• Title/Summary/Keyword: R&D Test Process

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Optimization of Electro-UV-Ultrasonic Complex Process for E. coli Disinfection using Box-Behnken Experiment (Box-Behnken법을 이용한 E. coli 소독에서 전기-UV-초음파 복합 공정의 최적화)

  • Kim, Dong-Seog;Park, Young-Seek
    • Journal of Korean Society of Environmental Engineers
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    • v.33 no.3
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    • pp.149-156
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    • 2011
  • This experimental design and response surface methodology (RSM) have been applied to the investigation of the electro-UV-ultrasonic complex process for the disinfection of E. coli in the water. The disinfection reactions of electro-UV-ultrasonic process were mathematically described as a function of parameters power of electrolysis ($X_1$), UV ($X_2$), and ultrasonic process ($X_3$) being modeled by use of the Box-Behnken technique, which was used for fitting 2nd order response surface model. The application of RSM yielded the following regression equation, which is empirical relationship between the residual E. coli number (Ln CFU) in water and test variables in coded unit: residual E. coli number (Ln CFU) = 23.69 - 3.75 Electrolysis - 0.67 UV - 0.26 Ultrasonic - 0.16 Electrolysis UV + 0.05 Electrolysis Ultrasonic + 0.27 $Electrolysis^2$ + 0.14 $UV^2$ - 0.01 $Ultrasonic^2$). The model predictions agreed well with the experimentally observed result ($R^2$ = 0.983). Graphical 2D contour and 3D response surface plots were used to locate the optimum range. The estimated ridge of maximum response and optimal conditions for residual E. coli number (Ln CFU) using 'numerical optimization' of Design-Expert software were 1.47 Ln CFU/L and 6.94 W of electrolysis, 6.72 W of UV and 14.23 W of ultrasonic process. This study clearly showed that response surface methodology was one of the suitable methods to optimize the operating conditions and minimize the residual E. coli number of the complex disinfection.

Application of Response Surface Method as an Experimental Design to Optimize Coagulation Tests

  • Trinh, Thuy Khanh;Kang, Lim-Seok
    • Environmental Engineering Research
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    • v.15 no.2
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    • pp.63-70
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    • 2010
  • In this study, the response surface method and experimental design were applied as an alternative to conventional methods for the optimization of coagulation tests. A central composite design, with 4 axial points, 4 factorial points and 5 replicates at the center point were used to build a model for predicting and optimizing the coagulation process. Mathematical model equations were derived by computer simulation programming with a least squares method using the Minitab 15 software. In these equations, the removal efficiencies of turbidity and total organic carbon (TOC) were expressed as second-order functions of two factors, such as alum dose and coagulation pH. Statistical checks (ANOVA table, $R^2$ and $R^2_{adj}$ value, model lack of fit test, and p value) indicated that the model was adequate for representing the experimental data. The p values showed that the quadratic effects of alum dose and coagulation pH were highly significant. In other words, these two factors had an important impact on the turbidity and TOC of treated water. To gain a better understanding of the two variables for optimal coagulation performance, the model was presented as both 3-D response surface and 2-D contour graphs. As a compromise for the simultaneously removal of maximum amounts of 92.5% turbidity and 39.5% TOC, the optimum conditions were found with 44 mg/L alum at pH 7.6. The predicted response from the model showed close agreement with the experimental data ($R^2$ values of 90.63% and 91.43% for turbidity removal and TOC removal, respectively), which demonstrates the effectiveness of this approach in achieving good predictions, while minimizing the number of experiments required.

