• Title/Summary/Keyword: Quantitative Method

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A quantitative determination of surfactant mixtures by FT-IR (FT-IR을 이용한 계면활성제 혼합물의 정량)

  • 최종근;노경원
    • Journal of the Society of Cosmetic Scientists of Korea
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    • v.21 no.2
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    • pp.129-139
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    • 1995
  • To confirm the usefulness of partial least-squares(PLS) and multiple scattering correction(MSC) method for quantitation of surfactants in [quantitative methods using FT-lR, reconsitituted mixtures of LAS, MES and ELA-9 were tested. Each mixture was dissolved in 50% EtOH, dried, and applied to the KBr cell. From the IR spectra of these mixture, the variance spectrum was obtained. After repeated calibrations for the various regios of this spectrum, we found that 1245-1130cm-1 and 1070-1010cm-1 showed the strong correlation with each component of the sample mixture: all the correlation coefficients were 1.000 and quantitative errors did not exceed 0.32%. From this result, we concluded that PLS method and MSC method are very useful and can be successfully applied to Quality control.

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Production Rules Based on the Rule-Based Model for Grinding Trouble-shooting (연삭가공 트러블슈팅을 위한 룰베이스 룰의 구성)

  • Lee, Jae-Kyung;Kim, Gun-Hoi;Song, Ji-Bok
    • Journal of the Korean Society for Precision Engineering
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    • v.17 no.8
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    • pp.106-112
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    • 2000
  • Cognition and control of grinding trouble occurring during the grinding process are classified into a quantitative knowledge which depends on experimental data and qualitative knowledge which relies on skiful engineers. grinding operations include a large number of functional parameters since there are several ways of coping with ginding trouble. One is the qualitative method which depends on empirical knowledge utilizing the skilful experts from the workshop the other is the quantitative method which utilizes the experimental data obtained by sensor. But they are all difficult to accomplish from the grinding trouble-shooting system The reason is that grinding troubles are not accomplish from the grinding trouble-shooting system,. The rason is that grinding troubles are not easily controlled in the quantitative method and therefore trouble-shooting has mainly relied on the knoledge of skiful engineers. Thus there is an important issue of how a grinding touble-shooting system can be designed and what knowledge is utilized among the large amount of grinding trouble information. In this paper basic strategy to develop the grinding database by taking rule-based model which is strongly depended upon experience and intuition is described.

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Improvement of Quantitative Condition Assessment Criteria for Reservoir Embankment Safety Inspection Considering Characteristics of Small Reservoirs in Korea (소규모 저수지의 특성을 고려한 제체 안전진단의 정량적 상태평가 기준 개선)

  • Jeon, Geonyeong;Bang, Donseok
    • Journal of The Korean Society of Agricultural Engineers
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    • v.63 no.5
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    • pp.27-38
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    • 2021
  • The physical condition assessment criteria of fill dam safety inspection are now weakly regulated and inappropriate for small agricultural reservoirs since these criteria have fundamental backgrounds suitable for large-scale dams. This study proposes the degree (critical values) of defects for the quantitative condition assessment of the embankment in order to prepare the condition assessment criteria for a small reservoir with a storage capacity of less than one (1) million cubic meters. The critical values of defects were calculated by applying the method that considers the size ratios based on the dimensional data of reservoirs, and the method of statistical analysis on the measured values of the defect degree which extracted from comprehensive annual reports on reservoir safety inspection. In comparison with the current criteria, the newly proposed critical values for each condition assessment item of the reservoir embankment are presented in paragraphs 4 and 6 of the conclusion. In addition, this study presents a method of displaying geometric figures to clarify the rating classification for condition assessment items with the two defect indicators.

