• 제목/요약/키워드: Pre-curing

검색결과 105건 처리시간 0.029초

국내 의료기기관리제도의 현황분석에 따른 정책적 제도개선 방안에 관한 연구 (A study on the system improvement policy according to the status analysis of medical device control system in Korea)

  • 이경만;백낙기;서종현
    • 대한안전경영과학회지
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    • 제12권3호
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    • pp.37-52
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    • 2010
  • This study is aimed at proposing the national policy for medical device control system in Korea as deeply analysed the present status of the system. On 1979, Korean government had started to inspect 24 kinds of the medical devices such as X-ray diagnostic equipments, medical sterilizer and etc. mostly imported from advanced countries which USA, Germany and Japan for the first time according to the Pharmaceutical Affairs Law. However medical devices were becoming consideration as an important partner of diagnosis, curing and alleviation of diseases by medical doctors and also much important keeping the health at home. Furthermore medical devices industry can be designated as a national growth engine industry. So it is necessary not only to harmonize to international standards but also the harmonization of the system including pre-market application and post-market surveillance, is strongly needed by the Korea Food and Drugs Administration(KFDA).

Study on Mechanical Properties Modification of Styrene Butadiene Rubber Composites Filling with Graphene and Molybdenum Disulfide

  • Xu, Li Xiang;Sohn, Mi Hyun;Kim, Yu Soo;Jeong, Ye Rin;Cho, Ur Ryong
    • 반도체디스플레이기술학회지
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    • 제18권3호
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    • pp.52-59
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    • 2019
  • Styrene-butadiene rubber (SBR) composites, incorporated with graphene, molybdenum disulfide and their hybrid in different filling ratio, were fabricated by a two roll-mill. The dispersion states of all the samples' matrix were employed by carbon black dispersion tester. The curing properties of the pre-vulcanized rubber composites were investigated, after molding by heating press machine, the tensile strength, storage modulus, friction coefficient, the swelling property had also been tested according to ASTM. The composite G1M10 (filling with 1 phr graphene and 10 phr molybdenum) showed the best mechanical properties and viscoelastic properties in this research with a better filler dispersion state and more compact matrix structure.

혼합 하중하에서의 고분자/거친금속 계면의 파손경로 (Failure Paths of Polymer/Roughened Metal Interfaces under Mixed-Mode Loading)

  • 이호영;김성룡
    • 한국재료학회지
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    • 제14권5호
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    • pp.322-327
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    • 2004
  • Copper-based leadframe sheets were oxidized in two kinds of hot alkaline solutions to form brown-oxide or black-oxide layer on the surface. The oxide coated leadframe sheets were molded with epoxy molding compound (EMC). After post mold curing, the oxide-coated EMC-leadframe joints were machined to form sandwiched Brazil-nut (SBN) specimens. The SBN specimens were used to measure the fracture toughness of the EMC/leadframe interfaces under mixed-mode (mode I + mode II) loading conditions. Fracture surfaces were analyzed by various equipment to investigate failure path. The results revealed that the failure paths were strongly dependent on the oxide type. In case of brown oxide, hackle-type failure was observed and failure path lay near the EMC/CuO interface with a little inclining to CuO at all case. On the other hand, in case of black oxide, quite different failure path was observed with respect to the distance from the tip of pre-crack and phase angle. Different failures occurred with oxide type is presumed to be due to the difference in microstructure of the oxides.

