• Title/Summary/Keyword: Rapid grain growth

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Rapid Grain Growth of $SrBi_2Nb_2O_9$ Thin Films for Improving Programming Characteristics of Ferroelectric Gate Field Effect Transistor (강유전체게이트 전계효과 트랜지스터의 정보저장특성 향상을 위한 $SrBi_2Nb_2O_9$ 박막의 급속 결정성장방법)

  • Lee, Chang-Woo
    • Journal of the Microelectronics and Packaging Society
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    • v.12 no.4 s.37
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    • pp.339-343
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    • 2005
  • Pt-$SrBi_2Nb_2O_9(SBN)-Pt-Y_2O_3-Si$ gate field effect transistors (MFMISFETs) have been fabricated and the SBN thin films are rapid thermal annealed in oxygen plasma. The grain size of the SBN becomes 4 times much larger than that of furnace annealed SBN films even at the same annealing temperature of $700^{\circ}C$, remnant polarization value of Pt-SBN-Pt is improved by 2 times. Using the rapid grain growth of SBN for the MFM-ISFET, memory window and programming characteristics of on/off states are fairly well improved.

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Microstructural changes of Al-Zn-Mg-Cu alloys containing Sc during hot extrusion and post heat treatments (Sc을 첨가한 Al-Zn-Mg-Cu 합금 압출재의 열처리에 따른 미세조직 변화)

  • 이혜경;서동우;이상용;이경환
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.10a
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    • pp.281-284
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    • 2003
  • The microstructural changes of Al-Zn-Mg-Cu alloy containing Sc during hot extrusion and post heat treatment is investigated. Two kinds of Al-Sc alloys with different alloying elements (B1, B2) are hot extruded to make I-shape bars at 380$^{\circ}C$, then the bars are solution treated at 480$^{\circ}C$ for 2hrs followed by artificial aging at 120$^{\circ}C$ for 24hrs. The interior microstructure of as extruded bar consists of elongated grains, however, fine equiaxed grains are mainly observed around surface. The microstructural gradient suggests that different restoration process can proceed during the hot extrusion. For B1 and B2, different grain growth behaviors are found around the surface during the post heat treatment. Rapid grain growth behavior around the surface is discussed related with the crystallographic orientation of the grain.

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Effect of Peak Temperature on the Grain Growth in Simulated HAZ of Cr-Mo-V Steel(T24) (Cr-Mo-V강(T24)의 재현 HAZ의 결정립 성장에 미치는 피크온도의 영향)

  • Lee, Kyong-woon;Lee, Seong-hyeong;Na, Hye-sung;Kang, Chung-Yun
    • Journal of Welding and Joining
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    • v.34 no.6
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    • pp.55-61
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    • 2016
  • Recently developed ferritic heat resistance steel, T24 was used to evaluate microstructure characteristics of simulated heat affected zone. Also, correlation between the prior austenite grain size and amount of $M_{23}C_6$ carbide dissolution was discussed. With the increasing of peak temperature, Grain size steadily increased up to $1050^{\circ}C$ and then rapidly increased at $1150^{\circ}C$. Of the peak temperature $950{\sim}1050^{\circ}C$, amounts of $M_{23}C_6$carbide dissolution are low. But Most of $M_{23}C_6$ carbide that is inhibited grain growth were dissolved above $1050^{\circ}C$ and decreased volume fraction of carbide. This indicates that grain growth may be achieved through dissolution of carbide in the base material. As of welding, due to very rapid heating rate, $M_{23}C_6$ carbide exists above equilibrium solution temperature that is $800^{\circ}C$, even at $1050^{\circ}C$. So, It was confirmed that close correlation between carbide dissolution in the base material and grain growth. Calculated grain size has a linear relationship with peak temperature, on the other hand, measured grain size discontinuously increased between $950{\sim}1050^{\circ}C$ and above $1050^{\circ}C$. Grain size of heat affected zone at $1350^{\circ}C$ peak temperature showed maximum 67um and minimum 4um. Also, The number of side showed 3 to 10.

