• Title/Summary/Keyword: Rapid densification

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Estimating Method of Surface Roughness Using Geographic Information (지리정보를 이용한 지표면조도 산정 방법)

  • CHOI, Se-Hyu;SEO, Eun-Su
    • Journal of the Korean Association of Geographic Information Studies
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    • v.18 no.3
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    • pp.1-10
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    • 2015
  • Rapid urban expansion and densification of the various industrial facilities affect the changes of topography and building in urban areas. Even if buildings proceed with high rise, they get mixed with low-rise buildings such as houses and industrial parks that have existed in the area. This may confuse the designer in estimating a surface roughness, an important factor in calculating the design wind velocity of building. This study analyzed the surface roughness by using a geographic information. Referring to the criteria of each country's building code, this study proposed a method to distinguish the surface roughness depending on the height of the surrounding buildings where the design building is located and calculated the surface roughness using 1:5000 topographic map and GIS. It is expected to solve problems that an existing designer calculates the surface roughness in a subjective manner and to help to design more rational buildings resistant to wind.

Preparation and Sintering Characteristics of Gd-Doped CeO2 Powder by Oxalate Co-Precipitation (옥살산 공침법에 의한 Gd-Doped CeO2 분말의 합성 및 소결 특성)

  • Han, In-Dong;Lim, Kwang-Young;Sim, Soo-Man
    • Journal of the Korean Ceramic Society
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    • v.43 no.10 s.293
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    • pp.666-672
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    • 2006
  • GDC20($Ce_{0.8}Gd_{0.2}O_{1.9}$) powder was synthesized by oxalate co-precipitation and milling and its thermal decomposition, phase formation, and sinterability were investigated. As-prepared precipitates were non-crystalline due to the milling process and completely decomposed at 400$^{\circ}C$ The powder calcined at 800$^{\circ}C$ for 2 h contained fine p]sty particles with an average size of 0.69 $\mu$m. Attrition milling of the calcined powder for 2 h had a little milling effect, resulting in a slight decrease in the particle size to 0.45 $\mu$m. The milled powder consisted of small spherical primary particles and some large particles, which had been agglomerated during calcination. Due to the excellent sinterability of the powder, sintering of the powder compacts for 4 h showed relative densities of 78.7% at 1000$^{\circ}C$ and 97.8% at 1300$^{\circ}C$, respectively. Densification was found to almost complete at temperature above 1200$^{\circ}C$ and a dense and homogeneous microstructure was obtained. A rapid grain growth occurred between 1200$^{\circ}C$ and 1300$^{\circ}C$. Grains in 0.1$\sim$0.5 $\mu$m sizes at 1200$^{\circ}C$ grew to 0.2$\sim$2 $\mu$m and their size distribution became broader at 1300$^{\circ}C$.

Phase Evolution, Microstructure and Microwave Dielectric Properties of Zn1.9-2xLixAlxSi1.05O4 Ceramics

  • Kim, Yun-Han;Kim, Shin;Jeong, Seong-Min;Kim, So-Jung;Yoon, Sang-Ok
    • Journal of the Korean Ceramic Society
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    • v.52 no.3
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    • pp.215-220
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    • 2015
  • Phase evolution, microstructure, and microwave dielectric properties of $Li_2O$ and $Al_2O_3$ doped $Zn_{1.9}Si_{1.05}O_4$, i.e., $Zn_{1.9-2x}Li_xAl_x-Si_{1.05}O_4$, ceramics (x = 0.02 ~ 0.10) were investigated. The ceramics were densified by $SiO_2$-rich liquid phase composed of the Li-Al-Si-O system, indicating that doped Li and Al contributed to the formation of the liquid. As the secondary phase, ${\beta}$-spodumene solid solution with the composition of $LiAlSi_3O_8$ was precipitated from the liquid during the cooling process. The dense ceramics were obtained for the specimens of $$x{\geq_-}0.06$$ showing the rapid densification above $1000^{\circ}C$, implying that a certain amount of liquid is necessary to densify. The specimen of x = 0.06 sintered at $1050^{\circ}C$ exhibited good microwave dielectric properties; the dielectric constant and the quality factor ($Q{\times}f_0$) were 6.4 and 11,213 GHz, respectively.

