• Membrane and Water Treatment
• /
• 제11권4호
• /
• pp.237-245
• /
• 2020

The effects of the mixed two solvents, Dimethylacetamide (DMAc) and Dimethylformamide (DMF), and Polyethylene glycol (PEG) and Polyvinylpyrrolidone (PVP) as additives on performance of Polyvinylidene fluoride (PVDF) membranes were studied. Initially, PEG200 was used as a primary additive at fixed percentage of 5% wt. PVP was then blended with PEG200 in different concentrations. PVDF and DMAc were used as polymer and solvent in the casting solutions, respectively. To control the diffusion rate of PVP in the presence of PEG200 and PVP blend, mixtures of DMAc and DMF were used as the mixed solvent in the casting solutions. Asymmetric PVDF membranes were prepared via phase inversion process in a water bath and the effects of two additives and two solvents on the membrane morphology, pure water flux (PWF), hydrophilicity and rejection (R) were investigated. Attenuated Total Reflection Fourier Transform Infrared Spectra (ATR-FTIR) analysis was used to show the residual PVP on the surface of the membranes. Atomic Force Microscopy (AFM) was utilized to determine roughness of membrane surface. The use of mixed solvents in the casting solution resulted in reduction of PVP diffusion rate and increment of PEG diffusion rate. Eventually, PWF and R values reduced, while porosity and hydrophilicity increased.

• 한국광학회지
• /
• 제15권3호
• /
• pp.214-221
• /
• 2004

색분산 보상에 사용되는 선형 첩 광섬유 격자의 제작에 있어서 Group Delay Ripple(GDR)을 줄이기 위한 apodization 기술에 대해 이론적으로 분석하고 실험적으로 규명하고자 한다. 첩격자의 제작에는 위상 마스크를 이용한 UV 빔 스캐닝 기법을 적용하였고, PZT(Piezoelectric transducer)를 이용하여 위상 마스크를 빔 스캐닝 중에 적절하게 흔들어줌으로써 apodization이 일어나도록 하였다. 이러한 모든 과정이 컴퓨터 제어로 이루어지기 때문에 다양한 apodization 프로파일을 적용할 수 있었다. Gaussian, Raised-cosine, Blackman, 그리고 Hyperbolic tangent 등의 프로파일을 적용하여 첩격자를 제작하였으며 실험 결과 0.05 nm 구간평균 peak-to-peak GDR이 20ps 이하로 감소하였다.

• 대한기계학회:학술대회논문집
• /
• 대한기계학회 2001년도 춘계학술대회논문집A
• /
• pp.26-36
• /
• 2001

Smart sensors and actuators have recently been developed. In this study, first, small-diameter fiber Bragg grating (FBG) sensors developed by the author, whose cladding and polyimide coating diameters were 40 and $52{\mu}m$, respectively, were embedded inside a laminate without resin-rich regions around sensors and the deterioration of mechanical properties of the composite laminate. The small-diameter FBG sensor was embedded in $0^{\circ}$ ply of a CFRP laminate for the detection of transverse cracks in $90^{\circ}$ ply of the laminate. The reflection spectra from the FBG sensor were measured at various tensile stresses. The spectrum became broad and had some peaks with an increase of the transverse crack density. Furthermore, the theoretical calculation reproduced the change in the spectrum very well. These results show that the small-diameter FBG sensors have a potential to detect the occurrence of transverse cracks through the change in the form of the spectrum, and to evaluate the transverse crack density quantitatively by the spectrum width. On the other hand, shape memory alloy (SMA) films were used to suppress the initiation and growth of transverse cracks in CFRP laminates. Pre-strained SMA films were embedded between laminas in CFRP laminates and then heated to introduce the recovery stress in SMA films and compressive stresses in the weakest plies ($90^{\circ}$ ply). The effects of recovery stresses are demonstrated in the experiments and well predicted using the shear-lag analysis and the nonlinear constitutive equation of SMA films.

• 한국정보통신학회:학술대회논문집
• /
• 한국해양정보통신학회 2007년도 추계종합학술대회
• /
• pp.268-270
• /
• 2007

NIR을 이용하여 시간 변화에 따른, 소 등심육의 부위별(살코기와 지방)특성을 조사 하였다. 소 등심육의 특성은 분광분석법을 사용하여 측정하였다. 육질은 총 세 가지 종류의 Sample로 구분 하여 각각의 Sample 마다 3Point 씩 Point를 정하여 측정 하였고, 냉동상태와, 20분경과 후 그리고 해동 40분경과 후를 측정 하였다. 측정결과 Moglobin의 분포에 따라 광도의 변화가 발생하였고, 이를 통해 소 등심육의 살코기와 지방 분포에 따라 고기 육질의 품질 판별 및 특성의 파악이 가능할 것으로 예상된다.

• 한국전기전자재료학회:학술대회논문집
• /
• 한국전기전자재료학회 2001년도 추계학술대회 논문집 Vol.14 No.1
• /
• pp.533-536
• /
• 2001

Single crystal cubic silicon carbide(3C-SiC) thin film were deposited on Si(100) substrate up to a thickness of $4.3{\mu}m$ by APCVD(atmospheric pressure chemical vapor deposition) method using hexamethyildisilane(HMDS) at $1350^{\circ}C$. The HMDS flow rate was 0.5 sccm and the carrier gas flow rate was 2.5 slm. The HMDS flow rate was important to get a mirror-like. The growth rate of the 3C-SiC films was $4.3{\mu}m/hr$. The 3C-SiC epitaxical layers on Si(100) were characterized by XRD(X-ray diffraction), raman scattering and RHEED(reflection high-energy electron diffraction), respectively. The 3C-SiC distinct phonons of TO(transverse optical) near $796cm^{-1}$ and LO(longitudinal optical) near $974{\pm}1cm^{-1}$ were recorded by raman scattering measurement. The deposition films were identified as the single crystal 3C-SiC phase by XRD spectra($2{\theta}=41.5^{\circ}$). Also, with increase of films thickness, RHEED patterns gradually changed from a spot pattern to a streak pattern.

