• 한국재료학회지
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• 제18권10호
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• pp.511-514
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• 2008

We have synthesized $Eu^{3+}$-doped $YVO_4$ phosphors by using a hydrothermal method and investigated their luminescent properties. Aqueous solutions of $Y_2O_3,\;V_2O_5,\;Eu_2O_3$, and nitric acid with various pH values were used as the precursors. The crystallinity, surface condition, and emission characteristics were examined using XRD, FT-IR, and photo-excited spectrometer. $Eu^{3+}$ incorporation followed by the efficient red emission strongly depends on the acidity of solution media. The emission intensity becomes stronger as the pH values increase to 7 and then gradually decreases. This phenomenon might be related to the hydroxyl quenching effect, which is induced by surface bound OH-groups.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2003년도 하계학술대회 논문집 Vol.4 No.2
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• pp.934-937
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• 2003

Glasses in the system $CuO-P_2O_5-V_2O_5$ were prepared by a press-quenching method on the copper plate. The glass-ceramics from these glasses were obtained by post-heat treatment, and the crystallization behavior and DC conductivities were determined. The conductivities of the glasses were range from $10^{-6}s.Cm^{-1}$ at room temperature, but the conductivities of the glass-ceramics were $10^{-3}s.Cm^{-1}$ increased by $10^3$ order. The crystalline product in the glass-ceramics was $CuV_2O_6$. Heat-treatment conditions influenced the crystal growth of $CuV_2O_6$ and conductivity. The linear relationship between in (${\sigma}T$) and $T^{-1}$ suggested that the electrical conduction in the present glass-ceramics would be due to a small polaron hopping(SPH) mechanism.

• Nuclear Engineering and Technology
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• 제53권6호
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• pp.2025-2037
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• 2021

The influence of lead cations on natural quartz (QZ) from Egypt as a glass shielding material for the composition with nominal formula (10Na₂O - (90 - x) QZ - xPbO (where x = 30, 35, 40, 45 and 50 mol %)) was examined. The studied samples are synthesized via the melt quenching method at 1050 ℃. The X-ray diffraction XRD patterns were confirmed the glass nature for studied samples. Moreover, the optical properties, and the transparency for all compositions were examined by UV-Vis spectroscopy. Also, the major elemental composition of the natural quartz were estimated via the X-ray fluorescence (XRF) technique. Further, the density and molar volume were determined. Furthermore, the nuclear shielding parameters such as, mass attenuation coefficient, effective atomic number, electronic density, the total atomic, and electronic cross sections as well as the mean free path, and the half value layer with different gamma ray energies (81 keV-1407 keV) were calculated. Besides, the results showed that the shielding behavior towards the gamma ray radiation for all glass samples was increased as the increment in PbO concentration in the glass system.

• 한국기계가공학회지
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• 제20권6호
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• pp.10-16
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• 2021

Drilling is a crucial process that takes up a significant amount of weight during machining operations. In addition, drill tip-type tools and related operations have been developed for manufacturing industries to achieve economic efficiency. In this study, SM45C carbon steel, widely used for machine structures, was utilized as the working material after quenching and tempering. Insert-tip types of carbide tools, such as TiN and TiAlN, were used as tool materials. Drilling conditions such as the spindle revolution, feed rate, step of cut, and tool diameter were used to measure roughness, roundness, and straightness using the orthogonal array table statistical method. The surface roughness, roundness, and straightness characteristics based on the conditions were analyzed using ANOVA. The results showed that the spindle speed and feed rate were the main factors influencing carbide insert-tip drilling under the same conditions as the experimental conditions.

