order to get an estheti restoration by In-Ceram and also to intercept the original core color.

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Heating & Drying Characteristics of Coating Layer by Induction Heating and Short-wave Infrared Heating (유도가열 및 근적외선 가열방법에 의한 표면처리 강판 도포층의 가열 및 건조 특성)

  • Kim T. S.;Yang J. W.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2004.08a
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    • pp.249-257
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    • 2004
  • Drying and curing characteristics of PCM resins using the induction heater and short-wave infrared emitter module was studied to develop a compact oven system for the high speed CCL and post-treatment equipment. Drying of the polyester resins using the induction heater and infrared heater showed that the blistering tendency of polyester resin coating increased regardless of additives and colors of resins as the heating rate and/or dry film thickness increased. The blistering of polyester resin coating layer occurred when the heating speed was over than $25^{\circ}C/sec$ for the dry film thickness of $19\~20um$, which is the typical thickness of finish coating in CCL. So did it when the heating speed was over than $40^{\circ}C/sec$ for the dry film thickness over than 10 um. The heating efficiency of paint coated steels by the infrared heating was strongly dependent on the colors of paint coating and generally increased for the dark surface and/or coating. But the faster drying of the PCM resin coatings increased the blistering tendency of coating layer. The blistering limit for the typical finish coating by the infrared heating was estimated as the heating rate slower than $20^{\circ}C/sec$ regardless of colors of PCM resins.

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A Study on Cause of Defects in NIL Molding Process using FEM (유한요소 해석을 이용한 나노임프린트 가압 공정에서 발생하는 결함 원인에 대한 연구)

  • Song, N.H.;Son, J.W.;Kim, D.E.;Oh, S.I.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.10a
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    • pp.364-367
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    • 2007
  • In nano-imprint lithography (NIL) process, which has shown to be a good method to fabricate polymeric patterns, several kinds of pattern defects due to thermal effects during polymer flow and mold release operation have been reported. A typical defect in NIL process with high aspect ratio and low resist thickness pattern is a resist fracture during the mold release operation. It seems due to interfacial adhesion between polymer and mold. However, in the present investigation, FEM simulation of NIL molding process was carried out to predict the defects of the polymer pattern and to optimize the process by FEA. The embossing operation in NIL process was investigated in detail by FEM. From the analytical results, it was found that the lateral flow of polymer resin and the applied pressure in the embossing operation induce the weld line and the drastic lateral strain at the edge of pattern. It was also shown that the low polymer-thickness result in the delamination of polymer from the substrate. It seems that the above phenomena cause the defects of the final polymer pattern. To reduce the defect, it is important to check the initial resin thickness.

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THE FILM THICKNESS AND RETENTION OF CAST CROWN USING ADHESIVE RESIN CEMENTS (접착성 레진 시멘트를 이용한 주조관의 피막후경과 유지력에 관한 연구)

  • Jung Young-Wan;Cho Hye-Won;Jin Tai-Ho
    • The Journal of Korean Academy of Prosthodontics
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    • v.30 no.3
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    • pp.437-443
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    • 1992
  • This study was performed to investigate the availability of adhesive resin cement for luting agent of cast crown. The resin cements used in this study were Panavia-Ex(Kuraray Co., Japan) and C & B-Metabond (Parkell Bio-Materials U.S.A.). Zinc phosphate cement was Flecks zinc cement(Mizzy Inc., U.S.A.) The film thickness of cast crown at gingival margin, lateral wall and occlusal surface was observed with measuring microscope(Modek MXT 70 Matsuzawa Seiki Co., Japan) and the retention of cast crown was measured with Instron Universal Test Machine (Instron Engineering Co., U.S.A.) The results were as follows : 1. The value of retention of cast crown was the highest in the use of Panavia-EX, followed by C & B-Metabond and 2inc phosphate cement, respectively. 2. There was no difference in film thickness among the three cements, but the film thickness in all cements was highest at occlusal surface.

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Effect of Epoxy Dielectric Cooling on existing metal Porticoes in GIS (GIS내 금속이물 존재시 에폭시 절연코팅의 효과)

  • 곽희로;구교선;김영찬
    • Journal of the Korean Institute of Illuminating and Electrical Installation Engineers
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    • v.17 no.2
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    • pp.95-101
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    • 2003
  • In this paper, partial discharges(PDs), lift off and breakdown voltage were measured when metal particles existed in a model GIS coated with epoxy resin on its bottom electrode, and the measured results were analyzed after comparing with the model DIS not coated. In order to presume the various fault case in GIS, we measured the experimental values with changing some experimental factors, such as the mixture ratio of SF$\_$6//N$_2$, the pressure of the gases, the kinds and diameter of the metal particles, and the coating thickness of the epoxy resin. As a result, the PDIV increased with the thickness of the epoxy resin, while the magnitude of PDs decreased at the same condition. The lift off voltages of steel alloy particles were higher than that of copper particles, and increased wit diameter of particles. Futhermore, the lift off voltages in the case of the electrode coated with epoxy resin were higher than that in the case of the uncoated one. In addition, the thicker the thickness of the epoxy resin was, the higher the breakdown voltage were. Thus, it was confirmed that the GIS coated with epoxy resin on its inner surface could be improved in insulation performance.