• 한국광학회지
• /
• 제6권4호
• /
• pp.296-301
• /
• 1995

광섬유격자와 단방향성 광섬유 loop mirror를 이용하여 단일모드로 발진하는 erbium첨가 광섬유레이저를 구성하였다. 이득매질인 erbium첨가 광섬유를 단방향성 loop내에 둠으로써 레이저광이 이득매질내에서 진행파를 이루도록 하고 loop 밖에서 반사 선폭이 0.2nm인 광섬유격자로 파장선택적 귀환시켜 주는 방식으로 공진기를 구성하였다. 수동형 광섬유 링공진기 형태의 광스펙트럼 분석기를 별도로 구성하여 광섬유레이저의 모드 스펙트럼을 관찰한 결과, 외부 온도변화로 인한 분 단위의 모드 튐을 제외하고는 대부분의 시간에 안정적인 단일모드 및 단일편광 상태의 특성을 나타냄을 확인할 수 있었다.

• 대한전자공학회논문지SD
• /
• 제37권9호
• /
• pp.23-30
• /
• 2000

본 논문에서는 InGaAs/InAlAs 다중 양자우물을 이용한 두가지 타입의 비대칭 Fabry-Perot 전광 스위치에 대한 해석을 시도하였다. 전광 스위치의 동작을 해석하기 위해서 먼저 양자우물의 광 흡수계수와 굴절율의 변화 특성을 계산하였다. 양자우물의 비선형성 해석 결과를 토대로 전광 수위치의 ON/OFF 비와 스위칭 속도를 비교하였다. 시뮬레이션 결과로부터, DBR을 이용한 구조의 전광 수위치는 DBR이 없는 형태의 전광 수위치보다 ON/OFF 비를 향상시킬 수 있을 뿐만 아니라 스위칭 시간도 단축시킬 수 있음을 알 수 있었다.

• 대한전자공학회:학술대회논문집
• /
• 대한전자공학회 2002년도 ITC-CSCC -3
• /
• pp.1531-1534
• /
• 2002

Shape description and its corresponding matching algorithm is one of the main concerns in MPEG-7. In this paper, a new method is proposed for shape registration of 2D objects for MPEG-7 Shapes are recognized using the Hu statistical moments in frequency domain. The Hu moments are moment-based descriptors of planar shapes, which are invariant under general translation, rotational, scaling, and reflection transformation. The image is transformed into frequency domain using Fourier Transform. Annular and radial wedge distributions fur the power spectra are extracted. Different statistical features (Hu moments) are found f3r the power spectrum of each selected transformed individual feature. The Euclidean distance of the extracted moment descriptors of the features are found with respect to the shapes in the database. The minimum Euclidean distance is the candidate for the matched shape. The simulation results are performed on the test shapes of MPEG-7.

• 한국입자에어로졸학회지
• /
• 제6권1호
• /
• pp.29-35
• /
• 2010

Transition metals such as V, Fe, and Ni were used to synthesize doped zinc oxide nanoparticles from mixed liquid precursors by using the flame spray pyrolysis (FSP). The effects of dopants on the powder properties such as morphology, specific surface area, crystal structure, and light adsorption were analyzed by TEM, BET, XRD, and UV-Vis diffuse reflection spectrum (DRS), respectively. The results showed that hexagonal wurtzite structured ZnO:M (M = V, Fe, Ni) nanoparticles were successfully synthesized by the FSP. The transition metal-doping resulted in the decrease in its particle size and crystallite size. The UV-vis absorption spectra of ZnO:M nanoparticles were also red-shifted. ZnO:V showed the highest MB degradation of 99.4% under the UV irradiation after 3 hrs.

• 약학회지
• /
• 제49권1호
• /
• pp.1-5
• /
• 2005

Near-infrared (NIR) spectroscopy has been widely applied in various field, since it is nondestructive and no sample preparation is required. In this paper, NIR spectroscopy was used for the determination of naproxen in a commercial pharmaceutical preparation. NIR spectroscopy was used to determine the content of naproxen in intact naproxen tablets containing 250 mg ($65.8\%$ nominal concentration) by collecting NIR spectra in the range of $1100{\sim}1750nm$. The laboratory-made samples had $46.1{\sim}85.5\%$ nominal naproxen concentration. The measurements were made by reflection using a fiber-optic probe and calibration was carried out by partial least square regression (PLSR). Model validation was performed by randomly splitting the data set into calibration and validation data set (63 samples as a calibration data set and 42 samples as a validation data set). The developed NIR calibration gave results comparable to the known values of tablets in a laboratorial manufacturing process with standard error of calibration (SEC) and standard error of prediction (SEP) of $1.06\%\;and\;1.04\%$, respectively. The NIR method showed good accuracy and repeatability. NIR spectroscopic determination in intact tablets allowed the potential use of real time monitoring for a running production process.