• Title/Summary/Keyword: R&D Phase

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THE ELECTROMAGNETIC PROPERTIES OF Mg-Mn FERRITES

  • Lee, D.Y.;Cho, S.I.;Shon, H.J.;Hur, W.D.
    • Journal of the Korean Magnetics Society
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    • v.5 no.5
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    • pp.552-555
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    • 1995
  • The magnetic properties of Mg-Mn ferrites were investigated in the composition range of $Mg_{a}Mn_{b}Fe_{c}O_{4\pm\delta}$ (a+b+c=3) with the addition of $Al_{2}O_{3}$. In $MgO-MnO-Fe_{2}O_{3}$ ternary system, the spinel single phase existed within the composition range of MgO-50 mol%, MnO-70 mol% and $Fe_{2}O_{3}-60\;mol%$. The saturation magnetic flux density increased with the increase of $Fe_{2}O_{3}$ content and showed the maximum at the stoichiometric composition of $(Mg,Mn)Fe_{2}O_{4}$. In $Mg_{x}Mn_{1-x}Fe_{2}O_{4}(x=0.2~0.8)$ system, the saturation magnetic flux density showed the maximum at $Mg_{0.2}Mn_{0.8}Fe_{2}O_{4}$. The addition of $Al_{2}O_{3}$ resulted in the decrease of saturation magnetic flux density but increased the electrical resistivity.

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Identification of Homoserine Lactone Derivatives Using the Methionine Functionalized Solid Phase Synthesis by Gas Chromatography/Mass Spectrometry

  • Moon, Hong-Sik
    • Archives of Pharmacal Research
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    • v.27 no.1
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    • pp.25-30
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    • 2004
  • Combinatorial homoserine lactone mixtures and individual products were obtained from the methionine-functionalized resin in solid-phase synthesis. The four-step process consisting of a coupling step of an N-Fmoc-L-methionine, deprotection of N-Fmoc group, N-coupling with a carboxylic acid, and cleavage reaction through a polymer supported strategy is described. Gas chromatography-mass selective detector (GC-MSD) techniques provide the most powerful methods for identifying both the combinatorial mixtures and individual products.

Development of phase shifter for Ka-band Passive Phase Array Seeker and Seeker Performance Analysis due to the Phase Error of Phase Shifter (Ka-대역 수동위상배열탐색기용 위상 변위기 개발 및 변위기 위상 오차에 의한 탐색기 성능 분석)

  • Kim, Youngwan;Woo, Seon-keol;Kwon, Jun-beom;Kang, Yeon-duk;Park, Jongkuk
    • The Journal of the Institute of Internet, Broadcasting and Communication
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    • v.19 no.3
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    • pp.149-155
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    • 2019
  • In this paper, phase shifter has been designed and manufactured to apply to passive phase array seeker for Ka-band and its performance was confirmed. It was designed as a key element for conducting electric beam steering by adjusting the phase of the array element. Insertion loss of less than 1.5dB and phase accuracy of less than $10^{\circ}$(RMS) in operation bandwidth of 1GHz were checked. The performance identified by the actual fabrication was further analyzed by applying the beam pattern analysis based on the array synthesis theory. The effect of the final performamnce of the proven phase shifter on the performance and pointing error and angular accuracy of the passive phase array antenna beam pattern was analyzed. Then, the validation of the proposed phase shifter has been made.

Determination and Ethylene Oxide(EO) Separation of Polysorbates by RP-HPLC (역상 HPLC에 의한 polysorbates의 산화에틸렌(EO) 분리 및 정량분석)

  • Lee, Yong-Hwa
    • Journal of the Korean Applied Science and Technology
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    • v.29 no.4
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    • pp.585-593
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    • 2012
  • The EO separation and quantitative determination of polysorbate 20, polysorbate 40, polysorbate 60 and polysorbate 80 was carried out by reversed phase HPLC. The water/acetonitrile was used for the mobile phase of gradient conditions. An YMC Pack Ph ($250mm{\times}4.6mm$ i.d., $5{\mu}m$) and Phenomenex C4 ($250mm{\times}4.6mm$ i.d., $5{\mu}m$) and the selected ELSD detector was applied. The analysis results of HPLC showed good linearity with correlation coefficient of $r^2$=0.997 in the rage of $180.2{\sim}980.5{\mu}g/mL$ and detection limit.