Effect of Quenching Temperature Change on Hardenability of AISI 51B20 Boron Steel (AISI 51B20 보론첨가강의 경화능에 미치는 오스테나이트화 온도의 영향)

  • Kim, Heon-Joo;Park, Moo-Yong
    • Journal of the Korean Society for Heat Treatment
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    • v.23 no.6
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    • pp.315-322
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    • 2010
  • Effect of hardenability, grain size and microstructural change according to the change of austenitizing temperature was analyzed in Jominy hardenability test of AISI 51B20 steel. Grain growth was small, 7 ${\mu}m$ and 12 ${\mu}m$ austenite grain sizes at austenitizing temperature of $900^{\circ}C$ and $1000^{\circ}C$, respectively, while rapid grain growth was observed up to 30 ${\mu}m$ austenite grain size at austenitizing temperature of $1100^{\circ}C$. As austenitizing temperature increased from $900^{\circ}C$ to $1100^{\circ}C$, hardenability in the region within 15 mm from end-quenched surface decreased due to the grains growth of bainite and martensite mixture, on the other hand the hardenability in the region exceeding 15 mm from end-quenched surface increased. Increased hardenability was attributed to different microstructures; pearlite, fine pearlite and bainite, and bainite and martensite structures at austenitizing temperature of $900^{\circ}C$, $1000^{\circ}C$ and $1100^{\circ}C$, respectively.

Nanostructure Ceramics of Silicon Nitride Produced by Spark Plasma Sintering

  • Hojo, Junichi;Hotta, Mikinori
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.323-324
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    • 2006
  • The nanostructure control of $Si_3N_4$ ceramics can be achieved by using fine starting powder and retardation of grain growth. The spark plasma sintering technique is useful to retard the grain growth by rapid heating. In the present work, the change of microstructure was investigated with emphasis on the particle size of starting powder, the amount of sintering additive and the heating schedule. The rapid heating by spark plasma sintering gave the fine microstructure consisting of equiaxed grains with the same size as starting particles. The spark plasma sintering of $Si_3N_4$ fine powder was effective to control the microstrucutre on nano-meter level.

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Genotypic Variation of Rapid Canopy Closure and Its Relationship with Yield of Rice (벼 조기초관폐쇄성의 품종 변이 및 수량과의 관계)

  • Fu, Jin-Dong;Lee, Byun-Woo
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.53 no.2
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    • pp.137-143
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    • 2008
  • Rapid canopy closure (RCC) is one of the physiological attributes that may enhance genetic yield potential of rice (Oryza sativa L.) in a growing season. Crop growth before canopy closure could be described by an exponential equation of $y\;=\;{\alpha}{\cdot}{\exp}({\beta}{\cdot}t)$ where $\alpha$ is the crop leaf area index (LAI) or shoot dry weight (DW), t is the thermal time, $\beta$ is the LAI or DW at the beginning of the exponential growth and is the relative growth rate of LAI ($m^2m^{-2}^{\circ}C^{-1}$) or DW($gg^{-2}^{\circ}C^{-1}$). Field experiment using 22 cultivars revealed that the exponential growth phase before canopy closure can be divided into two sections; an earlier section during which crop dry weight and LAI of varieties are highly dependent on $\alpha$ and a second section where crop dry weight and LAI are highly dependent on $\beta$. Grain weight had significantly positive correlation with $\alpha$ parameter and dry weight and LAI during early exponential phase. The parameter $\beta$ of the exponential growth curve had positive and significant correlation with the LAI and dry weight during the late exponential growth phase, grain number per unit area, and grain yield. There was genotypic difference for RCC parameters, $\alpha$ and $\beta$, indicating the possibility of genetic improvement for these traits.

