• 대한기계학회논문집A
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• 제27권7호
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• pp.1152-1158
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• 2003

The mechanical behavior of a commercially pure titanium (CP-Ti) is investigated at high temperature Split Hopkinson Pressure Bar (SHPB) compression test with high strain-rate. Tests are performed over a temperature range from room temperature to 1000$^{\circ}C$ with interval of 200$^{\circ}C$ and a strain-rate range of 1900 ∼ 2000/sec. The true flow stress-true strain relations depending on temperature are achieved in these tests. For construction of constitutive equation from the true flow stress-true strain relation, parameters for the Johnson-Cook constitutive equation is determined. And the modified Johnson-Cook equation is used for investigation of behavior of flow stress in vicinity of recrystalization temperature. The Modified Johnson-Cook constitutive equation is more suitable in expressing the dynamic behavior of a CP-Ti at high temperature, i.e. about recrystalization temperature.

• 한국세라믹학회지
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• 제34권11호
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• pp.1159-1164
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• 1997

Magnetite(Fe3O4) powders were synthesized through glycothermal reaction by using crystalline $\alpha$-FeOOH as precursor and ethyleanne glycol as solvent. The phase, morphology and particle size of synthesized powders were characterized by XRD and an SEM. When only ethylene glycol was used as solvent, the phase was transformed from $\alpha$-FeOOH to $\alpha$-Fe2O3 and finally Fe3O4 at 27$0^{\circ}C$ for 6hr without morphological change. But by addition of water, Fe3O4 powders were synthesized at 23$0^{\circ}C$ for 3hr through solution-recrystalization process. As the content of water addition increased, the particle shape changed from sphere to octahedron and the partcle size increased. When the excess amount of water added, residual $\alpha$-FeOOH or $\alpha$-Fe2O3 was recrystalized.

• 한국재료학회:학술대회논문집
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• 한국재료학회 1994년도 추계 학술발표 강연 및 논문 개요집
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• pp.180-180
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• 1994

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2007년도 춘계학술대회 논문집
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• pp.427-430
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• 2007

Gas turbine disk components have been used by Ni-base superalloys which have high temperature strength for enduring stress induced by high speed rotation. This study introduced the overview of development strategy of precision forging of turbine disk and closed-die forging process for manufacturing good quality gas turbine disk. To make superior quality turbine disk, it is important to select optimal forging process conditions like preform shape, die shape and forging temperature etc. In this paper, closed-die forging process has been studied through the rigid-plastic finite element simulation. Proposed forging process can be used for the successful manufacturing of small-size gas turbine disk.

• Journal of Ginseng Research
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• 제22권4호
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• pp.284-288
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• 1998

This study was carried out to establish a new efficient method for isolation and purification of ginsenosides. Silica gel column chromatography, having been used for the isolation of ginsenosides, is advantageous to obtain a large amount of ginsenosides. However, it has a disadvantage to isolate ginsenosides to their highest purity. In addition, normal-or reverse-phase HPLC method thus far reported is confined to quantitative analysis. Especially, it has not been possible to isolate racemic 20(S)- and 20(R)-ginsenoside Rg2. In this experiment, isolation and purification of ginsenosides were accomplished by Diaion HP-20 adsorption chromatography, silica gel column chromatography, recrystalization and Prep. HPLC with or without Prep. TLC. From this study, we could establish a new efficient method for isolation and purification of 9 major and/or minor ginsenosides.

• 한국미생물·생명공학회지
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• 제19권6호
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• pp.604-609
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• 1991

토양에서 분리한 Streptomyces nigrifaciens GMT-497호무터 G(+) bacteria에만 강한 항균활성을 갖는 항생물질 MT-497을 용매추출, silica column chromatography와 재결정화를 통하여 분리 정제하였다. MT-497의 UV, 융점, 원소분석, IR spectrum, $^1H-NMR$과 구성아미노산 분석을 통해 actinocin chromophore와 threonine, proline, methyl valine, sarcosine, aspartic acid로 구성된 peptide을 갖는 actinomvcin계열의 항생물질로 동정하였다.

• 소성∙가공
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• 제14권7호
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• pp.635-641
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• 2005

The crystal structure of magnesium was hexagonal close-packed (HCP), so its formability was poor at room temperature. But formability was improved in high temperature with increasing of the slip planes. Purpose of this paper was to know about the mechanical properties of magnesium alloy (AZ31B), before warm and hot forming process. The mechanical properties were defined by the tension and compression tests in various temperature and strain-rate. As the temperature was increased, yield·ultimate strength, K-value, work hardening exponent (n) and anisotropy factor (R) were decreased. But strain rate sensitivity (m) was increased. As strain-rate increased, yield·ultimate strength, K-value, and work hardening exponent (n) were increased. Also, microstructures of grains fined away at high strain-rate. These results would be used in simulations and manufacturing factor fer warm and hot forming process.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 2004년도 춘계학술대회 논문집
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• pp.80-83
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• 2004

High temperature deformation behavior of AZ31 Mg alloy was investigated in this study on the basis of a processing map $(\varepsilon\approx0.6)$. To construct a processing map, compression tests were carried out at wide range of temperatures and strain rates $(T=250\~500^{\circ}C,\;\varepsilon=10^{-4}\~100/s)$. Two regions of high deformation efficiency $(\eta)$ were identified as: (1) a dynamic recrystalization (DRX) domain at $250^{\circ}C$ and 1/s and (2) a superplasticity domain at $450^{\circ}C$ and $10^{-4}/s$. Possible deformation mechanisms operating at high temperature were discussed in relation to the activation energy. A two-stage deformation method was found to be effective in enhancing the superplasticity of AZ31 Mg alloy. From the two-stage deformation method, tensile elongation of $1200\%$ was obtained at the superplastic domain.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 1995년도 춘계학술대회논문집
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• pp.114-123
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• 1995

Hot workability and microstructural development of 7075Al alloy were studied by hot torsion test. With decling temperature from 440$^{\circ}C$ to 340$^{\circ}C$, and strain rate ranges form 5 ${\times}$10-3/sec to 5 ${\times}$10-1/sec , flow stress and microstructural development were analyzed . The hot resoration mechanism was found to be dynamic recrystalization (DRX) form the analysis of the flow curves and the microstructures. In multistage deformation with decreasing temperature grain refinement was obtained effectively compared to conventional thermomechanical treatment (TMT) process. The strain of the 1st stage deformation at 440$^{\circ}C$ was found to play an important role for the next stage deformation behavior at 380$^{\circ}C$.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 1996년도 추계학술대회 논문집
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• pp.1093-1097
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• 1996

The Substitution development of 7075-T6 Al alloy to 7050-T74 Al alloy in small arms to improve anti-stress corrosion cracking was processed along with mass productivity consideration. To meet 7050 Al alloy material characteristics Indirect extrusion type was adopted and local heating above recrystalization temperature in forging process had to be avoided. The T74 aging treatment was 12$0^{\circ}C$ -6hrs and 175$^{\circ}C$ -12hrs and was appropriate for both machanical and anti-cohesion properties. In accessment of field application test 7050Al alloy made parts of small arms showed equivalent or better performance than 7075 Al alloy.