• Title/Summary/Keyword: Quenching conditions

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Effects of Continuous Annealing Conditions on the Properties of Extra Low Cabon Steel Sheets Containing B, Nb and Ti (B, Nb 및 Ti를 함유한 극저탄소강판에서 연속열처리조건이 재질에 미치는 영향)

  • Lee, Jong-Mu;Yun, Guk-Han;Lee, Do-Hyeong
    • Korean Journal of Materials Research
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    • v.4 no.1
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    • pp.44-54
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    • 1994
  • Effects of cooling rate, cold reduction %, continuous annealing treatments on the recrystallization texture structure of the A1 killed extra low carbon steel sheet contaning Ti, Nb, and B were investigated. The texture coefficient ratio TC (222)/TC (200) tends to increase with decreasing the cooling rate of the coling process and increasing cold reduction %. However, the texture coefficient ratio tends to decrease as the cold reduction % increases from 80% to 90%, which may be due to the change of the primary texture structure from {554} (225) to {ill] (1 1%). The optimum fabrication procedures for the steel sheet with a maximum texture coefficient ratio may be : furnance cooling after the coiling treatment, 80% cold reduction and the continuous annealing treatment of holding at 80O0C for 1 min., water quenching and then holding at $450^{\circ}C$ for 5min.

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Recyclability Analysis of Slags Obtained at Gasification and Incineration-Melting Conditions (가스화와 소각 용융 조건에서 생성된 슬랙의 재활용성 분석)

  • 윤용승;이계봉
    • Journal of Energy Engineering
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    • v.13 no.1
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    • pp.82-91
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    • 2004
  • In order to utilize inorganic components in coal and wastewater sludge as an environmentally stable material, slag-forming is considered as one of the suitable methods better than producing as an ash. Coal slag that was produced by gasification as well as the slag made from wastewater sludge by incineration or melting process have been analyzed with the viewpoint of recyclability. Slags produced by water quenching exhibited a cracked shape that has a size of few millimeters with sharp edges. Slags contain the unburned carbon content below 0.15% and expose mostly amorphous structural characteristics. Analysis results in the extraction of heavy metal compounds demonstrate that both slags from coal and wastewater sludge could be utilized as a safe recycle material even with a Japanese environmental regulation that is ten times more stringent than the current Korean standard. Slags from coal and wastewater sludge show significant differences in contents of each heavy metal compound. Since the future trend of environmental regulation shifts to the control of total content for each heavy metal compound, proper mixing of slags that contain different heavy metal contents might be an option for manufacturing recycle materials.

Homology modeling of the structure of tobacco acetolactate synthase and examination of the model by site-directed mutagenesis

  • Le, Dung Tien;Yoon, Moon-Young;Kim, Young-Tae;Choi, Jung-Do
    • Proceedings of the Korean Society for Bioinformatics Conference
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    • 2003.10a
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    • pp.277-287
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    • 2003
  • Acetolactate synthase (ALS, EC 4.1.3.18; also referred to as acetohydroxy acid synthase) catalyzes the first common step in the biosynthesis of valine, leucine, and isoleucine in microorganisms and plants. Recently X-ray structure of yeast ALS was available. Pair-wise alignment of yeast and tobacco ALS sequences revealed 63% sequence similarity. Using Deep View and automatic modeling on Swiss model server, we have generated reliable models of tobacco ALS based on yeast ALS template with a calculated pair-wise RMSD of 0.86 Angstrom. Functional roles of four residues located on the subunit interface (H142, El43, M350, and R376) were examined by site-directed mutagenesis. Seven mutants were generated and purified, of which three mutants (H142T, M350V, and R376F) were found to be inactivated under various assay conditions. The H142k mutant showed moderately altered kinetic properties. The E143A mutant increased 10-fold in K$_m$ value while other parameters remained unchanged. The M350C mutant was strongly resistant to three tested herbicides, while the R376k mutant can bind with herbicide carder at similar affinity to that of wild type enzyme, as determined by tryptophan quenching study. Except M350V mutant, all other mutants were ate to bind with cofactor FAD. Taken together, it is likely that residues H142 and E143 are located at the active site, while residues M350 and R376 are possibly located at the overlapping region of active site and herbicide binding site of the enzyme. Our data also allows us to hypothesize that the interaction between side chains of residues M350 and R376 are probably essential for the correct conformation of the active site. It remains to be elucidated that, whether the herbicide, upon binding with enzyme, inactivates the enzyme by causing change in the active site allosterically, which is unfavorable for catalytic activity.

