• 한국염색가공학회지
• /
• 제23권2호
• /
• pp.107-117
• /
• 2011

Polyurethane (PU) was synthesized by one-shot process and the PU nanofiber was prepared by electrospinning. In this study, electrospun PU multi-membranes were prepared with various coating thickness ratio of base resin to top resin, where the base resin contains melamine curing agent and acid catalyst and the top resin contains water-repellent agent of fluoro-carbon compounds. The PU nanofiber multi-membranes were analyzed by field-emission scanning electron microscopy, differential scanning calorimeter, breathability, tensile strenth, air permeability and water resistance. The results showed that the PU multi-membrane provided excellent waterproof and moisture permeability.

• 한국복합재료학회:학술대회논문집
• /
• 한국복합재료학회 2001년도 춘계학술발표대회 논문집
• /
• pp.97-101
• /
• 2001

Composite materials have been applied widely in interior panels of buildings and transport vehicles. Recently good fire performance and weight reduction are key issues in the fields. In the present study we investigated effects of processing parameters on the performance of honeycomb sandwich panels, especially peel strength of the panel and fire performance. The processing parameters considered were types of matrix resin, resin contents, panel cure conditions, and surface painting process conditions. The results showed that the higher resin content provides the better peel strength. Controled cure steps are also needed to obtain good pee] strength. Paint processing parameters including base putty thickness and paint drying conditions and paint thickness are important to obtain good paint adhesion and good fire performance.

• 한국가구학회지
• /
• 제14권2호
• /
• pp.21-29
• /
• 2003

This study was carried out to investigate characteristics of plywood overlaid with softwood veneers densified by resin impregnation and compression. The resin impregnability of Korean pine veneer under atmospheric pressure soaking was greater than that of larch, and impregnability of melamine resin was slightly greater than phenolic resin. It was suggested that resin impregnation ratio was affected by density and thickness of veneer. The largest melamine resin impregnation ratio of 50.7% was obtained with 1.26mm thick Korean pine veneer, and the lowest phenolic resin impregnation ratio of 11.7% with 3.41mm thick larch veneer. Therefore, it was suggested that the vacuum-pres sure-soak treatment is required at thick larch veneer. In densifying resin-impregnated veneers, densification ratio from 13.4 to 31.2% was obtained by high pressure from 15.6 to $20.8kgf/cm^2$. Impregnation of melamine resin also showed relatively greater at densification than that of phenolic resin. So it showed the degree of densification of about 20% or greater. It was seemed that adhesive bonding strength of plywood(base panel) which was directly pressed and overlaid with resin-impregnated veneer was affected by resin tackiness after resin impregnation followed by semi-drying. In laboratory scale, melamine resin impregnation was more favorable for the development of adhesive bonding strength owing to moisture control.

• 한국치위생학회지
• /
• 제21권2호
• /
• pp.99-107
• /
• 2021

Objectives: To compare and evaluate the degree of abrasion of the denture base resin according to the type of denture cleansers. Methods: Denture base resin specimens were prepared and dried. The resin specimens were installed in the automatic brushing machine so that the toothbrush weighed 200 g. The brushing was performed 1,000 times each, a total of 10,000 times using (1) distilled water (DW), (2) non-abrasive cleanser (NAC), and (3) toothpaste (TP), respectively. Thirty specimens were allocated for each group. The thickness of abrasion by brushing was calculated by converting the weight of the specimen. Results: In all DW, NAC, and TP groups, significant differences were found in the average amount of abrasion of the resin specimen due to 1,000 to 10,000 brushings (p<0.001). The average abrasion amount of the resin specimen due to brushing 10,000 times was 2.31±1.20 ㎛ in DW group, 2.52±0.25 ㎛ in NAC group, 6.50±0.60 ㎛ in TP group, and the amount of abrasion in the TP group was statistically significant compared to other groups (p<0.001). Conclusions: The use of TP is not recommended as a method for maintaining the longevity of dentures and for oral health, and NAC was considered to be possible to be used as a denture cleanser because it had a similar amount of abrasion of that of DW.

