• Title/Summary/Keyword: Post-column

Search Result 290, Processing Time 0.018 seconds

Separation of Hg(II) by using the poly-NTOE(1, 12-diaza-3, 4:9, 10-dibenzo-5, 8-dioxacyclopentadeca-1, 12-ylene-2, 7-dihydroxyoctamethylene) in Liquid Chromatography (액체 크로마토그래피에서 Poly-NTOE(1, 12-diaza-3, 4:9, 10-dibenzo-5, 8-dioxacyclopentadeca-1, 12-ylene-2, 7-dihydroxyoctamethylene)를 이용한 Hg(II)의 분리)

  • Kim, Hae-Joong;Shin, Young-Kook;Kim, Si-Joong
    • Analytical Science and Technology
    • /
    • v.8 no.3
    • /
    • pp.259-264
    • /
    • 1995
  • The separation efficiency of metal ions by using the poly-NTOE(1, 12-diaza-3, 4:9, 10-dibenzo-5, 8-dioxacyclopentadeca-1, 12-ylene-2, 7-dihydroxyoctamethylene) has been determined by column chromatography in aqueous solution. Binding constants and separation factors for several poly-NTOE interactions were measured in aqueous solution. The order of these binding constants and separation factors with metal ions were Co(II)Zn(II) for the transition metal ions and Cd(II)

  • PDF

Low-Level Wind Shear (LLWS) Forecasts at Jeju International Airport using the KMAPP (고해상도 KMAPP 자료를 활용한 제주국제공항에서 저층 윈드시어 예측)

  • Min, Byunghoon;Kim, Yeon-Hee;Choi, Hee-Wook;Jeong, Hyeong-Se;Kim, Kyu-Rang;Kim, Seungbum
    • Atmosphere
    • /
    • v.30 no.3
    • /
    • pp.277-291
    • /
    • 2020
  • Low-level wind shear (LLWS) events on glide path at Jeju International Airport (CJU) are evaluated using the Aircraft Meteorological Data Relay (AMDAR) and Korea Meteorological Administration Post-Processing (KMAPP) with 100 m spatial resolution. LLWS that occurs in the complex terrains such as Mt. Halla on the Jeju Island affects directly aircraft approaching to and/or departing from the CJU. For this reason, accurate prediction of LLWS events is important in the CJU. Therefore, the use of high-resolution Numerical Weather Prediction (NWP)-based forecasts is necessary to cover and resolve these small-scale LLWS events. The LLWS forecasts based on the KMAPP along the glide paths heading to the CJU is developed and evaluated using the AMDAR observation data. The KMAPP-LLWS developed in this paper successfully detected the moderate-or-greater wind shear (strong than 5 knots per 100 feet) occurred on the glide paths at CJU. In particular, this wind shear prediction system showed better performance than conventional 1-D column-based wind shear forecast.

Validation study on numerical simulation of RC response to close-in blast with a fully coupled model

  • Gong, Shunfeng;Lu, Yong;Tu, Zhenguo;Jin, Weiliang
    • Structural Engineering and Mechanics
    • /
    • v.32 no.2
    • /
    • pp.283-300
    • /
    • 2009
  • The characteristic response of a structure to blast load may be divided into two distinctive phases, namely the direct blast response during which the shock wave effect and localized damage take place, and the post-blast phase whereby progressive collapse may occur. A reliable post-blast analysis depends on a sound understanding of the direct blast effect. Because of the complex loading environment and the stress wave effects, the analysis on the direct effect often necessitates a high fidelity numerical model with coupled fluid (air) and solid subdomains. In such a modelling framework, an appropriate representation of the blast load and the high nonlinearity of the material response is a key to a reliable outcome. This paper presents a series of calibration study on these two important modelling considerations in a coupled Eulerian-Lagrangian framework using a hydrocode. The calibration of the simulated blast load is carried out for both free air and internal explosions. The simulation of the extreme dynamic response of concrete components is achieved using an advanced concrete damage model in conjunction with an element erosion scheme. Validation simulations are conducted for two representative scenarios; one involves a concrete slab under internal blast, and the other with a RC column under air blast, with a particular focus on the simulation sensitivity to the mesh size and the erosion criterion.

