• Title/Summary/Keyword: Resin Fraction

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Characteristics of Barley Polyphenol Extract (BPE) Separated from Pearling By-products (보리 도정부산물로부터 분리한 폴리페놀 추출물의 특성)

  • Seog, Ho-Moon;Seo, Mi-Sook;Kim, Sung-Ran;Park, Yong-Kon;Lee, Young-Tack
    • Korean Journal of Food Science and Technology
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    • v.34 no.5
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    • pp.775-779
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    • 2002
  • Barley brans, divided into fractions I $(pearlers\;1{\sim}4)$, II $(pearlers\;5{\sim}20)$, and III $(pearlers \;21{\sim}24)$, germ, and broken kernels were collected as pearling by-products produced by an industrial process consisting of 24 consecutive barley pearlers. The pearling by-products were extracted with 75% ethanol, and polyphenol extracts were separated using Sepabeads SP-850 resin. Total polyphenol content was the highest (43.68%) in the polyphenol extract separated from fraction I. Polyphenol compounds analyzed by HPLC were tentatively identified as proanthocyanins and prodelphinidin polymers, which were known to have antioxidative and antimutagenic activities. Antioxidative abilities were estimated to be in the following order: fraction I>germ>fraction II>fraction III. At 0.01% polyphenol extract, angiotensin I-converting enzyme inhibitory activity was the highest in the germ fraction (40.04%). Nitrite-scavenging activity was over 70% in all fractions. Superoxide dismutase-like activity was in the range of $64{\sim}78%$ in fractions I and II.

The Separation of Ce, Pr, Nd and Sm from Rare Earth Oxides (1차 분리된 희토류산화물 중 Ce, Pr, Nd 및 Sm의 분리)

  • Yong-Kuen Lee;In-Wha Woo;Young-Gu Ha
    • Journal of the Korean Chemical Society
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    • v.24 no.6
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    • pp.434-443
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    • 1980
  • The purpose of this work was to separate Ce, Pr, Nd and Sm from rare-earth oxides by column chromatography. Rare earth solution were adsorbed into the Amberlite IR-120 resin and were eluted by the ammonia alkali solution of the EDTA. As a result of determinating rare earth metals of each fraction, Ce was separated very effectively and Nd and Sm partially separaed but Pr never separated.

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A Study on bending behavior of FRP sandwich beam with 2nd reinforced by double-lap-joint (Double-lap-joint 로 2차 보강 접착을 한 FRP Sandwich Beam의 굽힘 거동 특성에 관한 연구)

  • Son, Choong-Yul;Kim, Ik-Tae;Roh, Min-Shik;Kim, Sung-Jun;Kim, Sang-Ho
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2002.05a
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    • pp.185-190
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    • 2002
  • It has made a special study of bending behavior of F.R.P sandwich beams with bonded 2nd-reinforced plies. Specimens were made of Chopped Mat 300-450, Roving Clothes 570 and the mixture weight ratio of Resin versus hardener was 55:45 for bending tests. it was fabricated by hand lay-up method, hardened for 24 hours in nature, cut specimens according to ASTM standard C393-94 Knowing exact behavior of bonded area's stress and strain depends upon various bonded F.R.P length on which covered lap joint. We also considered shear stress in adhered area and have done computational estimation by ANSYS as well. This study reveals that the length of plies covered lap joint are longer, Failure stresses are remarkably larger.

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Mechanical Properties of Particle and Fiber Reinforced SMC Composites (입자와 섬유로 보강된 SMC 복합재의 기계적 특성에 관한 연구)

  • 정현조;윤성호
    • Transactions of the Korean Society of Automotive Engineers
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    • v.4 no.2
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    • pp.173-182
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    • 1996
  • An analytical model has been developed to predict the elastic properties of a filled resin reinforced by chopped fibers, a three-phase composite such as a filled sheet molding compound(SMC). In the model the matrix material and fillers form an effective matrix. The effective matrix is then considered to be reinforced with long fibers lying in the sheet plane but randomly oriented in the plane. Expressions for the resulting transversely isotropic composite properties are explicitly presented. Using this model, the Young's and shear moduli are calculated for the SMC sample with filler weight fraction of 35% and fiber content of 30%. The same properties are also determined experimentally. The agreement between the calculated and measured elastic moduli is found to be very good for the in-plane properties. However, the out-of-plane properties show a large difference because the effect of voids is not taken into account in the model.

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Experimental analysis of pultrusion process for phenolic foam composites (발포 복합재료 Pultrusion 공정의 실험적 해석)

  • Yun MyungSeok;Lee WooIl
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2004.10a
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    • pp.143-146
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    • 2004
  • Pultrusion process of phenolic foam composite is investigated. Phenolic foam composites provide heat and flame resistance with less weight. When made into foam, a variety of properties can be obtained with different bubble size and number density. In this study, effect of process variables on the foaming characteristics of phenolic resin composites during pultrusion process has been studied experimentally. The process variables considered are the heating temperature and the pulling speed as well as the mass fraction of blowing agent. Experiments were performed using a laboratory scale pultrusion apparatus. Optimal process condition was found by observing the micro-morphology.