• 대한치과기공학회지
• /
• 제37권4호
• /
• pp.205-212
• /
• 2015

Purpose: The objective of this study was to compare the surface roughness according to polishing process in conventional laboratory techniques used for polishing three different acrylic denture base resins. Materials and methods: Specimen preparation and surface polishing procedures were conducted to manufacturer's recommendation with three heat-polymerized denture base resins. Surface roughness and gloss were measured by a contact type tester and a LED gloss checker using thickness 2 mm and diameter 10 mm. There were five specimens for each acrylic resin material and polishing procedures. Mean average surface roughness (Ra) values of each specimen group were analyzed using a one-way ANOVA analysis of variance and Scheffe's post hoc test. Surfaces after surface roughness and gloss testing according to each polishing process were evaluated under a stereoscopic microscope. Results: The highest mean average surface roughness was measured($Ra=2.43{\pm}0.47$) for surfaces finished with a denture tungsten carbide bur in Triplex. The lowest surface roughness values ($Ra=0.11{\pm}0.07$) were determined in Vertex polished with a lathe. In addition, all materials revealed that surface roughness determined highly in HP1 and HP2 than other procedures. All correlation between surface roughness and gloss showed highly with three heat-polymerized resins. Specially, topmost correlation revealed than other material in Triplex. Significant differences in mean average surface roughness were found between polishing process used high speed lathe and low speed hand-piece. Conclusion: Laboratory polishing used to high speed was found to produce the smoothest surface of heat-polymerized denture base acrylic resin. Therefore, we recommended that high polishing process need to get smooth surface.

• Restorative Dentistry and Endodontics
• /
• 제17권1호
• /
• pp.36-54
• /
• 1992

The purpose of this study was to compare the shear bond strengths to ground dentin surfaces of four dentinal bonding agents in 193 teeth. Various dentin surfaces treated with four dentin bonding agents were attached with two restorative composite resins. The effectiveness of the bonding were tested by the monitoring the shear bond strength. The shear bond strengths were measured after 2 hours and 24 hours after surface conditioning with four dentin bonding agents. Effects of EDTA, the additive illumination, and sealer treatments without primer on bond strength to dentin surfaces were assessed. In addition the effects of the thickness of specimens ranging from 0.65 mm to 1.95 mm and the ratio of catalyst and base paste on the bond strength of chemical cure composite resin were estimated. The shear bond strength was determined by testing specimens in the Instron universal testing machine (Model No. 1122) at a crosshead speed of 1.0 mm/min. Following condusions were drawn: 1. The highest mean shear bond strengths of chemical cure composite resin to dentin conditioning with dentin bonding agents aged 2 hours were obtained, and then that was decreased with time followed by EDTA treatment. 2. In light cure composite resin, the shear bond strength was increased following dentin conditioning with bonding agents with time, irradiation time and EDTA treatment except in SB group. 3. The thicker the composite resin specimen was, the less the shear bond strength in chemical cure composite resin was. 4. In light cure composite resin, there was a little change in shear bond strength following dentin conditioning with bonding agents. 5. In chemical cure composite resin, the shear bond strength was the highest in the ratio of 1/1 of catalyst and base part. 6. Without a dentin primer, shear bond strength to dentin conditioned only with UB sealer was the highest among four sealers in light cure composite resin.

• 대한소아치과학회지
• /
• 제31권1호
• /
• pp.85-91
• /
• 2004

연구목적은 복합레진 중합 광원에 따른 치수강 온도 변화를 관찰하는 것이었다. 연구에 사용된 광중합기는 일반 플라즈마아크 광중합기, 저발열 플라즈마 아크 광중합기, 저출력 할로겐 광중합기, 저출력 LED 광중합기, 고출력 LED 광중합기의 다섯 개이었다. K-type thermocouple 온도계를 사용하여, 중합기 light guide tip에서의 온도를 측정하고, 잔존 상아질 두께가 1mm가 되도록 형성한 유구치 와동에 상아질 접착제만 도포한 군, ionomer glass를 함유한 base 또는 calcium hydroxide를 함유한 base를 0.5mm두께로 이장한 군에서 각각 레진 충전 전과 후의 치수강내 온도를 측정하였다. 중합기 light guide tip에서 측정한 온도는 일반 플라즈마가 $52.94^{\circ}C$로 가장 높았고, 저출력 LED가 $26.14^{\circ}C$로서 가장 낮았다. 레진충전 전의 치수강내 온도는 고출력 LED가 $41.60{\sim}43.34^{\circ}C$로 가장 높았고, 저출력 LED는 $36.50{\sim}36.76^{\circ}C$로서 가장 낮았다. 레진 충전 후의 치수강내 온도는 고출력 LED가 $40.22{\sim}40.94^{\circ}C$로 가장 높았고, 저발열 플라즈마와 저출력 LED는 온도 상승이 없었다. Base의 사용은 부분적인 열 차단 효과가 있었다.