Effect of Induction Heat Bending Process on the Properties of ASME SA106 Gr. C Carbon Steel Pipes

  • Kim, Ki Tae;Kim, Young Sik;Chang, Hyun Young;Oh, Young Jin;Sung, Gi Ho
    • Corrosion Science and Technology
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    • v.14 no.2
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    • pp.47-53
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    • 2015
  • Recently, the bending process is greatly applied to fabricate the pipe line. Bending process can reduce welding joints and then decrease the number of inspection. Thus, the maintenance cost will be reduced. Induction heat bending process is composed of bending deformation by repeated local heat and cooling. By this thermal process, corrosion properties and microstructure can be affected. This work focused on the effect of induction heating bending process on the properties of ASME SA106 Gr. C low carbon steel pipes. Microstructure analysis, hardness measurements, and immersion corrosion test were performed for base metal and bended area including extrados, intrados, crown up, and down parts. Microstructure was analyzed using an optical microscope and SEM. Hardness was measured using a Rockwell B scale. Induction heat bending process has influenced upon the size and distribution of ferrite and pearlite phases which were transformed into finer structure than those of base metal. Even though the fine microstructure, every bent area showed a little lower hardness than that of base metal. It is considered that softening by the bending process may be arisen. Except of I2, intrados area, the others showed a similar corrosion rate to that of base metal. But even relatively high rate of intrados area was very low and acceptable. Therefore, it is judged that induction heat bending process didn't affect boric acid corrosion behaviour of carbon steel.

The development of UV falme detector (UV 화재감지장치 개발)

  • Gwon, O-Seung;Jeong, Chang-Gi;Lee, Bok-Yeong
    • Fire Protection Technology
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    • s.28
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    • pp.48-54
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    • 2000
  • The technique detects radiant energy form a flaming fire of fuels contained carbonaceous material can be applied to fast growing fires. This technique applied detectors are ultimately effective when early detecting fire alarm system is required or the smoke and heat detectors can not applied. In Korea Fire regulation, a flame detector should be install in case that the installation height is higher than 20[m], chemical plant, hangar refinery. Therefore it is really necessary that a flame detector has to be developed as soon as possible. With foundation technique of flame detector, ideal sensing element and stable circuit design, a trial UV flame detector is manufactured. The stable and reliable technique of flame detector is established through the repeateed perfomance test and modification. An early detecting fire alarm device is developed through the modification, supplement of the structure and circuit. Results of the R & D for the manufacture of an excellent flame detecting device is carried out with the establishment of technique for the mass production and the qualified manufacturing process.

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A study on electrical and mechanical properties and press formability of a Cu/Ag composite sheet (Cu/Ag 복합판재의 전기/기계적 성질 및 프레스 성형성에 관한 연구)

  • Shin, Je-Sik
    • Design & Manufacturing
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    • v.6 no.1
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    • pp.95-100
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    • 2012
  • In this study, a novel Cu composite sheet with embedded high electric conduction path was developed as another alternative for the interconnect materials possessing high electrical conductivity as well as high strength. The Cu composite sheet was fabricated by forming Ag conduction paths not within the interior but on the surface of a high strength Cu substrate by damascene electroplating process. As a result, the electrical conductivity increased by 40% thanks to mesh type Ag conduction paths, while the ultimate tensile strength decreased by 20%. The interfacial fracture resistance of Cu composite sheet prepared by damascene electroplating increased by above 50 times compared to Cu composite sheet by conventional electroplating. For feasibility test for practical application, a leadframe for LED module was manufactured by a progressive blanking and piercing processes, and the blanked surface profile was evaluated as a function of the volume fraction of Ag conduction paths. As Ag conduction path became finer, pressing formability improved.

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Physical and Particle Flow Modeling of Shear Behavior of Non-Persistent Joints

  • Ghazvinian, A.;Sarfarazi, V.;Nejati, H.;Hadei, M.R.
    • Proceedings of the Korean Society for Rock Mechanics Conference
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    • 2011.09a
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    • pp.3-21
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    • 2011
  • Laboratory experiments and numerical simulations using Particle Flow Code (PFC2D) were performed to study the effects of joint separation and joint overlapping on the full failure behavior of rock bridges under direct shear loading. Through numerical direct shear tests, the failure process is visually observed and the failure patterns are achieved with reasonable conformity with the experimental results. The simulation results clearly showed that cracks developed during the test were predominantly tension cracks. It was deduced that the failure pattern was mostly influenced by both of the joint separation and joint overlapping while the shear strength is closely related to the failure pattern and its failure mechanism. The studies revealed that shear strength of rock bridges are increased with increasing in the joint separation. Also, it was observed that for a fixed cross sectional area of rock bridges, shear strength of overlapped joints are less than the shear strength of non-overlapped joints.

