• Korean Journal of Food Science and Technology
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• v.53 no.4
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• pp.391-398
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• 2021

As global interest in herbal medicines has increased, the adulteration of herbal medicines has become a critical safety issue. Adulteration with dyes to improve the appearance of low-quality products is of particular concern. This study aimed to develop a high-performance liquid chromatography (HPLC) method to detect dyes added as adulterants to Phellodendron. Samples were analyzed on a C18 column using 50 mM ammonium acetate and acetonitrile as the mobile phase. All calibration curves showed good linearity (r² ≥0.9999) over the five-point concentration range (1-50 mg/kg). Limit of detection ranged from 0.04-0.35 mg/kg, and limit of quantification ranged from 0.11-1.07 mg/kg. The repeatability and reproducibility for these measurements were 94.2-103.3% and 96.6-103.8% for accuracy and 0.14-2.28 RSD (%) and 0.80-2.37 RSD (%) for precision. Moreover, the measurement uncertainty of the low, medium, and high concentrations for 10 dyes was considered. Thus, this HPLC method is suitable for detecting color adulteration of Phellodendron.

• Food Science of Animal Resources
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• v.43 no.6
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• pp.949-960
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• 2023

This research aimed to validate a high-performance liquid chromatography method for the quantitative determination of bixin and norbixin in various foods. The Diode Array Detector (495 nm) technique was used. Method was validated for specificity, linearity, limit of detection (LOD), limit of quantification (LOQ), precision, and accuracy, and the measurement uncertainty was assessed. The calibration curve showed excellent linearity (r²≥0.9999) over the tested concentration range of 0.2-25 mg/L. The LOD and LOQ were 0.03-0.11 and 0.02-0.05 mg/L for bixin and norbixin, respectively. The intra-and inter-day accuracies and precisions were 88.0±1.3-97.0±0.5% and 0.2%-2.6% relative SD (RSD) for bixin and 88.2±0.8-105.8±0.8% and 0.3%-2.7% RSD for norbixin, respectively. Inter-laboratory validation for accuracy and precision was conducted in three laboratories, and these results all met the AOAC guidelines. In addition, the relative expanded uncertainty (<22%) satisfied the CODEX recommendation. Furthermore, products distributed in Korea were monitored for annatto extracts using the proposed method to demonstrate its application. The developed analytical method is reliable for quantifying bixin and norbixin in various foods.

• Nuclear Engineering and Technology
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• v.56 no.8
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• pp.3276-3285
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• 2024

This paper introduces the creation of a module for Uncertainty Quantification (UQ) specifically designed for VVER analysis through the implementation of the STREAM/RAST-V two-step approach. The aim was to expand the range of use by developing a UQ module tailored for analyzing VVER. This research presents two innovative computational functionalities: (1) development of a library for the pin-based pointwise energy slowing down method (PSM), and (2) extension of the analysis area to study hexagonal-geometry fuel assemblies. The proposed UQ scheme was evaluated through verification using UAM benchmark, and comparative analysis between codes using SCALE 6.2.2 for. STREAM provides an accuracy comparable to that of SCALE 6.2.2. Additionally, a PSM covariance library was utilized in the calculations, achieving 0.7941% and 0.7907% accuracies in the hot full power and hot zero power calculations, respectively. To assess the UQ sequences in the two-step method, the STREAM/RAST-V calculation scheme was verified using the STREAM lattice code. To conclude, this study furnishes comprehensive insights into the development of the UQ module within the two-step method for VVER analysis, and it validates its performance through utilization of the UAM benchmark.

• Proceedings of the Computational Structural Engineering Institute Conference
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• 2004.04a
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• pp.267-274
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• 2004

Since there is a large variation in measurements of the thickness of corroded elements, the thickness of corroded elements are considered as imprecise elements. There is also a considerable degree of uncertainty in a visual assessment of thickness loss. The remaining thickness of a severly corroded element may be represented by an imprecise which expresses the range over which there is uncertainty about the thickness. Therefore, the objective of this paper is to propose a new methodology to safety assessment using imprecise reliability into conventional safety assessment frameworks. For this purpose, this study presents a safety assessment model using Imprecise reliability for large civil structures and demonstrates the applicability of the approach to cable-stayed bridge projects.

