• Title/Summary/Keyword: Reference Analysis

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Preparation and Certification of Rice Flour Reference Materials for Trace Elements Analysis (미량원소분석을 위한 쌀분말 기준물질의 제조 및 검정)

  • Cho, Kyung-Haeng;Park, Chang-Joon;Woo, Jin-Choon;Suh, Jung-Ki;Han, Myung-Sub;Lee, Jong-Hae
    • Analytical Science and Technology
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    • v.11 no.4
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    • pp.271-280
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    • 1998
  • Rice flour reference materials were prepared from the unpolished rice grown in Korea and certified for elemental composition. The reference materials consist of two samples containing normal and high level. The reference material at elevated level was prepared by spiking to the normal rice flour six toxic elements of As, Cd, Cu, Cr, Hg, Pb with $1.0{\mu}g/g$ on a dry weight basis. Homogeneity of the prepared materials was evaluated through the determination of Ca, Cu, Fe, Mn, Zn by instrumental neutron activation analysis (INAA) and atomic absorption spectrometry (AAS). Small variance of elemental composition among interbottled samples assured homogeneity of the prepared materials. The materials were decomposed by high pressure digestion and microwave digestion method. INAA, AAS, inductively coupled plasma-atomic absorption spectrometry (ICP-AES), ICP-mass spectrometry (MS) and vapour generation techniques were employed to analyze the reference materials. From this independent analytical results, the certified or reference values are determined for As, Ca, Cd, Cr, Cu, Fe, Hg, K, Mg, Mn, Mo, Na, P, Pb, Se, Zn.

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Development of Reference Material Using Natural Seawater for Nutrient Analysis in Seawater (자연해수를 이용한 해수 중 영양염 분석용 표준물질 개발)

  • Rho, Taekeun;Kang, Dong-Jin;Kim, Eun-Soo;Kahng, Sung-Hyun;Cho, Sung Rok;Lee, Jung Moo;Park, Eun Ju;Moon, Cho-Rong
    • The Sea:JOURNAL OF THE KOREAN SOCIETY OF OCEANOGRAPHY
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    • v.20 no.1
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    • pp.29-35
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    • 2015
  • Dissolved nutrients in seawater are recognized as an essential biogeochemical factor for detecting global environmental changes. The importance of nutrient reference material for seawater has been increased greatly for the comparison of nutrient data, measured in different time and space in global ocean by various researchers with different levels in nutrient analysis skill. In this study, we described the homogeneity and stability of nutrient reference material for seawater using natural seawater, collected at a station of Shihwa Lake, at a coastal station near Uljin (surface water), and at a station over the Ulleung Basin (surface water and 1500 m depth water) and sterilized. Based on the homogeneity data, the nutrient reference materials has similar homogeneity compared to other nutrient reference materials. During 3-13 month period, there was no unidirectional trend of increase or decrease in nutrient concentration of newly developed nutrient reference material for seawater. However, a sustained measurement is required to check stability for longer period.

Load Fidelity Improvement of Piecewise Integrated Composite Beam by Irregular Arrangement of Reference Points (참조점의 불규칙적 배치를 통한 PIC보의 하중 충실도 향상에 관한 연구)

  • Ham, Seok Woo;Cho, Jae Ung;Cheon, Seong S.
    • Composites Research
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    • v.32 no.5
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    • pp.216-221
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    • 2019
  • Piecewise integrated composite (PIC) beam has different stacking sequences for several regions with respect to their superior load-resisting capabilities. On the interest of current research is to improve bending characteristics of PIC beam, with assigning specific stacking sequence to a specific region with the help of machine learning techniques. 240 elements of from the FE model were chosen to be reference points. Preliminary FE analysis revealed triaxialities at those regularly distributed reference points to obtain learning data creation of machine learning. Triaxiality values catagorise the type of loading i.e. tension, compression or shear. Machine learning model was formulated by learning data as well as hyperparameters and proper load fidelity was suggested by tuned values of hyperparameters, however, comparatively higher nonlinearity intensive region, such as side face of the beam showed poor load fidelity. Therefore, irregular distribution of reference points, i.e., dense reference points were distributed in the severe changes of loading, on the contrary, coarse distribution for rare changes of loading, was prepared for machine learning model. FE model with irregularly distributed reference points showed better load fidelity compared to the results from the model with regular distribution of reference points.