• 한국진공학회지
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• 제6권S1호
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• pp.53-58
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• 1997

It is well known that the equiatomic FeAl alloy crystallizes in a paramagnetic CsCl structure and is very stable in a wide temperature range owing to a significant charge transfer from Al to Fe. A presence of structural defects normally enhances the magnetic and magneto-optical properties of this alloy. In this study spin-resolved photoemission and magnetic circular dichroism (MCD) were carried out on both ordered and disordered $Fe_{0.52}Al_{0.48}$ alloy films. The disordered state in the alloy films was obtained by a vapor quenching deposition on cooled substrates. It is shown that the order-disorder transition in the Fe0.52Al0.48 alloy films leads to a significant change in the spin polarization. Form the MCD results the orbital and spin magnetic moments of the constituent atoms are obtained. According to the sum rule the spin and orbital magnetic moments of Fe in the disordered FeAl film are $\mu\frac{SR}{spin}=0.8\mu_B$ and $\mu\frac{SR}{orb}=0.14\mu_B$ respectively. The spin magnetic moment is also evaluated to be $\mu\frac{BR}{spin}=0.77\mu_B$ by the branching ration method employing a photon polarization of 90%.

• 천문학회보
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• 제44권2호
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• pp.38.3-38.3
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• 2019

We present newly discovered dwarf galaxy candidates in deep wide-field images of NGC 1291 obtained with KMTNet. We identify 15 dwarf galaxy candidates by visual inspection within the virial radius of NGC 1291. Using imaging simulations, we demonstrate that our imaging data is complete up to 26 mag arcsec^-2 or -10 abs.mag with > 70% of the completeness rate. We also apply automated detection method to find the dwarfs. However, the completeness and the reliability are relatively low compared to the visual inspection. We find that structural and photometric properties of dwarf candidates such as effective radius, central surface brightness, Sérsic index, and absolute magnitude appear to be consistent with those of known dwarf galaxies in nearby groups and clusters, except for color. NGC 1291, residing in a relatively isolated environment, tends to accompany bluer dwarf galaxies (≃0.58) than those in denser environment. It shows that the quenching of dwarfs is susceptible to the environment.

• Nuclear Engineering and Technology
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• 제56권9호
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• pp.3796-3803
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• 2024

By employing the melt-quenching technique, the ZnO-SrO-B₂O₃-PbO (ZSBP) glasses have been successfully fabricated. The derivative of Absorption Spectra Fitting (DASF) method was used to study the energy band gap (E_g) of the glasses which decreases from 3.57 eV to 3.39 eV. The structural properties have been studied using the Raman spectroscopy. The glass transition temperature (T_g) decreases with increase in concentration of the lead oxide. The current study examines the radiation shielding properties at 30.80-444 keV. The addition of PbO to the glasses resulted in a proportionate increase in the mass attenuation coefficient (MAC), suggesting a diminishing tendency in radiation transmission. At 30.80 keV, the MAC values are extremely high and range from 18.06 to 21.11 cm²/g. As density rises, the half value layer (HVL) decreases. In addition, the average HVL (${\overline{HVL}}$) decreases. The glass thickness required to reduce the radiation intensity to 90 %, 50 %, 25 %, and 10 % of its initial value is investigated at an energy of 35.80 keV. The T90 %, T50 %, T25 %, and T10 % values are 0.0020, 0.0132, 0.0264, and 0.0439 cm, respectively. The results suggest that a greater thickness of the radiation barrier is necessary to attain the necessary degree of attenuation.

• 한국결정성장학회지
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• 제21권2호
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• pp.82-86
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• 2011

인공경량 골재는 다결정질 소성체를 주 구성으로 하므로 골재 내부에 다량의 공극이 일정비율로 형성되는 것이 특징이다. 이러한 인공경량 골재는 조직 구조의 특성상 외부환경의 변화에 의해 수분이 비정상적인 이동을 보이는 경향이 있다. 다공질 재료의 수분 방출 특성은 일반적으로 기공률 및 기공크기 분포에 크게 좌우되지만, 인공적으로 소결 제조된 경우에는 표면에 생성된 치밀한 구조의 표피층에도 많은 영향을 받을 것으로 생각된다. 인공경량 골재 내부의 수분 이동에 미치는 요인은 골재내의 세공 및 공극의 분포와 형상, 크기, 그리고 프리웨팅 방법 등이 있으며 각 조건에 따라 상당한 차이를 보인다. 본 연구에서는 인공경량 골재를 제조하여 골재의 가압시 흡수 특성이나 침수시간에 대한 흡수율의 거동에 대한 명확한 규명을 함으로써 경량골재 펌프압송을 위한 기초적 자료를 제공하고자 하였다. 본 실험에 사용된 인공경량골재는 독일 'L'사의 상업용 인공경량골재와 본 연구팀이 제조한 2가지 조성의 인공경량골재를 사용하였으며, 골재 수분함침시간, 진공압력, 급냉조건을 변화시켜 골재의 흡수율을 측정하였다. 인공경량골재를 $300^{\circ}C$ 에서 급냉 하였을 경우 24시간 침수보다 높은 흡수율을 보였고, 진공압력에 따라 흡수율이 증가하는 경향이 있으며, -300 mmHg의 진공 압력시 24시간 침수보다 "L"사 골재는 54 %의 높은 증가를 보였으나 K622와 K73 골재는 비교적 적은 2 % 내외의 흡수율 증가양상을 보였다.