DEVELOPMENT AND APPLICATION OF SUBSTRUCTURE NON SUPPORTING FORMWORK FOR TOP-DOWN CONSTRUCTION

  • Mee-Ra Jeong;Hong-Chul Rhim;Doo-Hyun Kang;Kwang-Jun Yoo
    • 국제학술발표논문집
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    • The 3th International Conference on Construction Engineering and Project Management
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    • pp.788-793
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    • 2009
  • Constructing substructures by using Top-Down or Downward method needs an efficient formwork system because of difficulties in supporting concrete slabs from the bottom while excavation is in process. Existing underground formwork systems can be classified by three types: graded ground supported type (Slab On Grade, Beam On Grade), suspension type (Non Supporting Top Down Method), and bracket supported type (Bracket Supported R/C Downward). Each method has its own advantages and limits. Application of a specific formwork system for a given construction site is determined by various conditions and affect construction time and cost. This paper presents a newly developed underground non-supporting formwork system, which combines the advantages of a suspension type and a bracket supported type while it overcomes limits of two types. The developed system has a moving formwork which is supported by suspension cables hanging from the bracket placed at the top of pre-installed substructure columns. Then, the moving formwork is repeatedly lowered down for the next floor below to support concrete slab during curing. The details of this bracket and cable supported system have been investigated for the improvement of easiness in construction.

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Ethynyl 말단기를 갖는 Polyisoimide 올리고머의 합성 및 이들의 경화거동에 관한 연구 (Synthesis and Curing Behaviors of Polyisoimide Oligomers with Ethynyl End Groups)

  • 최석우;김보옥;김지흥;남성우;전붕수;김영준
    • 폴리머
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    • 제38권6호
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    • pp.774-781
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    • 2014
  • 4-ethynylaniline(4-EA) 혹은 4-phenylethynyl phthalic anhydride(4-PEPA)을 end-capper로 사용하여 분자량이 2500 g/mol 혹은 5000 g/mol로 조절되고, 반응성 ethynyl 기를 갖는 4,4'-diamino diphenyl ether(4,4'-ODA)/3,3',4,4'-benzophenone tetracarboxylic acid dianhydride(BTDA), 4,4'-ODA/4,4'-oxydiphthalic anhydride(ODPA)계 폴리아이소이미드 올리고머를 합성하여 이들의 중합 및 경화거동을 연구하였다. FTIR 분광분석을 통하여 이들 폴리아이소이미드 올리고머 말단에 반응성 ethynyl 기가 포함되어 있음을 확인할 수 있었다. 이미드화 반응은 폴리아이소이미드 올리고머의 화학구조에도 영향을 받을 뿐 아니라 올리고머의 분자량에도 영향을 받아 분자량 2500 g/mol 올리고머가 5000 g/mol 올리고머보다 대략 $10^{\circ}C$ 정도 낮은 온도에서 이미드화 반응이 일어났다. Ethynyl기의 가교반응은 이미드화 반응보다 높은 온도에서 일어났으며 4-EA로 end-cap된 폴리아이소이미드 올리고머에 대해서는 이 두 반응이 DSC 그래프에서 겹쳐서 나타났다. 4-PEPA로 end-cap된 4,4'-ODA/ODPA 폴리아이소이미드 올리고머에 대해 등 속도 가열 DSC 실험을 통해 이미드화 반응 및 가교반응에 대한 활성화 에너지와 지수앞인자를 구하였다. 이미드화 반응에 대한 활성화 에너지는 141 kJ/mol, 지수앞인자 값은 $1.45{\times}10^{13}min^{-1}$, 가교반응에 대한 활성화 에너지는 177 kJ/mol, 지수앞인자 값은 $2.90{\times}10^{13}min^{-1}$이 얻어졌다.

Glycidyltrimethylammonium Chloride(GTAC)를 이용한 양모 섬유 표면의 Silver Nanoparticle 부착 (Attachment of Silver Nanoparticles to the Wool Fiber Using Glycidyltrimethylammonium Chloride(GTAC))