A quantitative method for detecting meat contamination based on specific polypeptides

  • Feng, Chaoyan;Xu, Daokun;Liu, Zhen;Hu, Wenyan;Yang, Jun;Li, Chunbao
    • Animal Bioscience
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    • v.34 no.9
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    • pp.1532-1543
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    • 2021
  • Objective: This study was aimed to establish a quantitative detection method for meat contamination based on specific polypeptides. Methods: Thermally stable peptides with good responses were screened by high resolution liquid chromatography tandem mass spectrometry. Standard curves of specific polypeptide were established by triple quadrupole mass spectrometry. Finally, the adulteration of commercial samples was detected according to the standard curve. Results: Fifteen thermally stable peptides with good responses were screened. The selected specific peptides can be detected stably in raw meat and deep processed meat with the detection limit up to 1% and have a good linear relationship with the corresponding muscle composition. Conclusion: This method can be effectively used for quantitative analysis of commercial samples.

USE OF NEAR INFRARED FOR THE QUANTITATIVE ANALYSES OF BAUXITE

  • Walker, Graham S.;Cirulis, Robyn;Fletcher, Benjimin;Chandrashekar, S.
    • Proceedings of the Korean Society of Near Infrared Spectroscopy Conference
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    • 2001.06a
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    • pp.1171-1171
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    • 2001
  • Quantitative analysis is an important requirement in exploration, mining and processing of minerals. There is an increasing need for the use of quantitative mineralogical data to assist with bore hole logging, deposit delineation, grade control, feed to processing plants and monitoring of solid process residues. Quantitative analysis using X-Ray Powder Diffraction (XRD) requires fine grinding and the addition of a reference material, or the application of Rietveld analysis to XRD patterns to provide accurate analysis of the suite of minerals present. Whilst accurate quantitative data can be obtained in this manner, the method is time consuming and limited to the laboratory. Mid infrared when combined with multivariant analysis has also been used for quantitative analysis. However, factors such as the absorption coefficients and refractive index of the minerals requires special sample preparation and dilution in a dispersive medium, such as KBr to minimize distortion of spectral features. In contrast, the lower intensity of the overtones and combinations of the fundamental vibrations in the near infrared allow direct measurement of virtually any solid without special sample preparation or dilution. Thus Near Infrared Spectroscopy (NIR) has found application for quantitative on-line/in line analysis and control in a range of processing applications which include, moisture control in clay and textile processing, fermentation processes, wheat analysis, gasoline analysis and chemicals and polymers. It is developing rapidly in the mineral exploration industry and has been underpinned by the development of portable NIR spectrometers and spectral libraries of a wide range of minerals. For example, iron ores have been identified and characterized in terms of the individual mineral components using field spectrometers. Data acquisition time of NIR field instruments is of the order of seconds and sample preparation is minimal. Consequently these types of spectrometers have great potential for in-line or on-line application in the minerals industry. To demonstrate the applicability of NIR field spectroscopy for quantitative analysis of minerals, a specific example on the quantification of lateritic bauxites will be presented. It has been shown that the application of Partial Least Squares regression analysis (PLS) to the NIR spectra can be used to quantify chemistry and mineralogy in a range of lateritic bauxites. Important, issues such as sampling, precision, repeatability, and replication which influence the results will be discussed.

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Suggestion of the Relative Elevation Analysis Methods for Conservation of Local Topography : Focused on Analysis Range (지역규모의 지형경관 보전을 위한 상대고도 분석 방법론 제안 : 분석범위 설정을 중심으로)

  • Song, Wonkyong
    • Journal of the Korean Society of Environmental Restoration Technology
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    • v.17 no.5
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    • pp.19-28
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    • 2014
  • Given the structure of Korean mountains, it is more appropriate to apply the relative elevation method than the absolute elevation method. However, so far there were not suitable quantitative methodologies to analyze relative elevation, these analytical concepts were difficult to be utilized in urban environmental planning. This study suggested three methods for analyzing relative elevation, and one method for setting the analytical scope of relative elevation by calculating terrain relief. The results showed that the procedure considering 500m radius of each point and standardizing to 30% of the 7th height ridge was the most effective method to extract the local topography. This methodology is the quantitative tool to be able to conserve local important hills and ridges, and apply to fields of urban environmental planning and ecological restoration, especially urban ecological network.

