• Title/Summary/Keyword: Pretreatment method

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Growth of Carbon Nanotubes by Microwave Plasma Enhanced Chemical Vapor Deposition (마이크로웨이브 플라즈마 화학기상증착법에 의한 탄소나노튜브의 성장특성)

  • Choi Sung-Hun;Lee Jae-Hyeoung
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.19 no.6
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    • pp.501-506
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    • 2006
  • Carbon nanotubes (CNTs) were grown with a microwave plasma enhanced chemical vapor deposition (MPECVD) method, which has been regarded as one of the most promising candidates for the synthesis of CNTs due to the vertical alignment, the low temperature and the large area growth. MPECVD used methane ($CH_4$) and hydrogen ($H_2$) gas for the growth of CNTs. 10 nm thick Ni catalytic layer were deposited on the Ti coated Si substrate by RF magnetron sputtering method. In this work, the pretreatment was that the Ni catalytic layer in different microwave power (600, 700, and 800 W). After that, CNTs deposited on different pressures (8, 12, 16, and 24 Torr) and grown same microwave power (800 W). SEM (Scanning electron microscopy) images showed Ni catalytic layer diameter and density variations were dependent with their pretreatment conditions. Raman spectroscopy of CNTs shows that $I_D/I_G$ ratios and G-peak positions vary with pretreatment conditions.

A Study on the Analysis of Cation in Blood by Ion Chromatography (Ion Chromatography에 의한 혈액중에서 양이온의 분석에 관한 연구)

  • 박성우;김을환
    • Journal of Environmental Health Sciences
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    • v.17 no.1
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    • pp.89-94
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    • 1991
  • There are many pretreatment and detection methods for divalent cations in blood. But our purpose was to study the pretreatment of blood for the determination of cations by Ion Chromatography. We compared with recovery of Mg$^{++}$, and Ca$^{++}$ contained in plasma according to four pretreatment methods, that is, add of trichloroacetic acid and perchloric acid, dilution with distilled water and membrane filter method. As a result, add of trichloroacetic acid was found to be the most suitable method for good recovery of Mg$^{++}$ (98.0%) and Ca$^{++}$(96.0%) in plasma, and the Mg$^{++}$ and Ca$^{++}$ contents in plasma was 20 and 102 ($\mu$g/ml)

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A comparative measurement study of Pb, Cd using ICP-AES with different pretreatment methods (ICP-AES를 이용한 전처리방법에 따른 환경시료내 Pb, Cd의 측정 비교 연구)

  • 권태영;윤춘경;전지홍
    • Proceedings of the Korean Society of Agricultural Engineers Conference
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    • 1998.10a
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    • pp.513-520
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    • 1998
  • The evaluation of uncertainty in environmental elemental analysis can be difficult because of the wide variety of analytical sample and objectives. for the specification of measured, elemetal analysis need certain method and high pretreatment technique. The sample of Pb, Cd in paddy soil and sewage sludge were analyzed by same ICP-AES, but each using four different pretreatment technique ; 0.1N HCl extraction, AB-DTPA extraction and two Mixture Acid Digestion. The four technique gave comparable results for the analysis of lead and cadmium. Concentrations determined by Mixture Acid Digestion were more higher than those by 0.1NHCI extraction and AB-DTPA extraction.

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Optimization of Lipase Pretreatment Prior to Lipase Immobilization to Prevent Loss of Activity

  • Lee, Dong-Hwan;Kim, Jung-Mo;Shin, Hyun-Yong;Kim, Seung-Woo
    • Journal of Microbiology and Biotechnology
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    • v.17 no.4
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    • pp.650-654
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    • 2007
  • In our previous work, a method of pretreating lipase was developed to prevent loss of its activity during covalent immobilization. In this study, Rhizopus oryzae lipase was pretreated before immobilization and then immobilized on a silica gel surface. The effects of the various materials and conditions used in the pretreatment stage on the activity of immobilized lipase were investigated. Immobilized lipase pretreated with 0.1% of soybean oil had better activity than those pretreated with other materials. The optimal temperature, agitation speed, and pretreating time for lipase pretreatment were determined to be $40^{\circ}C$, 200rpm, and 45min, respectively. The activity of immobilized soybean oil pretreated lipase was 630U/g matrix, which is 20 times higher than that of immobilized non-pretreated lipase. In addition, immobilized lipase activity was maintained at levels exceeding 90% of its original activity after 10 reuses.