A Study on the Liquid Phase Sintering of Tungsten-Nickel-Manganese alloy (텅스텐-니켈-망간 합금의 액상소결에 관한연구)

  • Hong, Mun-Hui;Lee, Seong;Roh, Jun-Ung;Paik, Un-Hyeong
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 1995.11a
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    • pp.25-25
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    • 1995
  • Liquid phase sintering of 90W-6Ni-4Mn alloy has been investigated as functions of sintering atmosphere, heating rate, and reduction temperature. The present work accounts for the thermodynamic oxidatiodreduction reactions of constituent powders of W, Ni and Mn. By discounting these reactions, the previous investigations would obtain only the alloy with large pores and the lowered relative sintered density, by the liquid phase sintering under a dry hydrogen atmosphere. the sintering cycle consisted of a rapid heating to reduction temperatures under high purity nitrogen atmosphere, and holding for 4 hours and sintering at $1260^{\circ}C$ for 1 hour under a dry hydrogen gas. The relative density of the sintered alloy increased with increasing heating rate. As the reduction temperature increased, the relative density increased to the lm theotical density at the duction temture above $1150^{\circ}C$. The mimsturcatre of sintered alloys has been analysed by a scanning election microscope. The sintered density was compared with those obtained from the other investigators. It was found that the reduction $1150^{\circ}C$ results in the lowered densification of 90W-6Ni-4Mn alloy. This is caused by the fact that reducing reactions of W and Ni oxides contained in W an Ni powders concomitantly leads to oxidizing reaction of Mn powder the oxidized Mn is hardly reduced at sintering temperature and thereby remains large pores in the alloy. It is concluded that the W-Ni-Mn alloy with full density can be obtained by the precise control of atmosphere, heating rate, and sintering temperature.

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Fabrication of Nanostructured Ti from Ti and TiH2 by Rapid Sintering and Its Mechanical Properties (급속소결에 의한 Ti와 TiH2로부터 나노구조의 Ti 제조 및 기계적 특성)

  • Kim, Na-Ri;Cho, Sung-Wook;Kim, Won-Baek;Shon, In-Jin
    • Korean Journal of Metals and Materials
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    • v.50 no.1
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    • pp.34-38
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    • 2012
  • Titanium has good deformability, high hardness, high biocompatibility, excellent corrosion resistance and low density. Due to these attractive properties, it has been used in many industrial applications. Dense nanostructured Ti was sintered from mechanically activated Ti and $TiH_2$ powders by high frequency induction heating under pressure of 80 MPa. The advantage of this process is that it allows very quick densification to near theoretical density and inhibition of grain growth. $TiH_2$ powder was decomposed to Ti during sintering. The hardness of Ti increased and the average grain size of Ti decreased with increasing milling time. The average grain sizes of Ti samples sintered from Ti and $TiH_2$ powder milled for 5 hrs were about 26 nm, 44 nm, respectively. The hardness of Ti sintered from Ti and $TiH_2$ powder milled for 5 h was $504kg/mm^2$ and $567kg/mm^2$, respectively.

Mechanical Properties and Fabrication of Nanostructured Mg2SiO4-MgAl2O4 Composites by High-Frequency Induction Heated Combustion (기계적 활성화된 분말로부터 고주파유도 가열 연소합성에 의한 나노구조 Mg2SiO4-MgAl2O4 복합재료 제조 및 기계적 특성)

  • Shon, In-Jin;Kang, Hyun-Su;Hong, Kyung-Tae;Doh, Jung-Mann;Yoon, Jin-Kook
    • Korean Journal of Metals and Materials
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    • v.49 no.8
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    • pp.614-618
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    • 2011
  • Nanopowders of MgO, $Al_2O_3$ and $SiO_2$ were made by high energy ball milling. The rapid sintering of nanostructured $MgAl_2O_4-Mg_2SiO_4$ composites was investigated by a high-frequency induction heating sintering process. The advantage of this process is that it allows very quick densification to near theoretical density and inhibition of grain growth. Nanocrystalline materials have received much attention as advanced engineering materials with improved physical and mechanical properties. As nanomaterials possess high strength, high hardness, excellent ductility and toughness, undoubtedly, more attention has been paid for the application of nanomaterials. Highly dense nanostructured $MgAl_2O_4-Mg_2SiO_4$ composites were produced with simultaneous application of 80MPa pressure and induced output current of total power capacity (15 kW) within 2min. The sintering behavior, gain size and mechanical properties of $MgAl_2O_4-Mg_2SiO_4$ composites were investigated.