Test and simulation of circular steel tube confined concrete (STCC) columns made of plain UHPC

  • Le, Phong T.;Le, An H.;Binglin, Lai
    • Structural Engineering and Mechanics
    • /
    • v.75 no.6
    • /
    • pp.643-657
    • /
    • 2020
  • This study presents experimental and numerical investigations on circular steel tube confined ultra high performance concrete (UHPC) columns under axial compression. The plain UHPC without fibers was designed to achieve a compressive strength ranged between 150 MPa and 200 MPa. Test results revealed that loading on only the UHPC core can generate a significant confinement effect for the UHPC core, thus leading to an increase in both strength and ductility of columns, and restricting the inherent brittleness of unconfined UHPC. All tested columns failed by shear plane failure of the UHPC core, this causes a softening stage in the axial load versus axial strain curves. In addition, an increase in the steel tube thickness or the confinement index was found to increase the strength and ductility enhancement and to reduce the magnitude of the loss of load capacity. Besides, steel tube with higher yield strength can improve the post-peak behavior. Based on the test results, the load contribution of the steel tube and the concrete core to the total load was examined. It was found that no significant confinement effect can be developed before the peak load, while the ductility of post-peak stage is mainly affected by the degree of the confinement effect. A finite element model (FEM) was also constructed in ABAQUS software to validate the test results. The effect of bond strength between the steel tube and the UHPC core was also investigated through the change of friction coefficient in FEM. Furthermore, the mechanism of circular steel tube confined UHPC columns was examined using the established FEM. Based on the results of FEM, the confining pressures along the height of each modeled column were shown. Furthermore, the interaction between the steel tube and the UHPC core was displayed through the slip length and shear stresses between two surfaces of two materials.

Median Filtering Detection of Digital Images Using Pixel Gradients

  • RHEE, Kang Hyeon
    • IEIE Transactions on Smart Processing and Computing
    • /
    • v.4 no.4
    • /
    • pp.195-201
    • /
    • 2015
  • For median filtering (MF) detection in altered digital images, this paper presents a new feature vector that is formed from autoregressive (AR) coefficients via an AR model of the gradients between the neighboring row and column lines in an image. Subsequently, the defined 10-D feature vector is trained in a support vector machine (SVM) for MF detection among forged images. The MF classification is compared to the median filter residual (MFR) scheme that had the same 10-D feature vector. In the experiment, three kinds of test items are area under receiver operating characteristic (ROC) curve (AUC), classification ratio, and minimal average decision error. The performance is excellent for unaltered (ORI) or once-altered images, such as $3{\times}3$ average filtering (AVE3), QF=90 JPEG (JPG90), 90% down, and 110% up to scale (DN0.9 and Up1.1) images, versus $3{\times}3$ and $5{\times}5$ median filtering (MF3 and MF5, respectively) and MF3 and MF5 composite images (MF35). When the forged image was post-altered with AVE3, DN0.9, UP1.1 and JPG70 after MF3, MF5 and MF35, the performance of the proposed scheme is lower than the MFR scheme. In particular, the feature vector in this paper has a superior classification ratio compared to AVE3. However, in the measured performances with unaltered, once-altered and post-altered images versus MF3, MF5 and MF35, the resultant AUC by 'sensitivity' (TP: true positive rate) and '1-specificity' (FN: false negative rate) is achieved closer to 1. Thus, it is confirmed that the grade evaluation of the proposed scheme can be rated as 'Excellent (A)'.

Collapse failure mechanism of subway station under mainshock-aftershocks in the soft area

  • Zhen-Dong Cui;Wen-Xiang Yan;Su-Yang Wang
    • Geomechanics and Engineering
    • /
    • v.36 no.3
    • /
    • pp.303-316
    • /
    • 2024
  • Seismic records are composed of mainshock and a series of aftershocks which often result in the incremental damage to underground structures and bring great challenges to the rescue of post-disaster and the repair of post-earthquake. In this paper, the repetition method was used to construct the mainshock-aftershocks sequence which was used as the input ground motion for the analysis of dynamic time history. Based on the Daikai station, the two-dimensional finite element model of soil-station was established to explore the failure process of station under different seismic precautionary intensities, and the concept of incremental damage of station was introduced to quantitatively analyze the damage condition of structure under the action of mainshock and two aftershocks. An arc rubber bearing was proposed for the shock absorption. With the arc rubber bearing, the mode of the traditional column end connection was changed from "fixed connection" to "hinged joint", and the ductility of the structure was significantly improved. The results show that the damage condition of the subway station is closely related to the magnitude of the mainshock. When the magnitude of the mainshock is low, the incremental damage to the structure caused by the subsequent aftershocks is little. When the magnitude of the mainshock is high, the subsequent aftershocks will cause serious incremental damage to the structure, and may even lead to the collapse of the station. The arc rubber bearing can reduce the damage to the station. The results can offer a reference for the seismic design of subway stations under the action of mainshock-aftershocks.

