• Title/Summary/Keyword: Pre-chamber

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Preparing Hydrophobic Mesoporous Silica as an Effective Pre-concentration Agent Under Humid Condition

  • Park, Eun Ji;Cho, Youn Kyoung;Jeong, Myung-Geun;Kim, Dae Han;Jeong, Bora;Yoon, Hye Soo;Seo, Hyun Ook;Kim, Young Dok
    • Proceedings of the Korean Vacuum Society Conference
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    • 2014.02a
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    • pp.159.1-159.1
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    • 2014
  • We report a simple method for preparing hydrophobic mesoporous silica and its use as a pre-concentrating agent of gas analytes. Hydrophobic mesoporous silica was prepared by coating PDMS (polydimethylsiloxane) thin layer on commercial mesoporous silica with thermal deposition method in a sealed chamber. By using this method, we were able to coat PDMS layer on inner-walls of pores larger than 15 nm. Also, contact angle measured on a surface consisting of PDMS-coated mesoporous silica exceeded $150^{\circ}$, implying that the surface has high water repellency. Pre-concentration ability of PDMS-coated mesoporous silica and baremesoporous silica was tested under dry and humid conditions. Adsorption and molecular desorption of gas analytes was much enhanced by PDMS-coating on mesoporous silica under both dry and humid conditions. Therefore we suggest that PDMS-coated mesoporous silica can be an efficient pre-concentration agent in order to enhance sensitivity of various detectors.

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Characteristic as a Resonance Frequency of $SF_6$ Gas (SF6 가스중의 공진주파수에 따른 신호특성)

  • Lee, Y.H.;Lee, H.D.;Park, J.N.;Shin, Y.S.;Park, J.S.;Seo, J.M.
    • Proceedings of the KIEE Conference
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    • 2003.07c
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    • pp.1867-1869
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    • 2003
  • In this paper, chamber(Circuit breaker compartment of C-GIS) made of stainless steel with 4 mm width is used. Artificial defect was made on enclosure or HV conductor of chamber and $SF_6$ gas was injected into it according to pressure. In this experiment, Acoustic emission sensors of different types was used to compare sensitivity to detect acoustic signal occurred by Partial discharge(PD) of according to types and resonance frequency in $SF_6$ gas atmosphere. Sensors used in tests was R6I, R15I and 2/4/6 Pre-Amplifier connected with R6IU without pre. amp. In case of R6IU, gain was adjusted with 40 dB like other sensors and operated by differential mode. Post amplifier(post. amp) and band pass filter(BPF) were developed Gain of post. amp. is 60 dB and BPF has band width of $50{\sim}300$ kHz. Also, envelope circuit developed reduces frequency of AE sensor. As a result, in $SF_6$ atmosphere, R6IU and R6I had resonance frequency of 60 Hz was better than R15I. Also, R6IU was better than R6I because of type property of pre.amp. had differential mode.

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Effect of Moisture in a Vacuum Chamber on the Deposition of c-BN Thin Film using an Unbalanced Magnetron Sputtering Method (비대칭 마그네트론 스퍼터링 방법에 의한 질화붕소막의 증착시 반응실내의 초기 수분이 입방정질화붕소 박막의 형성에 미치는 영향)

  • Lee, Eun-Sook;Park, Jong-Keuk;Lee, Wook-Seong;Seong, Tae-Yeon;Baik, Young-Joon
    • Journal of the Korean Ceramic Society
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    • v.49 no.6
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    • pp.620-624
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    • 2012
  • The role of moisture remaining inside the deposition chamber during the formation of the cubic boron nitride (c-BN) phase in BN film was investigated. BN films were deposited by an unbalanced magnetron sputtering (UBM) method. Single-crystal (001) Si wafers were used as substrates. A hexagonal boron nitride (h-BN) target was used as a sputter target which was connected to a 13.56 MHz radiofrequency electric power source at 400 W. The substrate was biased at -60 V using a 200 kHz high-frequency power supply. The deposition pressure was 0.27 Pa with a flow of Ar 18 sccm - $N_2$ 2 sccm mixed gas. The inside of the deposition chamber was maintained at a moisture level of 65% during the initial stage. The effects of the evacuation time, duration time of heating the substrate holder at $250^{\circ}C$ as well as the plasma treatment on the inside chamber wall on the formation of c-BN were studied. The effects of heating as well as the plasma treatment very effectively eliminated the moisture adsorbed on the chamber wall. A pre-deposition condition for the stable and repeatable deposition of c-BN is suggested.