• Proceedings of the KSME Conference
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• 2001.06e
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• pp.714-719
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• 2001

The Holographic Particle Velocimetry system can be a promising optical tool for the measurements of three dimensional particle velocities. In this research, the optical system for double pulse holographic recording and reconstruction of particle images was developed. Validation experiments for the developed system were conducted measuring the velocities of glass beads on a rotating disk. Uncertainty analysis was performed to identify the sources of all relevant errors and to evaluate their magnitude. The measurement results of distance between glass beads, size, and velocities of them using holographic method compared reasonalbly well with the known values within acceptable range of errors.

• Proceedings of the KIEE Conference
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• 1997.07f
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• pp.1982-1984
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• 1997

In this paper, adaptive variable structure control is proposed for Electromagnetic Suspension(EMS). Although variable structure control shows excellent robustness to unstructured modelling uncertainty, such as flux leakage and saturation, it has several drawbacks that severely limit practical applicability such as high control activity and control chattering. To minimize these effects, the mass of the electromagnet and efficiency of levitation force are estimated on-line to reduce the range of system uncertainty. The effectiveness of the proposed control scheme is verified by experimental results using a 1.5kg electromagnet and DSP (TMS320C31).

• The KSFM Journal of Fluid Machinery
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• v.6 no.1 s.18
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• pp.57-65
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• 2003

The measurement uncertainties of an ultrasonic flowmeter were analyzed to evaluate its applicability to the measurement of the steam generator feedwater flow-rate in a nuclear power plant. The analyses of measurement uncertainties of a reactor power were also performed with the analyses of feedwater flow measurement uncertainties. Two ultrasonic flowmeters based on a cross-correlation technique and a transit time method were used in this study. The ultrasonic flowmeters were installed on a feedwater pipe line of a typical 1000 MWe Korea-standardized nuclear power plant to take the necessary data. The results have shown that the measurement uncertainties of the ultrasonic flowmeters are adequately smaller than those or a venturi meter. The research has also indicated that the measurement uncertainties of the reactor power based on the ultrasonic flowmeter uncertainties are sufficiently bounded by the uncertainty range usually assumed in nuclear safety analyses.

• Journal of the Korean Society for Precision Engineering
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• v.17 no.10
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• pp.95-101
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• 2000

The purpose of this study is to develop an improved measuring system, which allows for effectively measure spring clamping forces. This system consists of eight or twelve measuring points in order to acquire the clamping force distribution of the whole range of spring clamp. Each measuring point consists of load cells equipped with 4 strain gauges. Using different bearings, we calibrate the roundness of the measuring points. For quality control and database construction, a software system is established. furthermore, uncertainty is calculated to validate the confidence of this system. Various experiments confirm the effectiveness of this measuring system.

• The Transactions of the Korean Institute of Electrical Engineers B
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• v.54 no.5
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• pp.217-221
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• 2005

A inductive voltage divider(IVD) is widely used as a ratio arm of precise impedance measurement bridges at low frequencies of audio frequency range and a well fabricated IVD has ratio error of $10^{-7}$ order without any calibration. Recently, the order of $10^{-8}$ of the best measurement uncertainty is needed for calibration and maintenance of impedance standards as national standards. In order to achieve that uncertainty, the IVD which is used for a ratio arm of precise impedance measurement bridge should be calibrated within the uncertain of order of $10^{-8}$ For this purpose, a ratio calibration bridge for IVDs has been developed. The measurement uncertainties of both inphase and quadrature of the bridge are analyzed less then $3{\times}10^{-8}$ respectively at 1 kHz and 25 V.

• Transactions of the Korean Society of Mechanical Engineers B
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• v.26 no.4
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• pp.539-546
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• 2002

The Holographic Particle Velocimetry system can be a promising optical tool leer the measurements of three dimensional particle velocities. In this research, validation experiments for the development of holographic particle velocimetry system for spray droplets were conducted with measuring the velocities of glass beads on a rotating disk. Uncertainty analysis was performed to identify the sources of all relevant errors and to evaluate their magnitude. The measurement results of distance between glass beads, size, and velocities obtained with holographic method are compared reasonably well with the known values within acceptable range of errors.