The Effect of Foliage Clipping on the Growth and the Agronomic Characteristics, as Affected by its Time, Degree, and Nitrogen Top-Dressing, in Rice plants (절엽의 시기 및 정도, 그리고 절엽 후의 시비가 수도의 생육 및 수량제형질의 변화에 미치는 영향)

  • Eun-Woong Lee;Yong-Woong Kwon;Pyeong-Ki Yim
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.4 no.1
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    • pp.81-91
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    • 1968
  • To investigate the effects of foliage clipping time, degree, and nitrogen top-dressing after clipping on the growth and the agronomic characteristics, rice plants grown under ordinary cultural practices were clipped at the maximum tiller stage, 10 days prior to, and after that stage, respectively, with varying clipping, height, as 0, 1/3, 1/2, and 2/3 of plant height. And nitrogen was top-dressed at the rate of 0, 2, 4, 6 kg per 10 are immediately after clipping. The variety used was "Jinheung". The results obtained are outlined as follows: 1. Effect of clipping on the growth of rice plant: The subsequent growth was quite rapid during 10 days after clipping, and resulted, on the whole, in nearly complete recovery of defoliation by 20 days after clipping. a) Generally, the later the clipping time, the more growth accelerated. Rice plants clipped before the differentiation of ear primordia nearly recovered the damage, and in certain cases exceeded non-clipped plants in height. But the height of the rice plant clipped after the differentiation of ear primordia was somewhat smaller than that of non-clipped. b) Growth rate was rather rapid in the case of severe cutting, and the height of slightly clipped plants was taller than that of non-clipped plants. However, rice plants clipped to the extent of 2/3 of plant height did not fully recover the damage of defoliation compared to non-clipped plants. c) Nitrogen dressing was effective to rapid recovery of defoliation, the effect increasing with the increasing amount of application. d) Ear-heading was delayed in clipped plots, and this tendency was more apparent with later clipping time, more severe clipping, and increased amounts of nitrogen application after cutting. The range was 6 days at maximum. 2. Effect of defoliation on the yield and its components of rice plants: The yield response to clipping varied somewhat with its time, degree, and nitrogen application after cutting: yield increase of about 10% and decreasement of about 25% at maximum compared to the control plot. Grain yield of most plots was decreased. a) Clipping before the differentiation of ear primordia did not much affect the agronomic characteristics of rice plants. However, clipping after that growth stage decreased culm length, number of panicles, number of spikelets per panicle, and maturing rate of grain to some extent. Consequently this treatment resulted in decrease of about 10% in grain and straw production in spite of increase in panicle length and effective tillering rate. b) Slight, clipping decreased number of spikelets per panicle a little, and the yield of grain and straw by 4-5%, although effective tillering rate was somewhat increased. With severe clipping, panicle kngth, number of panicles, and number of spikelets per panicle decreased more, and the yield of grain and straw decreased about 10%. c) Nitrogen dressing after clipping at the rate of 2 kg per 10 are was effective in increasing grain yield. Nitrogen application over the rate of 4 kg per 10 are increased culm length, number of spikelets per panicle, and straw production, but this decreased the maturing rate, and the 1, 000-grains weight to some extent and resulted in decrease of grain yield.

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Application of rapid thermal annealing process to the aluminum induced crystallization of amorphous silicon thin film (비정질 실리콘의 부분적 알루미늄 유도 결정화 공정에서의 급속 열처리 적용 가능성)

  • Hwang, Ji-Hyun;Yang, Su-Won;Kim, Young-Kwan
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.29 no.2
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    • pp.50-53
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    • 2019
  • In this study, polycrystalline silicon thin film useful for the solar cells was fabricated by AIC(Aluminum Induced Crystallization) process. A diffusing barrier for this process is prepared with $Al_2O_3$. For the maximization of the grain size of the polycrystalline silicon, a selective blasting of the $Al_2O_3$ diffusing barrier was conducted before annealing treatment. The heat treatment for the activation of the amorphous-Si (a-Si) layer was carried out with Rapid Thermal Annealing (RTA) process. Crystallization of the a-Si layer was analyzed with XRD. It was confirmed that a-Si was crystallized at $500^{\circ}C$ and the silicon crystal is observed to be formed and the grain size of the polycrystalline silicon was observed to be $15.9{\mu}m$.

