• Journal of Powder Materials
• /
• v.22 no.2
• /
• pp.87-92
• /
• 2015

Metallic porous materials have many interesting combinations of physical and geometrical properties with very low specific weight or high gas permeability. In this study, highly porous Cu foam is successfully fabricated by a slurry coating process. The Cu foam is fabricated specifically by changing the coating amount and the type of polyurethane foam used as a template. The processing parameters and pore characteristics are observed to identify the key parameters of the slurry coating process and the optimized morphological properties of the Cu foam. The pore characteristics of Cu foam are investigated by scanning electron micrographs and micro-CT analyzer, and air permeability of the Cu foam is measured by capillary flow porometer. We confirmed that the characteristics of Cu foam can be easily controlled in the slurry coating process by changing the microstructure, porosity, pore size, strut thickness, and the cell size. It can be considered that the fabricated Cu foams show tremendous promise for industrial application.

• Korean Journal of Materials Research
• /
• v.14 no.12
• /
• pp.857-862
• /
• 2004

Production of titanium powder directly from tantalum oxides ($TiO_2$) pellet through an electronically mediated reaction (EMR) by calciothermic reduction has been investigated. Feed material ($TiO_2\;pellet$) and reductant (Ca-Ni alloy) were charged into electronically isolated locations in a molten calcium chloride ($CaCl_2$) bath at $950^{\circ}C$. The current flow through an external circuit between the feed (cathode) and reductant (anode) locations was monitored during the reduction of $TiO_2$. The current approximately 3.2A was measured during the reaction in the external circuit connecting cathode and anode location. After the reduction experiment, pure titanium powder with low nickel content was obtained even though Ca-Ni alloy was used as a reductant. These results demonstrate that titanium powder can be produced without direct physical contact between the feed and reductant. In certain experimental conditions, pure titanium powder with approximately $99.5\;mass\%$ purity was successfully obtained.

• Proceedings of the Korean Institute of Building Construction Conference
• /
• 2003.05a
• /
• pp.23.2-29
• /
• 2003

As the bentonite is main material to prevent from collapse of drilling hole at underground excavation works, the quantity of bentonite is increasingly used on construction industry day by day. But, the discarded bentonite that is excessively used at underground excavation works causes various environmental trouble such as soil and water pollution etc. Therefore, this study aims to propose a foundamental report about pozzolan reaction of discarded Bentonite powder by heat-treatment and cooling as concrete mineral admixture. To find out the strength-development properties of mortar with discarded Bentonite powder by indirect cooling & cooling using of water after heat-treatment, the experiments such as flow test, and compressive strength test on curing age of mortar are excuted. As a result of this study, discarded Bentonite powder can be utilized as concrete mineral admixture by heat-treatment and especially, the strength-development properties of mortar mixing with discarded Bentonite powder is superior to the situation of $600^{\circ}C$.60min-cooling using of water.

• Journal of the Korean institute of surface engineering
• /
• v.49 no.6
• /
• pp.507-512
• /
• 2016

Expensive silver powder is used to form electrodes in most IT equipment, and recently, many attempts have been made to lower manufacturing costs by developing powders with Ag-Ni or Ag-Cu core-shell structures. This study examined the sintering behavior of Ag-Ni electrode powder with a core-shell structure for silicon solar cell with high energy efficiency. The electrode powder was found to have a surface similar to pure Ag powder, and cross-sectional analysis revealed that Ag was uniformly coated on Ni powder. Each electrode was formed by sintering in the range of $500^{\circ}C$ to $800^{\circ}C$, and the specimen sintered at $600^{\circ}C$ had the lowest sheet resistance of $5.5m{\Omega}/{\Box}$, which is about two times greater than that of pure Ag. The microstructures of electrodes formed at varying sintering temperatures were examined to determine why sheet resistance showed a minimum value at $600^{\circ}C$. The electrode formed at $600^{\circ}C$ had the best Ag connectivity, and thus provided a better path for the flow of electrons.