Cost comparison of pretreatment processes in large SWRO desalination plant (대규모 해수담수화 플랜트에서의 전처리공정 비용 분석)

  • Kim, Youngmin;Kim, Jin-Ho;Lee, Sangho;Lee, Chang-Kyu;Park, Kwang Duk;Choi, June-Seok
    • Journal of Korean Society of Water and Wastewater
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    • v.27 no.5
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    • pp.555-560
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    • 2013
  • A cost analysis method for pretreament processes of a large scale seawater desalination plant was considered using a cost estimation model, WaTER (Water Treatment Estimation Routine). This model is based on cost functions of U.S. EPA to conduct economic analysis of water treatment facilities. A virtual seawater desalination plant which has pretreatment production capacity of $100,000m^3$ per day was chosen as a model plant. Dual media filtration and microfiltration systems were compared as pretreatment process, and the following reverse osmosis process was modeled. As a result, microfiltration showed a price competitiveness in condition of operating with reverse osmosis process by reducing the loads of water treatment and membrane cleaning despite it's high annual cost.

Effect of Applying Pretreatment Methods before cooking for decreasing the Microbiological Hazard of Cooked Dried fish in Foodservice establishments (건어물을 이용한 조리음식의 미생물학적 위해 감소를 위한 조리 전처리 적용 효과)

  • 배현주;이재학;오세인
    • Korean journal of food and cookery science
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    • v.19 no.5
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    • pp.555-561
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    • 2003
  • The purpose of this study was to analyze the microbiological hazards of dried fish (Jwieochae, Ojingeochae and Bugeochae), and to apply pretreatment methods to increase the safety of cooked dried fish within foodservice establishments. Microbiological inspections were conducted on Total Plate Count, Coliforms, E. coli, E. coli O157:H7, Staphylococcus aureus, Salmonella spp. and Listeria monocytogenes. The study results are summarized as follows. According to the Hazard analysis, there are many problems showing high numbers in terms of Total Plate Count and Coliforms, which were both well over acceptable standard levels. E. coli and Staphylococcus aureus were detected at certain foodservice establishments, while E. coli O157:H7, Salmonella spp. and Listeria monocytogenes were not detected at all. By applying various pretreatment methods, such as washing, blanching, pan frying and microwave heating, the levels of microbiological hazards were able to be controlled and lowered. Blanching was the most effective method, followed by panfrying, microwave heating and washing. The Total Plate Counts gradually decreased with increasing number of times washed and seconds panfried. From these results, it is concluded that to guarantee food safety, cooked dried fish raw materials should be kept hygienically and appropriate pretreatment methods applied before cooking.

Dyeing Properties of Bacterial Cellulose Fabric using Gardenia Jasminoides, Green Tea, and Pomegranate Peel, and the Effects of Protein Pretreatment (치자, 녹차, 석류껍질을 활용한 박테리아 셀룰로오스 섬유소재의 염색성과 단백질 전처리의 영향)

  • Yerim Hwang;Hyunjin Kim;Hye Rim Kim
    • Journal of the Korean Society of Clothing and Textiles
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    • v.48 no.3
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    • pp.511-527
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    • 2024
  • The aim of this study was to impart color to bacterial cellulose (BC) fabric using various natural plant-based dyes-namely, gardenia jasminoides, green tea, and pomegranate peel. A protein pretreatment was also applied to improve the BC fabric's dyeability and mechanical properties. The BC fabric's dyeing and mordanting conditions when using plant-based natural dyes were determined by changes in the K/S values. The dyeability of BC samples dyed with green tea or pomegranate peel improved when they were pretreated with soy protein isolate (SPI) prior to dyeing. Moreover, the SPI pretreatment was efficient in improving the BC fabric's tensile strength and flexibility. This study proposes a method for dyeing BC fabric that uses plant-based natural dyes and confirms the effects of the protein pretreatment on the fabric's dyeability and durability.

Effect of SAA Pretreatment on SSF at Low Temperature to Bioethanol Production from Rice Straw (암모니아수 침지 전처리 공정을 이용한 볏짚의 저온 동시당화발효)