Non-Contact Level on Air Levitation Table with Porous Chamber Array (다공성 패드를 갖는 챔버의 배열에 따른 공기 부상 테이블의 비접촉 부상 수준에 대한 연구)

  • Kim, Joon Hyun;Jeong, Young Suk;Lee, Tae Geol;Kim, Tae Hoon;Jung, Hyo Jae
    • Journal of the Korean Society of Manufacturing Technology Engineers
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    • v.22 no.6
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    • pp.913-920
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    • 2013
  • This paper presents an applicable basic design that can configure non-contact levitation table for conveying a large sheet of glass. The suggested air levitation table consists of a series of air chambers with porous pads and fans as the conveyor system. The air supply chambers are arrayed to supply an adequately strong upward airflow for supporting the glass. Levitation is controlled by the size and discharge velocity, of the chamber arrays, as well as the glass supporting height. After pre-evaluation of the glass rigidity and the filer functional performance, a one-way fluid structure interface (FSI) analysis is performed for predicting pressure and deflection working of the 8G glass in the transverse and longitudinal directions, respectively. After comparing calculated levels of flatness of the glass, it determines the chamber array for the linear non-contact conveying motion.

Arc Ion Plating Deposition System의 Bias 종류에 따른 TiN 박막의 특성평가

  • Kim, Wang-Ryeol;Park, Min-Seok;Kim, Dae-Yeong;Kim, Hyeon-Seung;Gwon, Min-Cheol
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.08a
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    • pp.208-208
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    • 2012
  • 최근 환경문제가 많이 제기되면서 친환경적 운송수단인 자전거 개발과 관련하여 다양한 기술개발이 이루어지고 있다. 그 중 고부가가치의 서스펜션 포크의 프레임에 고기능성 표면처리로 Arc ion plating deposition system (AIPDS)을 이용하여 부식, 내마모 특성이 뛰어난 TiN 박막을 증착시켰다. AIPDS는 기존의 arc system과 달리 다원계 소재 코팅 공정조건 확립을 위하여 chamber wall에 2개의 rectangular type sputter source를 장착하고 소재의 pre-treatment 용 linear type ion source를 설치하였다. 장비의 Chamber 중앙에는 pipe형 arc cathode를 설치하였으며, 그 주위를 anode 역할을 하는 copper 코일로 감아 이는 발생한 arc를 target인 cathode 축을 중심으로 방향성을 가지고 회전하여 진행 할 수 있도록 유도 하였다. 이 시스템에서 증착된 TiN 박막은 bias 전압 변화에 따른 박막의 구조 및 물성을 평가하였다. XRD 장비를 통하여 TiN 박막의 상분석을 진행하였고, 마모테스터, 원자현미경, 마이크로 비커스 경도기 등을 이용하여 기계적 특성을 평가하였다.

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Parametric Study on Combustion Characteristics of CNG Fuel (연소실 매개변수에 따른 천연가스 연소 특성)

  • Lee, Seang-Wock;Song, Young-Mo;Baik, Doo-Sung
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.32 no.7
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    • pp.513-517
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    • 2008
  • A parametric study was made to understand the fundamentals of combustion of CNG fuel in a constant volume chamber in the respect of swirl effect, and the numbers of spark ignition. Optical devices were applied for the visualization of the physics of combustion, and combustion pressures and exhaust emission were measured at several equivalence ratios by controlling speeds of a swirling motor. When the speed of a swirling motor was raised the combustion conditions were improved. The corresponding maximum combustion pressure and heat release rate were increased and the speed of flame propagation was getting faster. This research may contribute to improve the performance of CNG engine and reduce emissions in future.

An Investigation of HCCI Combustion Processes of Stratified Charge Mixture Using Rapid Compression Machine (급속압축 장치를 이용한 불균일 예혼합기가 HCCI연소에 미치는 영향에 관한 연구)

  • Lim, Ock-Taeck
    • Transactions of the Korean Society of Automotive Engineers
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    • v.17 no.3
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    • pp.8-14
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    • 2009
  • Effect of heterogeneity of combustion chamber has been thought as one of the way to avoid dramatically generating heat in HCCI Combustion. The purpose of this research is to investigate the effect of heterogeneity, especially thermal stratification and fuel strength stratification on HCCI Combustion fueled with DME and n-Butane. Thermal stratification is formed in Combustion Chamber of Rapid Compression Machine with 3 Kinds of pre-mixture has different properties. The stratified charge mixture is adiabatic compressed and on that process, in cylinder gas pressure and two-dimensional chemiluminescence images are measured and analyzed.