Discrete Model Reference Adaptive Control Based on Hyperstability Theory (Hyperstability 이론에 기초를 둔 이산기준모델적응제어)

  • 함운철;최계근
    • Journal of the Korean Institute of Telematics and Electronics
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    • v.25 no.5
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    • pp.482-489
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    • 1988
  • In this paper, we proposed a generalized model reference adaptive control theory which can be applied to single-input single-output discrete system by using V.M.Popov's hyperstability theory. As the result of theoretical analysis, it is proved that the discrete adaptive control scheme proposed by Narendra is a special case of the adaptive control schemes proposed in this paper. Also we suggest a variety of parameter adaptiations methods of controller through hyperstability theory.

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An Analysis on International Trade Information Effects of Internet Electronic Commerce (인터넷 전자상거래(EC)의 국제무역정보 효과분석)

  • Lee, Je-Hong
    • International Commerce and Information Review
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    • v.1 no.2
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    • pp.69-95
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    • 1999
  • Internet EC accomplish to simply electronic business from all process integration of production, marketing and customer service. Also customers gain to goods information by one-line product reference, order, product information exchange and negotiate to low cost for high quality goods. Therefore, Purpose of this study is to introduce the building method of efficient EC, helping understand EC, and analysing its present state in the Korean enterprises and efficiency on international trade information.

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J Estimations For Axial Surface Cracked Pipes Under Pressure (축방향 표면균열이 존재하고 내압을 받는 직관의 J 예측 방법)

  • Oh, Chang-Sik;Song, Tae-Kwang;Kim, Yun-Jae
    • Proceedings of the KSME Conference
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    • 2007.05a
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    • pp.1824-1829
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    • 2007
  • In the present paper, limit pressures for axial surface cracked pipe are proposed, and a reference stress based J estimation method is also provided based on the proposed limit pressure solutions. Employed cracks are assumed to be constant-depth, internal surface cracks, and wide ranges of variables are considered.

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Validation of Radioanalytical Techniques for Nuclear Waste Characterisation

  • Warwick, Phillip E.
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.17 no.4
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    • pp.363-373
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    • 2019
  • Waste characterisation associated with nuclear site decommissioning relies on radiochemical analysis of a diverse range of sample types, requiring extensive validation of analytical techniques using matrix-matched materials. The absence of relevant reference materials has hindered robust method development and validation. The paper discusses how method validation in support of nuclear waste characterisation can be achieved without using reference materials. The key stages in an analytical procedure are evaluated and a multi-stage approach is proposed with the ultimate aim of determining an operational envelope for an analytical procedure.

Preliminary Conceptual Design and Cost Analysis of the DUPIC Fuel Fabrication Plant

  • Park, Jongwon;Wonil Ko;Lee, Jaesol;Inha Jung;Park, Hyunsoo
    • Proceedings of the Korean Nuclear Society Conference
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    • 1996.05c
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    • pp.441-446
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    • 1996
  • A preliminary conceptual design of the DUPIC fuel fabrication plant with production capacity of 400 MTHE/yr is presented. Capital and operating costs are also included. The levelized unit fabrication cost (LUC) for a reference mode was estimated at $509/kgHE, and sensitivity of some variable parameters to this reference was analysed.

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Chaos in nonlinear control systems

  • Lee, Joon-Suh;Chang, Kun-Soo
    • 제어로봇시스템학회:학술대회논문집
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    • 1994.10a
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    • pp.758-762
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    • 1994
  • Complicated dynamical behavior can occur in model reference adaptive control systems when two external sinusoidal signals are introduced although the plant and reference model are stable linear first older systems. The phase portrait plot and the power spectral analysis indicate chaotic behavior. In the system treated, a positive Lyapuniov exponent and non-integer dimension clearly manifest chaotic nature of the system.

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CFD ANALYSIS OF SUBSONIC AIRFOIL WIND TUNNEL TEST (아음속 익형 풍동시험 전산해석)

  • Kim, C.W.;Lee, Y.G.
    • 한국전산유체공학회:학술대회논문집
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    • 2007.10a
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    • pp.167-170
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    • 2007
  • In the present paper, wall correction method is reviewed and applied to the numerical experimental results obtained at the wind tunnel condition. The corrected lift coefficient agrees well with the reference data generated from the grid having very far boundary. However the corrected drag coefficient presents some deviation from the reference data.

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