A Design of K-Band Low Phase noise Oscillator by Direct Coupling of K-band Dielectric Resonator (유전체 공진기의 직접결합에 의한 K-Band 저위상잡음 발진기 설계)

  • Lim, Eun-Jae;Han, Geon-Hee;Rhee, Young-Chul
    • The Journal of the Korea institute of electronic communication sciences
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    • v.9 no.1
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    • pp.17-24
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    • 2014
  • In this paper, we analysed coupling coefficient between dielectric resonator of high dielectric constant and microstrip line to design for low phase noise dielectric resonator by direct coupling. Also we analysed phase noise of dielectric resonance oscillator with parallel feedback circuit to complement Q by high dielectric constant. We obtained a result from high-stability dielectric oscillator which is optimum designed through analysis of dielectric resonance oscillator phase noise and coupling coefficient. The result is that the phase noise was -83.3dBc/Hz@1KHz at 20.25GHz when we used about 3.6 coupling coefficient and ${\epsilon}_r$=30 dielectric resonator of 20.25GHz dielectric resonance oscillator. As a result, we suggested the direct-connect design method by frequency multiplication mode to prevent phase noise loss at K-Band.

Synchrotron SAXS Study on the Micro-Phase Separation Kinetics of Segmented Block Copolymer

  • Lee, Han-Sup;Yoo, So-Ra;Seo, Seung-Won
    • Fibers and Polymers
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    • v.2 no.2
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    • pp.98-107
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    • 2001
  • The phase transition behavior isothermal micro-phase separation kinetics of polyester-based thermoplastic elastomer were studied using the synchrotron X-ray scattering(SAXS) method. The structural changes occurring during heating period were investigated by determining the changes of the one-dimensional correlation function, interfacial thickness and Porod constant. Based on the abrupt increases of the domain spacing and interfacial thickness, a major structural change occurring well below the melting transition temperature is suggested. Those changes are explained in terms of melting of the thermodynamically unstable hard domains or/and the interdiffusion of the hard and soft segments in the interfacial regions. SAXS profile changes during the micro-phase separation process were also clearly observed at various temperatures and the separation rate was found to be sensitively affected by the temperature. The peak position of maximum scattering intensity stayed constant during the entire course of the phase separation process. The scattering data during the isothermal phase separation process was interpreted with the Cahn-Hilliard diffusion equation. The experimental data obtained during the early stage of the phase separation seems to satisfy the Cahn-Hilliard spinodal mechanism. The transition temperature obtained from the extrapolation of the diffusion coefficient to zero value turned out to be about 147$\pm$$2^{\circ}$, which is close to the order-disorder transition temperature obtained from the Porod analysis. The transition temperature was also estimated from the inveriant growth rate. By extrapolating the inveriant growth rate to zero, a transition temperature of about 145$\pm$$\pm$$2^{\circ}$ was obtained.

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A Study On The Three-Phase Bridge Type Converter Furnished Diode-Bridge Circuits (Diode-Bridge방식 3상 Thyristor순역전력 변환장치의 개발에 관한 연구)

  • Cheul U Kim
    • 전기의세계
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    • v.23 no.4
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    • pp.60-65
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    • 1974
  • This paper is to study on the pilot work of bi-directional S.C.R. power converter adopted by the method of diode-bridge type circuit. This apparatus acts as a converter when it is used in convering 3-phase a.c source to d.c output, and it can be used as an inverter which recovering surplus d.c power to a.c source when d.c load become active to cause the induced voltage higher than the presetted point of d.c output voltage. At the same time, its d.c voltage varies continuously in the presetted range of positive and/or negative polarity. As a result of test, the AC/DC bi-directional power converter represents maximum converting efficiency of 91% and power factor of 0.98. Furthermore, this converter also can be applied as a cycleconverter by varying the period of gate triggering signal.