Resin Impregnation of Sawdust Board for Making Woodceramics (I) - Effect of Impregnation Method and Time on Physical and Mechanical Properties -

  • Oh, Seung-Won
    • Journal of the Korean Wood Science and Technology
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    • v.32 no.3
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    • pp.25-32
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    • 2004
  • This research work explored physical and mechanical properties of impregnated sawdust boards from three softwood species (P, densifora, L. kaemferi, and P. koraiensis) with phenol-formaldehyde (PF) resin by various vacuum treatment methods of combining pressure, vacuum, and ultrasonic waves. Simultaneous vacuum and ultrasonic wave treatments with no pressure resulted in the greatest increase in resin content, density, dimensional changes (thickness and length), bending strength, and hardness of impregnated board. This result seemed to be attributed to the ultrasonic wave treatment.

Densification Characteristics of Softwood Veneers Treated by Resin Impregnation (침엽수단판의 수지함침처리에 의한 압밀화 특성)

  • 서진석
    • Journal of the Korea Furniture Society
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    • v.14 no.2
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    • pp.21-29
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    • 2003
  • This study was carried out to investigate characteristics of plywood overlaid with softwood veneers densified by resin impregnation and compression. The resin impregnability of Korean pine veneer under atmospheric pressure soaking was greater than that of larch, and impregnability of melamine resin was slightly greater than phenolic resin. It was suggested that resin impregnation ratio was affected by density and thickness of veneer. The largest melamine resin impregnation ratio of 50.7% was obtained with 1.26mm thick Korean pine veneer, and the lowest phenolic resin impregnation ratio of 11.7% with 3.41mm thick larch veneer. Therefore, it was suggested that the vacuum-pres sure-soak treatment is required at thick larch veneer. In densifying resin-impregnated veneers, densification ratio from 13.4 to 31.2% was obtained by high pressure from 15.6 to $20.8kgf/cm^2$. Impregnation of melamine resin also showed relatively greater at densification than that of phenolic resin. So it showed the degree of densification of about 20% or greater. It was seemed that adhesive bonding strength of plywood(base panel) which was directly pressed and overlaid with resin-impregnated veneer was affected by resin tackiness after resin impregnation followed by semi-drying. In laboratory scale, melamine resin impregnation was more favorable for the development of adhesive bonding strength owing to moisture control.

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A STUDY ON THE POLYMERIZATION STRESS OF COMPOSITE RESINS (복합레진의 중합수축력에 관한 연구)

  • Kim, Boo-Rang;Choi, Ho-Young;Min, Byung-Soon;Park, Sang-Jin;Choi, Gi-Woon
    • Restorative Dentistry and Endodontics
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    • v.17 no.2
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    • pp.331-341
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    • 1992
  • The purpose of this study was to measure the polymerization contraction stress of two types of composite resins; chemical cured type(Cliarfil F II, Kuraray, Japan) and photo-cured type(Photo-Clearfil Bright, Kuraray, Japan). The stresses of composite resin by contraction measured with specially designed measuring device(Fig. 1). The stresses caused by shrinkage during hardening of specimens were measured according to the type of composite resins, thickness of specimen(0.65, 1.30 and 1.95mm), and ratio of catalyst to base in case of only chemical cured composite resin(0.5, 1.0 and 1.5). As the composite resin specimen shrank on hardening, the load cell recorded force vs time automatically on pen-recorder(Toa, Japan) with a cross-head speed 60mm/hr at 0~10 voltages up to 2 hours. The experiments were conducted in a room maintained at $23{\pm}2^{\circ}C$ and relative humidity $50{\pm}10%$. The results were as follows. 1. The contraction stress during hardening was higher in photo cured composite resin than in chemical cured composite resin. 2. The contraction stress during hardening was increased with thickness of composite resin specimen. 3. In chemical cured composite resin, the polymerization contraction stress was decreased with ratio of catalyst and base. 4. The contraction stress during polymerization was higher in early time after insertion of photo cured composite resin and chemical cured composite resin.

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