Development of Measurement System for Quantitative Measurement of Cantilever in Atomic Force Microscopy (원자간격 현미경의 캔틸레버의 정량적 특성평가를 위한 계측 시스템 개발)

  • Kweon, Hyun-Kyu;Nam, Ki-Ho
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.6 no.2
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    • pp.22-27
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    • 2007
  • In this study, the two methods of stiffness measurement(Spring constant) of cantilever were proposed for quantitative measurement in Atomic Force Microscopy(AFM). As the 1st method for the measurement of stiffness, the probe method, which is used in the measurement of the semiconductor mechanical and electrical properties, was applied to the measurement of the cantilever. Experiments by the probe method were performed finding the resistance value of cantilever. As the results, the resistance was measured differently along with the dimension and the thickness of cantilever that determined the stiffness(spring constant) of the lever. As the 2nd method, the vibration characteristics(Dunkerley expression) is used to obtain the stiffness of the complex structure which is combined by AFM cantilever and the standard cantilever. We measured the resonant frequency from the complex structure using the micro stages and stereo microscope. As the results, we confirmed that the vibration characteristics(Dunkerley expression) is effected the micro complex structure of AFM cantilever.

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A Convenient HPLC/ELSD Method for the Quantitative Analysis of Betaine in Lycium chinense

  • Lee, Sang-Myung;Park, Chae-Kyu;Cho, Byung-Goo;Cho, Kyoung-Shim;Min, Byung-Sun;Bae, Ki-Hwan
    • Natural Product Sciences
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    • v.17 no.2
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    • pp.104-107
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    • 2011
  • In order to facilitate the quality control of betaine from the fruits of Lycium chinense, we have developed a rapid and simple method for quantitative determination. Determination was achieved on a Discovery C18 column with an isocratic solvent system of 0.32% perfluoropentanoic acid aqueous-acetonitrile at a flow-rate of 0.5 mL/min and detected an ELSD. The method was reproducible with intra- and inter-day variations of less than 6% (R.S.D). The recoveries were in the range of 90.01~100.05%. The method turned out to be fast and simple, furthermore, to have a good selectivity and sensitivity for the quantity determination of betaine in the fruits of L.chinense.

A Novel Unweighted Combination Method for Business Failure Prediction Using Soft Set

  • Xu, Wei;Yang, Daoli
    • Journal of Information Processing Systems
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    • v.15 no.6
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    • pp.1489-1502
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    • 2019
  • This work introduces a novel unweighted combination method (UCSS) for business failure perdition (BFP). With considering features of BFP in the age of big data, UCSS integrates the quantitative and qualitative analysis by utilizing soft set theory (SS). We adopt the conventional expert system (ES) as the basic qualitative classifier, the logistic regression model (LR) and the support vector machine (SVM) as basic quantitative classifiers. Unlike other traditional combination methods, we employ soft set theory to integrate the results of each basic classifier without weighting. In this way, UCSS inherits the advantages of ES, LR, SVM, and SS. To verify the performance of UCSS, it is applied to real datasets. We adopt ES, LR, SVM, combination models utilizing the equal weight approach (CMEW), neural network algorithm (CMNN), rough set and D-S evidence theory (CMRD), and the receiver operating characteristic curve (ROC) and SS (CFBSS) as benchmarks. The superior performance of UCSS has been verified by the empirical experiments.

Development of Measurement Method of Musculoskeletal Load for Construction Workers using Wearable Motion Recognition Sensor (웨어러블 장비를 이용한 건설 근로자 근골격계 부하 측정방안 제시)

  • Pyo, Ki-Youn;Lee, Dong-Min;Cho, Hun-Hee;Kang, Kyung-In
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2019.05a
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    • pp.123-124
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    • 2019
  • In the labor-intensive construction site, potential threats of the musculoskeletal diseases mainly caused by various repetitive physical tasks, vulnerable environment, and the aging of the labor worker exist. However, quantitative measuring method of construction labor worker's work posture has not been improved yet. This study proposed musculoskeletal measuring method by using wearable motion recognition sensor for quantitative evaluation and analysis of working posture of construction workers. This method is expected to be used as a basic data for posture analysis and prevention construction safety accidents, as well as physical workload and labor productivity analysis by labor work type.

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