  • 이승영;설인환;이재웅
    • 한국염색가공학회지
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    • 제28권2호
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    • pp.70-76
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    • 2016
  • Silver nanoparticles(AgNPs) were attached to wool fibers using glycidyltrimethylammonium chloride(GTAC), which is a type of quaternary ammonium salt. GTAC, which contains an epoxy functional group that, under high temperatures, generates a ring-opening reaction with wool fibers, which contain the amine group. Then, the AgNPs are attached to the surface of the GTAC-treated wool fibers by treatment with a silver colloidal solution. The process involves the following procedures: (1) The wool fibers are immersed in the GTAC solution, followed by pre-drying at $80^{\circ}C$ and curing at $180^{\circ}C$ to induce an alteration in the chemical structure; and (2) The wool fibers treated with GTAC are immersed in the silver colloid at $40^{\circ}C$ for 120 min to chemically induce a strong attachment of the AgNPs to the wool fibers. Scanning electron microscopy was used to analyze the influence of the concentrations of GTAC and the silver colloid, as well as the influence of the applied temperature of the silver colloid on the wool fibers, and the influence of the morphological changes in the wool fiber surfaces. As a result, the enhanced concentrations of GTAC and the silver colloid together with an elevated applied temperature of silver colloid have a tendency to increase in Ag atomic%.

성숙도 개념을 이용한 Whitetopping 포장의 현장 적용 (The Application of Maturity Method on Whitetopping Construction)

  • 정종석;조윤호;이강원
    • 한국도로학회논문집
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    • 제7권1호
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    • pp.83-92
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    • 2005
  • 성숙도는 비파괴시험으로 현장 콘크리트 강도를 시간과 온도의 함수로 추정하는 방법이다. 본 연구의 주목적은 실내실험에서 추정한 성숙도 곡선을 이용하여 whitetopping의 줄눈절삭과 교통개방의 시간을 결정하는 것이다. 또한 대기온도가 콘크리트 슬래브 온도와 성숙도에 미치는 영향을 평가하였고, 줄눈절삭과 교통개방시기를 결정하기 위해 성숙도 곡선을 개발하였다. i-button을 슬래브 내부에 설치하여 온도를 계측하였고, strain gauge를 이용하여 변위를 측정하였다. 실내실험에서 얻어진 성숙도 곡선을 이용하여 현장 압축강도를 예측한 결과, 현장 압축강도와 성숙도 곡선에서 예측된 압축강도와는 상당한 차이를 나타냈다. 이와 같은 결과는 현장의 양생조건, 대기온도, 풍속을 포함하는 여러 인자가 현장콘크리트 강도에 중요한 영향을 미치는 것으로 판단되었다. 여러 인자 중에서 대기온도의 변화에 따른 슬래브 온도와 성숙도 값에 미치는 영향을 평가한 결과, 대기온도는 슬래브 온도와 성숙도에 큰 영향을 미치는 것을 알 수 있었다. 특히 대기온도에 따른 성숙도 곡선의 기울기는 감소하였으며, 이는 대기온도가 감소함에 따라 성숙도 값이 급격히 감소하였다.

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건물의 3차원 구조체에 대한 전열해석 프로그램 개발 중 3차원 모델의 해석 오류 저감을 위한 사전 수정 방법 연구 (preprocessing methodology to reducing calculation errors in 3 dimensional model for development of heat transfer analysis program for 3 dimensional structure of building)

  • 이규성;이주희;이용준
    • KIEAE Journal
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    • 제16권1호
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    • pp.89-94
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    • 2016
  • This study is part of three-dimensional(3D) heat transfer analysis program developmental process. The program is being developed without it's own built in 3D-modeller. So 3D-model must be created from another 3D-modeller such as generic CAD programs and imported to the developed program. After that, according to the 3D-geometric data form imported model, 3D-mesh created for numerical calculation. But the 3D-model created from another 3D-modeller is likely to have errors in it's geometric data such as mismatch of position between vertexes or surfaces. these errors make it difficult to create 3D-mesh for calculation. These errors are must be detected and cured in the pre-process before creating 3D-mesh. So, in this study four kinds of filters and functions are developed and tested. Firstly, 'vertex error filter' is developed for detecting and curing for position data errors between vertexes. Secondly, 'normal vector error filter' is developed for errors of surface's normal vector in 3D-model. Thirdly, 'intersection filter' is developed for extracting and creating intersection surface between adjacent objects. fourthly, 'polygon-line filter' is developed for indicating outlines of object in 3D-model. the developed filters and functions were tested on several shapes of 3D-models. and confirmed applicability. these developed filters and functions will be applied to the developed program and tested and modified continuously for less errors and more accuracy.