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A Feasibility Study of RTM Application on Secondary Fairing Structure of Aircraft (비용절감을 위한 항공기 2차 Fairing구조물의 RTM 적용 가능성 연구)

  • 김태곤;이동준;이건영;신대영
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2002.10a
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    • pp.189-192
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    • 2002
  • The autoclave process is frequently utilized in the manufacturing of aircraft parts because of the low void content and high fiber volume fraction. However, due to the slow curing process (5∼8 hours per part) and it's limited producibility for complicated shape, this process is very expensive and applied to the relatively simple geometry structures. RTM is considered as an alternative process to overcome the limitation of autoclave process. In this study, the idea of RTM application on the secondary Fairing structure of aircraft has been proved to be technically feasible and very cost effective by changing the multiple part of subassembly into one integral composite structure.

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Studies on the Amino Acids Composition of Makjang (막장의 아미노酸 組成에 關한 硏究)

  • Hong Dae Shin;Joo Ok Yoon
    • Journal of the Korean Chemical Society
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    • v.7 no.1
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    • pp.6-12
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    • 1963
  • Amino acid composition of Makjang was determined by combined usage of ion exchanged resin and paper chormatography in the following states. a. A fraction soluble in water b. Hydrolysate of the whole Makjang c. Same as a. (p.p.t. formed by tungstic acid or trichloroacetic acid being removed) d. Hydrolysate of c. (T and TCA) By comparing amino acid composition of Makjang with that of its raw material, we found that decomposition of essential amino acids during brewing is slight. From the amino acid composition of a,b,c,d, we discussed the ratio of amino acid liberation during brewing and assumed that Makjang contains peptide-like substances composing of glutamic acid and aspartic acid.

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A study of FRP bonded Double lap joints of Tensile and bonded joint Characteristic (FRP 본딩한 복합재료의 인장을 받는 Double Lap 조인트의 음력과 접합 조인트의 특성)

  • 손충열;김익태;최재원;이강수
    • Proceedings of the Korea Committee for Ocean Resources and Engineering Conference
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    • 2000.10a
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    • pp.47-52
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    • 2000
  • F.R.P specimens were made by mixture CM(chopped mat) 450-104 matrix & RC(roving clothes)570-100 Roving, the mixture ratio Resin: hardener (92:8) for tensile test. It was also made of plates by hand lay-up method and was been cured for 24 hours and then was cut tensile specimens in accordance with ASTM D638 Type 3. Knowing exact behavior of bonded area's stress and strain when the tensile test was going on, the test specimens were made of 2 plies laminae of F.R.P in each for supporting cut part in middle of specimen length. And in middle part also were covered of F.R.P plies of 1/2, 2/3 length of specimen in each as well. Also we consider shear stress in adhered area. This study reveals that as plys length is more longer, rupture stress grows remarkably larger.

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RESEARCH PAPERS : CHARACTERIZATION OF DISSOLVED ORGANIC MATTER IN A SHALLOW EUTROPHIC LAKE AND INFLOWING WATERS

  • Kim, Yong-Hwan;Lee, Seon-Hwa;Akio, Imai;Kazuo, Matsushige
    • Environmental Engineering Research
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    • v.7 no.2
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    • pp.93-101
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    • 2002
  • The seasonal patterns of dissolved organic matter (DOM) in Lake Kasumigaura, a shallow, eutrophic lake, and serveral DOM sources in its catchment area were investigated. DOM was fractionated using three resin adsorbents into classes: aquatic humic substances (AHS=humic acid+fulvic acid), hydrophobic neutrals (HoN), hydrophilic acids (HiA), bases (BaS) and hydrophilic neutrals (HiN). The DOM produced significantly different fraction distributions depending on the origin of sample. AHS and HiA prevailed over AHS in the lake while AHS and HiA existed at almost the same concentration levels in the rivers. AHS seems to be a more dominant component in rever water than lake water. The dominance of organic acids was also observed in the DOM sources: forest stream (FS), plowed field percolate (PFP), domestic sewage (DS) and sewage treatment plant effluent (STPE).

A Study on the Fracture Toughness of Glass-Carbon Hybrid Composites (유리-탄소 하이브리드 복합재료의 파괴인성에 관한 연구)

  • No, Ho-Seop;Go, Seong-Wi
    • Journal of the Korean Society of Fisheries and Ocean Technology
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    • v.28 no.3
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    • pp.295-305
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    • 1992
  • The critical strain energy release rate and the failure mechanisms of glass-carbon epoxy resin hybrid composites are investigated in the temperature range of the ambient temperature to 8$0^{\circ}C$. The direction of laminates and the volume fraction are [(+45, -45, 0, 0) sub(2) ] sub(s), 50%, respectively. The major failure mechanisms of these composites are studied using the scanning electron microscope for the fracture surface. Results are summarized as follows: 1) The critical strain energy release rate shows a maximum at ambient temperature and it tends to decrease as temperature goes up. 2) The critical strain energy release rate increases as the content of glass increases, and especially shows dramatic increase for the high glass fiber content specimens. 3) Major failure mechanisms can be classfied such as localized shear yielding, fiber-matrix debonding, matrix micro-cracking, and fiber pull-out and/or delamination.

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