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A Study on the Removal Characteristics of Phenol Using Waste CDQ Dust as Adsorbent (폐CDQ 분진을 흡착제로 한 페놀제거특성에 관한 연구)

  • Kim, Jin-Wha;Lee, Jung-Min;Kim, Dong-Su
    • Journal of Korean Society of Environmental Engineers
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    • v.22 no.7
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    • pp.1213-1223
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    • 2000
  • The adsorption characteristics of phenol has been studied by using CDQ (Cokes Drying Quenching) dust as an adsorbent. The adsorption capacity of CDQ dust was shown to be 42% about removal for 300 ppm phenol solution at the equilibrium adsorption time of 60 min. Removal percentage of phenol increased as the initial phenol concentration was raised in the experimental conditions and the adsorption behavior was explained well by Freundlich adsorption isotherm. Kinetic study showed that the adsorption followed 1st, 1.5th, and 2nd-order rate equation in the sequence as the adsorption time passed. Since the adsorption amount of phenol was increased as the adsorption temperature was raised, the adsorption was thought to be endothermic, and several thermodynamic parameters have been calculated based upon experimental data. Adsorbed amount of phenol on CDQ dust changed little according to the variation in the solution pH except for the slight decrease under the strong alkaline condition.

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Analysis of the Aluminum Extrusion Process Equipped with the Continuous Heat Treatment System

  • Lee, Bong-Sang;Cho, Young-Hee;Lee, Jeong-Min;Lim, Hak-Jin;Koo, Jar-Myung;Yoon, Bo-Hee;Lee, Tae-Hyuk;Lee, Jong-Hyeon
    • Korean Journal of Materials Research
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    • v.21 no.1
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    • pp.39-45
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    • 2011
  • In this study, the heat flow of the plant scale aluminum extrusion process was investigated to establish optimum continuous heat treatment conditions. During the extrusion of 6061 aluminum alloy, processing parameters such as the extrusion pressure, speed and temperature histories of billets were logged as a function of time. The surface temperature of the billets increased at constant ram speed, while it decreased with decreases of the ram speed. In order to maintain the billet temperature within a solutionizing temperature range prior to the succeeding water quenching step, the ram speed or the temperature of the blower should be controlled. The temperature histories of the billets during the extrusion and hot air blowing processes were successfully simulated by using the velocity boundary model in ANSYS CFX. The methodology to design an optimum process by using a commercial simulation program is described in this study on the basis of the metallurgical validation results of the microstructural observation of the extrudates. The developed model allowed the advantages of taking into account the motion of the extrudate coupled with the temperature change based on empirical data. Calculations were made for the extrudate passing through the isothermal chamber maintained at appropriate temperature. It was confirmed that the continuous heat treatment system is beneficial to the productivity enhancement of the commercial aluminum extrusion industry.

A Study on the Electrical Discharge Blind Hole Tap Machining of STD11 with Copper Electrode (구리전극봉을 이용한 합금공구강재(STD11)의 비관통 방전 탭 가공에 관한 연구)

  • Park, In-Soo;Wang, Duck-Hyun;Kim, Gi-Tae
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.16 no.3
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    • pp.38-44
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    • 2017
  • The technology of electrical discharge tap machining may be appropriate for making thread out of highly brittle material. Especially, it is very difficult to machine tap with the traditional method if the brittle material has been hardened by quenching. In this study, the shape of electrical discharge blind hole tap machining was analyzed by discharge time, discharge current, and the flushing hole condition after quenched the tool steel of STD11 has discharged the tap shape with a screw-shaped copper(Cu) electrode. An experimental design was planned and analyzed by Taguchi robust experimental design. The result showed that the shape of the blind hole discharge tap was influenced by the flushing hole, discharge time, and discharge current. The most important factor of the processing conditions was found to be the discharge current. When blind hole EDM with a copper electrode with a flushing hole was conducted, the discharged shape was found to be smooth and the angle of the discharged tapped thread was also found to be close to the thread angle of $60^{\circ}$. As the values of discharge time and discharge current increased, the EDMed surface coarsened due to the increase of the single discharge energy and the shape of the thread collapsing.

Study on Combustion Performance and Burning Velocity in a Micro Combustor (초소형 연소기에서 연소성능과 연소속도에 대한 연구)

  • Na Hanbee;Lee Dae Hoon;Kwon Sejin
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.29 no.6 s.237
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    • pp.662-670
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    • 2005
  • The effect of heat loss on combustion performance and burning velocity of micro combustors in various conditions were exploited experimentally. Three different gases were used, and various geometric matrixes were considered to figure out the phenomena of combustion in a micro combustor. The micro combustors used in this study were constant volume combustors and had cylindrical shape. Geometric parameter of combustor was defined as combustor height and diameter. The effect of height was exploited parametrically as 1mm, 2mm and 3 mm and the effect of diameter was parameterized to be 7.5 mm and 15 mm. Three different combustibles which were Stoichiometric mixtures of methane and air, hydrogen and air, and mixture of hydrogen and air with fuel stoichiometry of two were used. By pressure measurement and visualization of flame propagation, characteristic of flame propagation was obtained. Flame propagations which were synchronized with pressure change within combustor were analyzed. From the analysis of images obtained during the flame propagations, burning velocity at each location of flame was obtained. About $7\%$ decrease in burning velocity of $CH_4/Air$ stoichiometric mixture compared with previous a empirical result was observed, and we can conclude that it is acceptable to use empirical equations for laminar premixed flame burning velocity to micro combustions. Results presented in this paper will give fine tool for analysis and prediction of combustion process within micro combustors.