Palfique Estelite의 경화전후 색조 변화에 관하여 (COLOR CHANGES OF PALFIQUE ESTELITE BETWEEN PRE AND POST IRRADIATIONS)

  • 유타가 요시마;하루히또 다까기;노리꼬 사이렌지;하루히또 이께다;다가시 구로다;히데오 오노세
    • 대한심미치과학회지
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    • 제6권1호
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    • pp.10-17
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    • 1997
  • It is pointed out that the color of composite resin is changing according to it's ploymerization and this color change is a harmful effect for the clinical satisfacion of composite resin restoration. The purpose of this study was to compare the changes of color of newly developed composite resins between before and after exposure of activating light. Five Compostie resins (8 shades) were employed: Palfique Estelite(UL, U, DY, G ; Tokuyama), Photo Clearfil A (US : Kuraray), Photo Clearfil Bright (US ; Kuraray), GC Graft LC(A3 ; GC), Silux Plus(U; 3M), Tristirnulus values of each material were determined before and after curing-light exposure by using a Micro Multi Photometer (MMP-1001, Nihon Denshoku Kogyo). The values were transformed into $L^*\;a^*\;b^*$ system and color changes of the resins were evaluated by the changes of $L^*$, $a^*$ and $b^*$ values for the individual shades. In addition, the effects of resin thickness and background color on color changes were also studied The finding were as follows: 1. Color changes of $L^*$, $a^*$ and $b^*$ values were recognized due to the light exposure for all products. The $b^*$ values of Palfique Estelite showed negligible changes for all shades. 2. The $b^*$ values were affected strongly by the background color, especially when decreasing the brightness on the background color.(Request original article reprints to Dr. Aoshima)

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Shear bond strength between CAD/CAM denture base resin and denture artificial teeth when bonded with resin cement

  • Han, Sang Yeon;Moon, Yun-Hee;Lee, Jonghyuk
    • The Journal of Advanced Prosthodontics
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    • 제12권5호
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    • pp.251-258
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    • 2020
  • PURPOSE. The bond strengths between resin denture teeth with various compositions and denture base resins including conventional and CAD/CAM purposed materials were evaluated to find influence of each material. MATERIALS AND METHODS. Cylindrical rods (6.0 mm diameter × 8.0 mm length) prepared from pre-polymerized CAD/CAM denture base resin blocks (PMMA Block-pink; Huge Dental Material, Vipi Block-Pink; Vipi Industria) were bonded to the basal surface of resin teeth from three different companies (VITA MFT®; VITA Zahnfabrik, Endura Posterio®; SHOFU Dental, Duracross Physio®; Nissin Dental Products Inc.) using resin cement (Super-Bond C&B; SUN MEDICAL). As a control group, rods from a conventional heat-polymerizing denture base resin (Vertex™ Rapid Simplified; Vertex-Dental B.V. Co.) were attached to the resin teeth using the conventional flasking and curing method. Furthermore, the effect of air abrasion was studied with the highly cross-linked resin teeth (VITA MFT®) groups. The shear bond strengths were measured, and then the fractured surfaces were examined to analyze the mode of failure. RESULTS. The shear bond strengths of the conventional heat-polymerizing PMMA denture resin group and the CAD/CAM denture base resin groups were similar. Air abrasion to VITA MFT® did not improve shear bond strengths. Interfacial failure was the dominant cause of failure for all specimens. CONCLUSION. Shear bond strengths of CAD/CAM denture base materials and resin denture teeth using resin cement are comparable to those of conventional methods.