Micronization of water-soluble pharmaceuticals with a low-temperature Bubble Dryer

  • Seol , Eun-Young;Jung, Young-Hwan;Kim, Jung-In;Seo, Youn-Mi;Chung, Hye-Shin;Lee, Hee-Yong
    • Proceedings of the PSK Conference
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    • 2003.10b
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    • pp.236.3-237
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    • 2003
  • Fine particles of water-soluble pharmaceuticals were prepared using a new micronization method, Carbon Dioxide Assisted Nebulization in a Bubble Dryer(CAN-BD). The process utilized mixtures of CO$_2$ in aqueous solution at supercritical conditions to form an emulsion. The aerosols were dried with pre-heated nitrogen, and the drying chamber was operated at near atmospheric pressure. The dry particles were collected on membrane filter at the bottom of the drying chamber. Several processing parameters such as flow rate, temperature, pressure, solid concentration and processing scale were accessed using NaCl, human serum albumin, and granulocyte-colony stimulating factor as model pharmaceuticals. (omitted)

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The Characteristics of Pulverized Coal Combustion in the Two Stage Cyclone Combustor

  • Joo, Nahm-Roh;Kim, Ho-Young;Chung, Jin-Taek;Park, Sang-Il
    • Journal of Mechanical Science and Technology
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    • v.16 no.9
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    • pp.1112-1120
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    • 2002
  • Numerical investigations on air staging and fuel staging were carried out with a newly designed coaxial cyclone combustor, which uses the method of two stage coal combustion composed of pre-combustor and main combustor. The pre-combustor with a high air/fuel ratio is designed to supply gas at high temperature to the main combustor. To avoid local high temperature region in this process, secondary air is injected in the downstream. Together with the burned gas supplied from the pre-combustor and the preheated air directly injected into main combustor, coals supplied through the main burner react rapidly at a low air/fuel ratio. Strong swirling motion of cyclone combustor keeps the wall temperature high, which makes slagging combustion possible. Alaska, US coal is used for calculations. Predictions were made for various coal flow rates in the main combustor for fuel staging and for the various flow rate of secondary air in the pre-combustor for air staging. In-scattering angles are also chosen as a variable to increase residence times of coal particles. Temperature fields and particle trajectories for various conditions are described. Predicted temperature variations at the wall of the combustor are compared with corresponding experimental data and show a similar trend. The in-scattering angle of 20° is recommended to increase the combustion efficiency in the main chamber.

Determination of Optimal Storage Condition for Pre-packed Hanwoo Loin

  • Seol, Kuk-Hwan;Park, Tu San;Oh, Mi-Hwa;Park, Beom-Young;Cho, Seong In;Lee, Mooha
    • Food Science of Animal Resources
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    • v.33 no.3
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    • pp.390-394
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    • 2013
  • The aim of this study was to determine the optimal storage condition of pre-packed Hanwoo beef without freezing. Hanwoo loin was purchased from a local distributor at 48 h after slaughter, then sliced in $1.5{\pm}0.5$ cm thickness, and packed in a polyethylene (PE) tray covered with linear low-density polyethylene (LLDPE) film. The studied factors to set the optimal storage condition were chamber temperature (5, 2.5 and $-1^{\circ}C$ for 14 d), cooling method (direct and indirect cooling system), and ultraviolet (UV) light irradiation for beef surface sterilization (0, 30, 60, and 120 min). The changes of pH, thiobarbituric acid reactive substances (TBARS) and number of aerobic bacteria were measured during storage. Beef samples stored in $-1^{\circ}C$ showed the minimal increasing rate in TBARS and microbial growth. After 15 d of storage, there was no significant difference in pH and TBARS values. However, the microbial population of beef stored in direct type cooling chamber ($4.25{\pm}0.66$ Log CFU/g) was significantly lower than that of beef stored in indirect type chamber ($6.47{\pm}0.08$ Log CFU/g) (p<0.05). After 4 d of storage, 60 or 120 min UV light irradiated beef samples showed significantly lower microbial population, and at 14 d of storage, 60 min UV irradiated beef sample showed significantly lower microbial population ($3.14{\pm}0.43$ Log CFU/g) than control ($4.46{\pm}0.13$ Log CFU/g) (p<0.05). However, TBARS values of 60 or 120 min UV light irradiated beef samples were significantly higher than non-irradiated beef sample after 4 d of storage (p<0.05).