• Computers and Concrete
• /
• v.21 no.2
• /
• pp.111-116
• /
• 2018

Establishment of test methods to assess the fresh properties of self-compacting concrete (SCC) are required to ensure the homogeneity in fresh and hardened states. This paper discusses the suitability of a simple test method for assessing the slump flow and stability of SCC by testing on self-compacting mortar (SCM) fraction. The proposed test method aims at investigating slump flow diameter test and sieve stability test of SCC by testing SCM fraction with a plunger penetration apparatus. A central composite modeling design was performed to evaluate the effects of water/cement ratio (W/C), superplasticizer dosage (SP) and powder marble content (MP) on slump flow diameter, stability and plunger penetration test of fresh SCC. The responses of the derived statistical models are slump flow (Sf), sieve stability (S) and plunger penetration (P). Relationships obtained in this study show acceptable correlations between plunger penetration test value and slump flow diameter test results and stability. It should note that the developed relationships are very useful to predict slump flow diameter and stability of studied SCC mixtures by carrying out a simple plunger penetration test on its mortar, which can save labour and time in laboratory experiments.

• Proceedings of the Korea Concrete Institute Conference
• /
• 2001.05a
• /
• pp.263-268
• /
• 2001

In this study, the physical and mechanical characteristics of Bottom-ash exhausted from each of steam power plant was considered. The comparative objects were Bottom-ash in which a lot of powder contained and that in which less than that relatively contained. The difference in quantity of powder showed different effect on the character of flow. This study was undertaken on the use of Bottom-ash as a fine aggregate, and showed the optimum mixing and the character of flow according to each rate. And this study showed the quantity of water and binder added in different Bottom-ash was differently used.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.22 no.2
• /
• pp.444-450
• /
• 1998

In the present investigation, it is attempted to derive a yield function and associated flow rules of loose metal powders to predict plastic deformation and density change during compaction. The loose metal powders yield by shear stress as well as hydrostatic stress and the yield strength is much smaller in tension than compression. Therefore, a yield function for the powders is expressed as a shifted ellipse toward the negative direction in the hydrostatic stress axis in the space defined by the two stresses. Each of parameters A, B and .delta. used in the yield function is expressed as a function of relative density and it is determined by uniaxial strain and hydrostatic compressions using Cu powder. Flow rules obtained by imposing the normality rule to the yield function are applied to the analyses of unidirectional, bidirectional and hydrostatic compressions, resulting in an excellent agreement with experiments. The yield function is further examined by checking volume changes in plane stain, uniaxial strain and shear deformations.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.20 no.7
• /
• pp.2182-2195
• /
• 1996

Densification characteristics and behavior of tool steel powder compact during high temperature forming processes were investigated under pressure less sintering, sinter forging and hot isostastic pressing. In pressureless sintering, full density was obtained at a closely controlled temperature near the solidus of the material. Finite element calculations from constitutive model for densification by power law creep and diffusional flow were compared with experimental data. Agreements between theoretical calculations and experimental data were good in hot isostatic pressing but not as good in sinter forging.

• Journal of Powder Materials
• /
• v.10 no.6
• /
• pp.448-455
• /
• 2003

$TiO_2$ nanopowder has been synthesized by means of the flame method using a precursor of titanium tetraisopropoxide (TTIP, Ti$(OC_3H_7)_4)$. In order to clarify the effect of cooling rate of hot flame on the formation of $TiO_2$ crystalline phases, the flame was controlled by varying the mixing ratio and the flow rate of gases. Anatase phase was predominantly synthesized under the condition having the steep cooling gradient in flame, while a slow cooling gradient enabled to form almost rutile $TiO_2$ nanopowder of above 95%.

• Proceedings of the Korean Society for Technology of Plasticity Conference
• /
• 1999.03b
• /
• pp.129-130
• /
• 1999

The superplastic deformation characteristics is powder metallurgy(PM) Al-Li alloy has been studied within the framework of a recently proposed internal variable theory of superplasticity(SSP). The flow curves were obtained by performing a series of load relaxation tests at the temperature range from 45$0^{\circ}C$ to 52$0^{\circ}C$ It has been found that the overall flow curves were separated into the grain boundary sliding(GBS) and the accommodating dislocation glide processes/ The tensile curves were also obtained to clarify the superplastic deformation bahavior of PM Al-Li alloy. The microstructural features of PM AL-Li alloy have been examined through the transmission electron microscopy.