• 대한용접접합학회:학술대회논문집
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• 대한용접접합학회 2009년 추계학술발표대회
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• pp.100-100
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• 2009

본 논문에서는 원자력발전소 1차 계통의 스테인리스강 저합금강 이종금속용접부 및 스테인리스강 동종용접부의 잔류응력을 평가하고 스테인리스강 용접부의 응력부식균열 민감성에 대해 고찰하였다. 노즐 안전단의 이종금속용접부 및 안전단 배관의 동종용접부 제작 및 소재가공에 의행 생성되는 잔류응력을 예측하기 위해 열 탄소성 유한요소법 수치해석을 수행하였으며, 용접공정과 함께 표면의 잔류응력에 기여하는 절삭 및 연삭가공과 소재의 담금질 공정을 열 탄소성적으로 모사하였다. 전산해석 결과, 스테인리스주강의 담금질 잔류응력은 무시할 수 없는 상당한 크기이므로 배관 용접잔류응력 평가 시 소재의 담금질 효과를 고려해야 할 것으로 판단된다. 이종금속 용접과 동종금속 용접공정이 보수용접 없이 정상적인 절차(내면에서 외면으로 적층)로 완성된다면, 냉각재 환경에 노출되는 용접부 내면의 잔류응력은 재료의 응력부식균열 민감성에 영향을 주지 않을 것으로 판단된다. 한편, 안전단 배관 동종용접부의 연삭가공에 의해 내면의 잔류응력이 크게 상승하는 것으로 예측되었으므로, 내면의 연삭가공 이후 표면잔류응력 완화처리(예, 버핑)가 필요하다.

• 한국재료학회지
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• 제8권8호
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• pp.693-698
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• 1998

$AI_{2}$$O_{3}$와 $Na_{2}$O가 AFD법에 의해 제조된 sodium borosilicate 유리박막의 특성에 미치는 영향을 조사하였다. $AI_{2}$$O_{3}$함량이 증가함에 따라 $66SiO_2-27B_2O_3-7Na_2O$유리박막의 상분리는 억제되었으며, 6.0wt%의$ AI_{2}$$O_{3}$가 첨가되었을 때 공기중 급냉조건하에서 상분리가 없는 유리박막이 얻어졌다. $AI_{2}$$O_{3}$함량이 1.5에서 6.0wt%로 증가함에 따라 유리박막의 굴절율은 1.4610에서 1.4701로 선형적으로 증가하였으며, 복굴절률을 나타내는 TE 모드와 TM 모드의 차이도 점차적으로 증가하였다. 그러나 복굴절률은 유리박막을 전이온도 이하에서 재열처리함으로써 감소시킬 수 있었다. $66SiO_2-27B_2O_3-7Na_2O$+6wt% $AI_{2}$$O_{3}$에 $Na_2O$의 함량을 증가시켜 Na2O/B2O3가 0.23, 0.34, 0.45, 0.56인 유리박막을 제작하였다. Na2O/B2O3의 비가 증가함에 유리박막의 굴절율 및 복굴절률은 증가하는 경향이 있었다. 또한 $Na_2O/B_2O_3$의 비가 증가함에 따라 유리박막의 상분리는 가속화되었다.