• 구강회복응용과학지
• /
• 제28권4호
• /
• pp.327-337
• /
• 2012

본 연구에서는 광중합형 석영 섬유인Quarts Splint$^{TM}$ Mesh를 중심으로 다양한 강화재의 의치상 보강 효과에 대해 알아보고자 하였다. 의치상 레진으로 Lucitone199$^{(R)}$와 QC-20을 사용하였으며 강화재로 폴리에틸렌 섬유인 Ribbond$^{(R)}$, Quarts Splint$^{TM}$ Mesh, 금속 격자 강화재를 사용하였다. $2.0{\times}10.0{\times}65.0mm$ 시편을 각각 10개씩 제작하였으며 $2.5{\times}10.0{\times}65.0mm$, $3.0{\times}10.0{\times}65.0mm$ 시편도 제작하였다. Lucitone199$^{(R)}$ 레진은 QC-20 레진보다 높은 굽힘강도를 나타내었으며, 대조군에서 유의차를 나타내었다(p<0.05). Lucitone199$^{(R)}$ 및 QC-20 레진으로 제작한 2.0 mm 두께 시편에서 굽힘강도는 금속 격자 강화재, Quarts Splint$^{TM}$ Mesh, Ribbond$^{(R)}$, 대조군 순으로 감소되었다. Lucitone199$^{(R)}$ 레진을 이용하여 제작한 두께 2.0 mm, 2.5 mm 시편에서 Quarts Splint$^{TM}$ Mesh로 보강한 군은 대조군보다 유의하게 높은 굽힘강도를 나타내었으며(p<0.05), 두께 3.0 mm 시편에서는 유의차가 없었다.

• 대한소아치과학회지
• /
• 제27권3호
• /
• pp.410-418
• /
• 2000

치아수복시 마무리 과정에서의 연마는 수복물의 수명 및 심미성을 결정하는 중요한 과정으로서 연마시 마찰열의 발생으로 인하여 치수에 위해작용을 줄 수 있으므로 주의를 하여야 한다. 여러 가지 수복 재료를 연마하는 동안 치수내에서 발생하는 열의 변화를 수복물 종류, 이장재 종류, 잔존 상아질의 두께, 연마 시간의 차이에 따라 조사하고자 발치된 구치에 수복물을 충전한 후 aluminum-oxide coated disc를 이용하여 연마하는 과정에서 thermocouple을 이용하여 치수내 온도값을 측정하였으며, 이에 대한 통계적 분석을 시행하여 다음과 같은 결과를 얻었다. 모든 경우에서 연마 시간이 증가함에 따라 치수내 온도가 증가하였으며, 아말감 연마시 다른 수복 재료에 비해 큰 온도 증가치를 보였으나 composite resin, glass ionomer cement, 그리고 compomer에서는 연마에 따른 온도 변화차가 관찰되지 않았다. 아말감 하방에 이장재를 사용한 경우에 이장재를 사용하지 않았을 경우에 비해 온도 증가량이 적었으며, 다른 수복재에서는 이장재 사용여부에 따른 온도 증가량의 차이는 존재하지 않았다. 본 실험에서 사용된 이장재 중 glass ionomer cement와 zinc phosphate cement에 비해 zinc oxide eugenol cement의 열 차단 효과가 가장 작았다. 수복물에 간헐적인 연마를 시행한 경우, 지속적인 연마를 시행한 경우에 비해 온도 증가량이 작았으며, 아말감 하방의 잔존 상아질의 두께가 감소하면 온도 증가량이 더 커졌으나, 다른 세 종류의 수복재에서는 잔존 상아질의 두께에 따른 차이가 발생하지 않았다.

• The Journal of Advanced Prosthodontics
• /
• 제7권5호
• /
• pp.368-374
• /
• 2015

PURPOSE. The aim of the study was to evaluate the effect of abutment shade, ceramic thickness, and coping type on the final shade of zirconia all-ceramic restorations. MATERIALS AND METHODS. Three different types of disk-shaped zirconia coping specimens (Lava, Cercon, Zirkonzahn: ${\phi}10mm{\times}0.4mm$) were fabricated and veneered with IPS e.max Press Ceram (shade A2), for total thicknesses of 1 and 1.5 mm. A total of sixty zirconia restoration specimens were divided into six groups based on their coping types and thicknesses. The abutment specimens (${\phi}10mm{\times}7mm$) were prepared with gold alloy, base metal (nickel-chromium) alloy, and four different shades (A1, A2, A3, A4) of composite resins. The average $L^*$, $a^*$, $b^*$ values of the zirconia specimens on the six abutment specimens were measured with a dental colorimeter, and the statistical significance in the effects of three variables was analyzed by using repeated measures analysis of variance (${\alpha}$=.05).The average shade difference (${\Delta}E$) values of the zirconia specimens between the A2 composite resin abutment and other abutments were also evaluated. RESULTS. The effects of zirconia specimen thickness (P<.001), abutment shade (P<.001), and type of zirconia copings (P<.003) on the final shade of the zirconia restorations were significant. The average ${\Delta}E$ value of Lava specimens (1 mm) between the A2 composite resin and gold alloy abutments was higher (close to the acceptability threshold of 5.5 ${\Delta}E$) than th ose between the A2 composite resin and other abutments. CONCLUSION. This in-vitro study demonstrated that abutment shade, ceramic thickness, and coping type affected the resulting shade of zirconia restorations.