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The Magnetic and Magnetostrictive Properties of Melt-Spun Ribbons of B Containing Terfenol-D Alloys

  • Kim, S. R.;S. Y. Kang;S. H. Lim
    • Journal of Magnetics
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    • v.2 no.1
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    • pp.1-6
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    • 1997
  • The magnetic and magnetostrictive properties of melt-spun ribbons of the alloys (R0.33Fe0.67)1-xBx (R=Tb0.3Dy0.7 and 0$\leq$x$\leq$0.06) are ivestigated as a function of wheel speed during melt-quenching. The saturation magnetiation of the alloys with a crystalline phase ranges from 70 to 80 emu/g and does not vary substantially with the B content. The saturation magnetization of an amorphous phase, which is formed at the condition of thigh wheel speed and high B content, is reduced significantly, however. The coercive force is minimum at x= 0.02 and increases monotonously with the further increase of B content when the microstructure mainly consists of a crystalline phase, but again it is reduced significantly by the formation of an amorphous phase. The low field sensitivity of magnetostriction with magnetic field is found to be good for the alloys with x$\leq$0.04 over a wide range of wheel speed. This magnetostrictive behavior is in contrast with that observed previously for Dy-Fe and Tb-Fe based alloys and is thought to be due to low intrinsic magnetocrystalline anisotropy of the compound.

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Phase Stability of Laser-ablated $SmBa_2Cu_3O_{7-y}$ thin Films Investigated by Raman Scattering Spectroscopy

  • Kim, G.;Jeong, A.R.;Jo, W.;Park, D.Y.;Cheong, H.;Tsukada, A.;Hammond, R.H.;Beasley, M.R.
    • Progress in Superconductivity
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    • v.11 no.2
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    • pp.141-146
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    • 2010
  • Phase stability diagram and boundary of a- and c-axis orientation of $SmBa_2Cu_3O_{7-y}$ (SmBCO) thin films grown by pulsed laser deposition (PLD) were reported with studies based on x-ray diffraction [1]. Four different samples are systematically analyzed: normal c-axis oriented orthorhombic $SmBa_2Cu_3O_{7-y}$, a-axis oriented $SmBa_2Cu_3O_{7-y}$, c-axis oriented orthorhombic $SmBa_2Cu_3O_{7-y}$ with $Sm_2BaCuO_5$ phase, and a mixture with c-axis oriented orthorhombic $SmBa_2Cu_3O_{7-y}$ and anomalously long-c tetragonal $SmBa_2Cu_3O_x$. Raman scattering spectroscopy equipped with polarization analysis elucidates the crystal orientation and the origin of the growth of the materials. It indicates that the technique can be used for quality control of conductor manufacturing processes as well as for enhancement of the materials properties.

Building Transparency on the Total System Performance Assessment of Radioactive Repository through the Development of the Cyber R&D Platform; Application for Development of Scenario and Input of TSPA Data through QA Procedures (Cyber R&D Platform개발을 통한 방사성폐기물 처분종합성능평가(TSPA) 투명성 증진에 관한 연구; 시나리오 도출 과정과 TSPA 데이터 입력에서의 품질보증 적용 사례)

  • Seo, Eun-Jin;Hwang, Yong-Soo;Kang, Chul-Hyung
    • Journal of Nuclear Fuel Cycle and Waste Technology(JNFCWT)
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    • v.4 no.1
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    • pp.65-75
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    • 2006
  • Transparency on the Total System Performance Assessment (TSPA) is the key issue to enhance the public acceptance for a radioactive repository. To approve it, all performances on TSPA through Quality Assurance is necessary. The integrated Cyber R&D Platform is developed by KAERI using the T2R3 principles applicable for five major steps : planning, research work, documentation, and internal & external audits in R&D's. The proposed system is implemented in the web-based system so that all participants in TSPA are able to access the system. It is composed of three sub-systems; FEAS (FEp to Assessment through Scenario development) showing systematic approach from the FEPs to Assessment methods flow chart, PAID (Performance Assessment Input Databases) being designed to easily search and review field data for TSPA and QA system containing the administrative system for QA on five key steps in R&D's in addition to approval and disapproval processes, corrective actions, and permanent record keeping. All information being recorded in QA system through T2R3 principles is integrated into Cyber R&D Platform so that every data in the system can be checked whenever necessary. Throughout the next phase R&D, Cyber R&D Platform will be connected with the assessment tool for TSPA so that it will be expected to search the whole information in one unified system.

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