Characterization of rapidly consolidated γ-TiAl

  • Kothari, Kunal;Radhakrishnan, Ramachandran;Sudarshan, Tirumalai S.;Wereley, Norman M.
    • Advances in materials Research
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    • v.1 no.1
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    • pp.51-74
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    • 2012
  • A powder metallurgy-based rapid consolidation technique, Plasma Pressure Compaction ($P^2C^{(R)}$), was utilized to produce near-net shape parts of gamma titanium aluminides (${\gamma}$-TiAl). Micron-sized ${\gamma}$-TiAl powders, composed of Ti-50%Al and Ti-48%Al-2%Cr-2%Nb (at%), were rapidly consolidated to form near-net shape ${\gamma}$-TiAl parts in the form of 1.0" (25.4 mm) diameter discs, as well as $3"{\times}2.25"$ ($76.2mm{\times}57.2mm$) tiles, having a thickness of 0.25" (6.35 mm). The ${\gamma}$-TiAl parts were consolidated to near theoretical density. The microstructural morphology of the consolidated parts was found to vary with consolidation conditions. Mechanical properties exhibited a strong dependence on microstructural morphology and grain size. Because of the rapid consolidation process used here, grain growth during consolidation was minimal, which in turn led to enhanced mechanical properties. Consolidated ${\gamma}$-TiAl samples corresponding to Ti-48%Al-2%Cr-2%Nb composition with a duplex microstructure (with an average grain size of $5{\mu}m$) exhibited superior mechanical properties. Flexural strength, ductility, elastic modulus and fracture toughness for these samples were as high as 1238 MPa, 2.3%, 154.58 GPa and 17.95 MPa $m^{1/2}$, respectively. The high temperature mechanical properties of the consolidated ${\gamma}$-TiAl samples were characterized in air and vacuum and were found to retain flexural strength and elastic modulus for temperatures up to $700^{\circ}C$. At high temperatures, the flexural strength of ${\gamma}$-TiAl samples with Ti-50%Al composition deteriorated in air by 10% as compared to that in vacuum. ${\gamma}$-TiAl samples with Ti-48%Al-2%Nb-2%Cr composition exhibited better if not equal flexural strength in air than in vacuum at high temperatures.

A Manufacturing Process analysis of Large Exhaust Valve Spindle considering Microstructure Evolution (미세조직 변화를 고려한 대형 배기밸브 스핀들 제조공정 해석)

  • Jeong Ho-Seung;Cho Jong-Rae;Park Hee-Cheon
    • Journal of Advanced Marine Engineering and Technology
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    • v.29 no.8
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    • pp.938-945
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    • 2005
  • The microstructure evolution in hot forging process is composed of dynamic recrystallization during deformation as well as grain growth during dwell time. Therefore, the control of forging parameters such as strain, strain rate. temperature and holding time is important because the microstructure change in hot working affects the mechanical properties. Modeling equations are developed to represent the flow curve. grain size. recrystallized volume fraction and grain growth phenomena by various tests. The developed modeling equations were combined with thermo-viscoplastic finite element modeling to predict the microstructure change evolution during hot forging process. The large exhaust valve spindle (head diameter of 512mm) was simulated by closed die forging with hydraulic press and cooled in air after forging. The preform was heated to each 1080 and 1150$^{\circ}C$. Numerical calculation was performed by DEFORM-2D. a commercial finite element code. Heat transfer can be coupled with the deformation analysis in a non-isothermal deformation analysis. In order to obtain the fine and homogeneous microstructure and good mechanical properties in forging. the FEM would become a useful tool in the simulation of the microstructure development. In forging, appropriate temperature, strain and strain rate and rapid cooling are required to obtain the fine grain microstructure The optimal forging temperature and effective strain range of Nimonic 80A for large exhaust valve spindle are about 1080$\∼$l120$^{\circ}C$ and 150$\∼$200$\%$.