The Study on Automation and Development of Strip Continuous Casting by Twin Roller Type (쌍로울형 박판연속주조공정의 개발과 자동화에 관한 연구)

  • Lee, Sang-Mae;Kim, Young-Do;Baek, Nam-Ju;Gang, Chung-Gil
    • Journal of the Korean Society for Precision Engineering
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    • v.7 no.1
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    • pp.37-52
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    • 1990
  • In this study, the characteristics of cooling and rolling during strip casting process is obtained in comparison with the experimental and analytical results. The prupose of this study is to effectively analyze the thermal and mechanical deformation of roller applying the results of the heat transfer and the pressure distribution to boundary conditions. And then the relation between strip thickness and roll deformation is shown. The second purpose is to obtain the proper condition of the continuous casting for stainless steel. The summary and conclusions can be made on the basis of the results obtained by the theories and experiments. a) The strip casting condition for the fine surface quality of tin-alloy as-cast material was obtained in accordance with the velocity of roll rotation and initial roll gap. b) The experimental condition that the dimension of the cast strip thickness coincide with that of the initial roll gap was according to the experimental result of continuous casting by twin-roll type. c) The thermoelastic finite element model to calculate the roll deformation is represented. Thermoelastic model prediction for the roll deformation are in good agreement with the experimental results considering the thermal expansion of the roll. d) The higher cooling rates were obtained by a twin-roller quenching technique. Also quenched microstructure of the rapidly solidified shell was verified. e) The magnitude of roll deformation due to the thermal expansion and roll separating force is quantit- atively represented in the analysis of continuous casting for stainless steel.

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A Study on Ageing Characteristics and Alloy Elements of SiCp Reinforced Al Matrix Composites (SiCp입자강화 Al 복합재료에 대한 합금원소의 영향과 시효특성에 관한 연구)

  • Kim, Sug-Won;Lee, Ui-Jong;Woo, Kee-Do;Kim, Dong-Keun
    • Journal of Korea Foundry Society
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    • v.21 no.1
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    • pp.7-14
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    • 2001
  • The research on new DRA(discontinuous reinforced alloy) and CRA(continous reinforced alloy) composites has been carried out to improve the properties of ceramic fiber and particle reinforced metal matrix composites(MMCs). Effects of alloying elements and aging conditions on the microstructures and aging behavior of Al-Si-Cu-Mg-(Ni)-SiCp composite have been examined. The specimens used in this study were manufactured by duplex process. The first squeeze casting is the process to make precomposite and the second squeeze casting is the process to make final composite. The hardening behavior was accelerated with decreasing the size of SiCp particle in the composites. It is considered that the dislocation density increased with increasing SiCp size, due to the different thermal deformation between Al matrix and SiCp during quenching after the solution treatment. Peak aging time to obtain the maximum hardness in 3 ${\mu}m$ SiCp reinforced Al composite was reduced than that in large size(5, 10 ${\mu}m$) of SiCp because of difference in dislocation density. Aging hardening responce(${\Delta}H$ = $H_{Max}.-H_{S.T}$) of composites was greater than that of unreinforced Al alloy because of higher density of second phases in matrix.

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The Effects of Heat-treatment on the Mechanical Properties of High Chromium Cast Irons (고크롬 주철의 기계적 특성에 미치는 열처리 영향)

  • Kim, Sug-Won;Kim, Ki-Kon;Park, Jin-Sung;Kim, Dong-Keun;Yoon, Young-Gap
    • Journal of Korea Foundry Society
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    • v.25 no.1
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    • pp.23-29
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    • 2005
  • Mechanical characteristics of Hi-Cr cast irons containing 16.8%Cr and 3.0%C were studied with various heat treatments. After as-cast Y-block ingots were annealed fully, the ingots were machined into cylinderical specimens with the size of 9mm in diameter and 20mm in length in order to investigate the effect of heat-treatments on mechanical characteristics of high Cr cast irons. All specimens were heat-treated by quenching- tempering, austempering and cyclic heat at the various temperatures(950, 1000, 1050 and $1100^{\circ}C$) respectively. The wear amount was measured for each heat-treated specimens against the counterpart of a hardened SKD11 steel at the following conditions; wearing velocity: 0.7 m/s, load: 100N and sliding distance: 70 km. After as-cast specimens were annealed, fine $M_{3}C$ carbides were formed, which affected the hardness and the wear resistance of Hi-Cr specimens. High hardness and good wear resistance were appeared on the specimens treated at 950 and $1000^{\circ}C$ and the austempered specimens show excellent wear resistance as well as high hardness.