Experimental Study on Accelerated Carbonation Characteristics of OPC Paste for CSC-Based Low Carbon Precast Concrete Products (CSC 기반 저탄소 콘크리트 2차제품 제조를 위한 OPC 페이스트의 촉진탄산화 특성에 관한 실험적 연구)

  • Yoon, Jun-Tae;Kim, Young-Jin;Sim, Sang-Rak;Ryu, Dong-Woo
    • Journal of the Korea Institute of Building Construction
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    • v.24 no.3
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    • pp.285-295
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    • 2024
  • This study investigated the impact of accelerated carbonation on Ordinary Portland Cement(OPC) paste that had undergone steam curing at 500℃·hr. Two carbonation environments were examined: atmospheric carbonation(1atm, 20% CO2) and pressurized carbonation(5atm, 99% CO2). Chemical analysis using X-ray diffraction(XRD) and Fourier-Transform Infrared spectroscopy(FT-IR) were conducted, along with physical characterization via scanning electron microscopy(SEM) and compressive strength testing. Results indicated that atmospheric carbonation with 20% CO2 concentration significantly densified the internal microstructure of the OPC paste, leading to enhanced compressive strength. Conversely, pressurized carbonation at 5atm with 99% CO2 concentration resulted in rapid densification of the surface structure, which hindered CO2 diffusion into the sample. This limited the extent of carbonation and prevented the improvement of physical properties.

Lightweight Aggregate Bloating Mechanism of Clay/Incinerated Ash/Additive System (점토/소각재/첨가제계 인공 경량골재의 발포기구)

  • Kwon, Yong-Joon;Kim, Yoo-Taek;Lee, Ki-Gang;Kim, Young-Jin;Kang, Seung-Gu;Kim, Jung-Hwan;Park, Myoung-Sik
    • Journal of the Korean Ceramic Society
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    • v.38 no.9
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    • pp.811-816
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    • 2001
  • The influence of the incinerated ash and additives on glass phase formation of lightweight aggregate, weight-lightening, and the bloating mechanism was investigated. Clay was used as base materials and incinerated ash was added from 0 to 30wt%. The additives such as $Na_2CO_3,\;CaCo_3,\;K_2CO_3,\;MgCO_3$, and a little amount of waste oil were added to the mixed body. In clay/incinerated ash/additive system, it turned out that $CaCO_3\;and\;MgCO_3$ were the components for glass phase formation and $Na_2CO_3$ was the component for both glass phase formation and weight-lightening. The small addition of waste oil from 0.5wt% to 3.0wt% affect on the bloating of aggregate. Incinerated ash had a good effect on the glass phase controlling. The most effective condition controlling glass phase and bloating of aggregate was 10wt% incinerated ash, 2wt% waste oil at 1200$^{\circ}$C. The bloating mechanism of lightweight aggregate is as follows; 1) micro-crack formation caused by thermal-shock and gas generation from inside of aggregate, 2) volume expansion by glass phase formation on the aggregate surface and rapid gas bloating inside of aggregate, 3) densification after bloating.

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The Effects of Electrode Distance on the Formation of $(ZnS)_{1-x}(SiO_2)_x$ Protective Films in Phase Change Optical Disk by R.F. Sputtering Method (R.F. Sputtering 방법에 의한 상변화형 광디스크의 $(ZnS)_{1-x}(SiO_2)_x$ 보호막 형성에 미치는 전극거리의 영향)

  • Lee, Jun-Ho;Kim, Do-Hun
    • Korean Journal of Materials Research
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    • v.9 no.12
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    • pp.1245-1251
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    • 1999
  • Phase-change optical disk very rapid recording, high densification of data, resulting in high feedback rate and good C/N(carrier to noise) ratio of a feedback signal. However, repetitive thermal energy may cause the deformation of a disk or the lowering of an eliminability and a cyclability of the recording. The lowering of the cyclability can be reduced by insertion of thin layer of ZnS-$SiO_2$ dielectric thin film in appropriate disk structure between the upper and lower part of the recording film. Using the Taguchi method, optimum conditions satisfying both the optimized quality characteristic values and the scattering values for film formation were found to be the target R.F. power of 200W, the substrate R.F. power of 20W, the Ar pressure of 6mTorr, and the electrode distance of 6cm. From the refractive index data, the existence of the strong interaction between the electrode distance and Ar pressure was confirmed, and so was the large effect of the electrode distance on transmittance. According to the analysis of TEM and XRD, the closer the electrode distance was, the finer was the grain size due to the high deposition rate. However, the closer electrode distance brought the negative effect on the morphology of the film and caused the reduction of transmittance. AFM and SEM analyses showed that the closer the electrode distance was, the worse was the morphology due to the high rate of the deposition. Under optimum condition, the deposited thin film showed a good morphology and dense microstructure with less defects.

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