  • Jang, Suh Yoon;Kim, Jun Seok
    • Korean Chemical Engineering Research
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    • v.52 no.4
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    • pp.430-435
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    • 2014
  • Physical and chemical barriers, caused by the close association of the main components of cellulosic biomass, hinder the hydrolysis of cellulose to fermentable sugars. Since the main goal of pretreatment is to increase the enzyme accessibility improving digestibility of cellulose, development of an effective pretreatment process has been considered to be important. In this study, SAA (Soaking in Aqueous Ammonia) was chosen as pretreatment because this is the simple and low-cost method. Rice straw of which the production is outstandingly high in domestic agriculture residues in Korea was chosen as raw material. SSA pretreatment with various reaction time of 3 h to 72 h was tested. The enzymatic hydrolysis and SSF (Simultaneous Saccharification and Fermentation) were performed at three different temperature (30, 40 and $50^{\circ}C$) to investigate performance of SSF upon various pretreatment conditions. As a result, this SAA treated-rice straw was found to have great potential for effective enzymatic hydrolysis and SSF with lower enzyme dosage at lower temperature ($30^{\circ}C$) than its conventional SSF. In SAA addition, SAA reduced fermentation time to 24 h owing to increase the initial hydrolysis rate substantially.

Computed tomography evaluation and pretreatment for a safe nasotracheal intubation, avoiding nasal cavity injuries (Nasotracheal intubation시 비강 내 외상을 줄이기 위한 술전 computed tomography를 이용한 평가 및 전처지)

  • Kim, Han-Lim;Yun, Kyoung-In;Kim, Kyung-Soo;Kang, Hyun;Choi, Young-Jun
    • Journal of the Korean Association of Oral and Maxillofacial Surgeons
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    • v.36 no.3
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    • pp.197-201
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    • 2010
  • Introduction: In a surgery of the oral cavity, nasotracheal intubation is often carried out to secure the surgical field. By passing a tracheal tube through the nasal cavity to the pharynx, the nasotracheal intubation can lead to complications that do not occur with oral intubation, such as nasal bleeding and submucosal aberration etc. The purpose of this study is to examine the method of CT evaluation and pretreatment for a safe nasotracheal intubation. Materials and Methods: Among 30 patients who orthognathic surgery was performed at Chung-Ang University Hospital during the period August 2009 to October 2009, 30 patients were included. The 30 patients were divided into two groups; 15 patients intubated with CT evaluation with pretreatment, and the other 15 patients intubated with no pretreatment. We evaluated nasal bleeding of the two groups during nasotracheal intubation. Results: CT evaluation with pretreatment group had a significantly lower incidence of nasal bleeding than the group with no pretreatment. Conclusion: CT evaluation with pretreatment helps to minimize nasal bleeding during nasotracheal intubation.

The Effect of Extrusion Treatment on Aqueous Ammonia Soaking Method in Miscanthus Biomass Pretreatment (억새 바이오매스 전처리에서 압출 처리가 액상 암모니아 침지 처리에 미치는 영향)

  • Bark, Surn-Teh;Koo, Bon-Cheol;Choi, Yong-Hwan;Moon, Youn-Ho;Ahn, Seung-Hyun;Cha, Young-Lok;Kim, Jung-Kon;An, Gi-Hong;Suh, Sae-Jung;Park, Don-Hee
    • New & Renewable Energy
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    • v.6 no.4
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    • pp.6-14
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    • 2010
  • Pretreatment of cellulosic biomass is necessary before enzymatic saccharification and fermentation. Extrusion is a well established process in food industries and it can be used as a physicochemical treatment method for cellulosic biomass. Aqueous ammonia soaking treatment at mild temperatures ranging from 60 to $80^{\circ}C$ for longer reaction times has been used to preserve most of the cellulose and hemicellulose in the biomass. The objective of this study was to evaluate the effect of extrusion treatment on aqueous ammonia soaking method. Extrusion was performed with miscanthus sample conditioned to 2mm of particle size and 20% of moisture content at $200^{\circ}C$ of barrel temperature and 175rpm of screw speed. And then aqueous ammonia soaking was performed with 15%(w/w) ammonia solution at $60^{\circ}C$ for 1, 2, 4, 8, 12 hours on the extruded and raw miscanthus samples respectively. In the combined extrusion-soaking treatment, most compositions removal occurred within 1~2 hours and on a basis of 1 hour soaking treatment values, cellulose was recovered about 85% and other compositions, including hemicellulose, are removed about 50% from extruded miscanthus sample. The combined extrusion-soaking treated and soaking only treated samples were subjected to enzymatic hydrolysis using cellulase and ${\beta}$-glucosidase. The enzymatic digestibility value of combined extrusion-2 hours soaking treated sample was comparable to 12 hours soaking only treated sample. It means that extrusion treatment can shorten the conventional long reaction time of aqueous ammonia soaking. The findings suggest that the combination of extrusion and soaking is a promising pretreatment method to solve both problems for no lignin removal of extrusion and long reaction time of aqueous ammonia soaking.