• Title/Summary/Keyword: Recrystallize

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Identification of the Antibiotic-Producing Chstridium sp. KH-431 and Purification of the Antibiotics (항생물질을 생산하는 Clostridium sp. KH-431의 동정 및 항생물질의 정제)

  • 홍수형;김미정;박용복;이재근;하지홍
    • Microbiology and Biotechnology Letters
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    • v.21 no.1
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    • pp.41-46
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    • 1993
  • A strain showing antibiotic activities against various bacteria and fungi was selected from approximately 2,000 microorganisms obtained from soil samples. This strain, designated as KH-431, was identified as a Clostridium sp. by its morphological, physiological and biochemical characteristics. The highest production of the antibiotics was achieved in a fermentation medium containing sorbitol, yeast extract, d-biotin and $CaCl_2$ The antibiotics were isolated from the culture broth by solvent extraction using ethyl acetate, silica gel column chromatography and recrystallization. Two kinds of antibiotics, KG-431A and KG-431B were obtained after the purification procedure, and only KG-431B was successful to recrystallize.

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The Thickness of Recrystallization Layer and Mechanical Properties According to Extrusion Exit Temperature (압출 출구 온도에 따른 Al 6061 합금의 표면 재결정층 두께 변화 및 기계적 특성 변화)

  • Kim, S.B.;Park, T.H.;Kim, H.G.;Lee, S.M.;Kim, H.K.
    • Transactions of Materials Processing
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    • v.30 no.5
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    • pp.219-225
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    • 2021
  • When extruding Al6061 alloys, deformation energy is deposited inside the extruded alloy depending on the deformation and the temperature of extrusion. This creates a Peripheral Coarse Grain (PCG) on the surface, where relatively more deformation energy. of the extruded alloy has been accumulated. Furthermore, since the deformation of materials continues while the materials recrystallize, it is important to examine the effect of deformation energy on dynamic recrystallization in the process of extruding Al alloys along with their microstructure. Prior studies explain the theory behind PCG growth though quantitative analysis on PCG growth of Al alloys during extrusion processes has not yet been addressed. This study aims to measure the generated PCG thickness which determines the correlation between extrusion outlet temperature and its effect on mechanical properties. Surface structure observations were performed using Optical Microscope (OM) and mechanical properties were evaluated through tensile strength and hardness measurement. Throughout this study, we endevoured to find the optimum condition of extrusion exit temperature of Al6061 and confirmed improved d reliability. This study describes the effect of the complex process variables such as exit temperature on the thickness of PCG layer for the Al6061 alloy using the 200 tons extrusion press. We therefore, discovered that the PCG layer thickness was 117 ㎛ at temperatures between 460 ℃ to 520 ℃.