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Application of Reversed-Phase Solid Phase Extraction for the HPLC Analysis of Microcystins in Water (다량 시료중 마이크로시스틴의 농축 및 분석)

  • Kim, Myeong-Hee;Kim, Tae-Seung;Kim, Tae-Keun;Park, Sun Ku
    • Analytical Science and Technology
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    • v.13 no.3
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    • pp.399-402
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    • 2000
  • To determine the concentrations of microcystins present in lake water or in tap water using high performance liquid chromatography, it is necessary to concentrate a large volume of water samples (about 20 L) into very small volume (0.1-0.3 mL). Concentration can be conveniently done when disc type solid phase extraction (SPE) apparatus is used. Using this apparatus we have investigated the recovery rates of three kinds of microcystins, RR, YR, LR. The recovery rates were relatively low and the reproducibilities were not good either. It is expected, however, that the appropriate selection of the disc conditioning and eluting solvents and reproducible reconcentration process after SPE will improve both the recovery rates and the reproducibilities.

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Diamond Conditioner Wear Characterization for a Copper CMP Process

  • Boruckia, L.;Zhuang, Y.;Kikuma, R.;Rikita, N.;Yamashita, T.;Nagasawa, K.;Lee, H.;Sun, T.;Rosales-Yeomans, D.;Philipossian, A.;Stout, T
    • Transactions on Electrical and Electronic Materials
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    • v.8 no.1
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    • pp.15-20
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    • 2007
  • Conditioner wear, copper polish rates, pad temperature and coefficient of friction (COF) are measured for two novel Mitsubishi Materials Corporation designs during an extended wear and polishing test. Both designs are coated with a $Teflon^{TM}$ film to reduce substrate wear and chemical attack. Using optical interferometry, changes in the coating that result in gradual changes in diamond exposure are measured. Theories of the COF, conditioning, and polishing are applied to explain the observed performance differences between the designs.

An Estimation on Characteristics of SOG Film for MEMS Application (MEMS 응용을 위한 SOG 막의 특성 평가)

  • Kim, Hyoung-Dong;Lee, Seong-Jun;Pack, Seung-Ho;Kim, Chul-Ju
    • Proceedings of the KIEE Conference
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    • 1995.11a
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    • pp.609-611
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    • 1995
  • In this study, we experimented the properties of SOG film as sacrificials layers in surface micromachining and made $SiO_2$ films through spin, bake, cure process. When we culled SOG films once, SOG film thickness is 1000 $\sim$ 3000 ${\AA}$. Then we coaled 200-${\AA}$ SOG film on 9000 ${\AA}$-CVD oxide and then we fabricated test structure, cantilever and ring/beam structure. We estimated deformed structure by SEM. As the results, The deformation of the structure layer in the SOG-coated sacrificial layers is small compared with that or the structure layer on CVD oxide or PSG. In the future, we use multi coated SOG films, SOG film become adequate material as sacrificial layer.

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A Study on The Optimization of Three-Dimensional Forging Processes Using The Sensitivity Method (민감도 해석을 이용한 3차원 단조공정의 최적설계에 대한 연구)

  • Lee S. R.;Yang D. Y.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2005.10a
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    • pp.277-280
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    • 2005
  • A shape optimization is applied to achieve a design objective in three-dimensional forging processes. In multi-stage forging processes, among the important design aspects, the die shape fur preforming is regarded as the design variable since it influences the forged part relatively higher than the others. The rigid-plastic finite element method and the sensitivity method are employed and formulated to solve a formulated optimization problem. An approximation scheme is also used for the direction search during the optimization. The upset forging of a square box is selected as a test example in order to demonstrate and verify the optimization process of this study. After the optimization, the optimized shape of the die yields a finial product of desire shape.

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