Analysis of selenoaminoacids and selenoproteins in blood serum of sows fed by selenium fortified feed (셀레늄강화 사료를 먹인 모돈 혈청에서의 셀레노아미노산 및 셀레노단백질 분석)

  • Park, Myungsoon;Lee, Sung Hoon;Pak, Yong-Nam
    • Analytical Science and Technology
    • /
    • v.28 no.3
    • /
    • pp.196-203
    • /
    • 2015
  • Selenium species (inorganic selenium, selenoaminoacids, and selenoproteins) were analyzed using anion exchange and affinity chromatography, which were connected to ICP/MS for the blood serum of sows fed by seleniumfortified feed. The Anion Exchange PRP X-100 column was used for the analysis of inorganic selenium (Se4+ and Se6+) and selenoaminoacids. The HEP column was used to separate SelP from GPx+SeAlb in selenoproteins. A quantitative analysis was performed using the post-column isotope dilution technique. The lactating sows were divided into three groups and fed by selenium fortified feed (organic 0.3 mg/kg, 0.6 mg/kg and inorganic 0.6 mg/kg) for four weeks. The test groups showed increases in selenoaminoacids compared with the control group, except the inorganic feed group. There was no significant difference between the organic feed groups. All test groups showed increases in selenoproteins. In particular, SelP showed a large increase that was 1.5 times higher than the other proteins.

A Study on the Structural Behavior and the Strength of Circular Hollow Steel(CHS) Section Columns (원형강관 기둥의 구조적인 거동 및 강도에 관한 연구)

  • Kang, Doo Won;Kwon, Young Bong
    • Journal of Korean Society of Steel Construction
    • /
    • v.21 no.5
    • /
    • pp.505-514
    • /
    • 2009
  • This paper describes the structural behavior and the ultimate strengths of circular hollow steel (CHS) sections based on a series of compression tests. The ultimate strengths of CHS section columns are mainly dependent on both diameter-thickness ratio and column slenderness ratio. For the CHS sections with a high diameter-thickness ratio, an elastic or an inelastic local buckling may occur prior to the overall buckling, and it may decrease the column strength. Test sections were fabricated from SM400 steel plate of 2.8 mm and 3.2 mm in thickness and were tested to failure. The diameter-thickness ratios of the test sections ranged from 45 to 170 to investigate the effect of local buckling on the column strength. The compression tests indicated that the CHS sections of lower diameter-thickness ratio than the yield limit in the current design specifications showed an inelastic local buckling and a significant post-buckling strength in the local mode. Their ultimate stresses were larger than the nominal yield stress. It was known that the allowable stresses of the sections predicted by the Korean Highway Bridge Design Specifications (2005) were too conservative in comparison with test results. The Direct Strength Method which was newly developed was calibrated for application to the CHS sections by the experimental and numerical results. The Direct Strength Method proposed can predict properly the ultimate strength of CHS section columns whether a local buckling and an overall buckling occur nearly simultaneously or not.

Estimation of Impurities from Commercially Available Glycyrrhizin Standards by the HPLC/ESI-MS (HPLC/ESI-MS에 의한 글리시리진 표준품의 불순물 추정)

  • Myung, Seung-Woon;Min, Hye-Ki;Kim, Myungsoo;Kim, Young Lim;Park, Seong-Soo;Cho, Jung Hee;Lee, Jong-Chul;Cho, Hyun-Woo;Kim, Taek-Jae
    • Analytical Science and Technology
    • /
    • v.13 no.4
    • /
    • pp.504-510
    • /
    • 2000
  • The impurity profiles from the raw materials of glycyrrhizin were performed by the high performance liquid chromatography (HPLC)/electrospray ionization (ESI)- mass spectrometry (MS). For the HPLC experiment, a $C_{18}$($3.9{\times}300mm$, $10{\mu}m$) column was used and the mobile phase was acetic acid/$H_2O$ (1:10):acetonitrile=3:2 with a flow rate of 0.8 ml/min. The effluent was splitted into the ratio of 50:1 and went into the ESI-MS. Three to six impurities were found and informed of the identification of the structure of the impurities by ESI-MS. And the structures of impurities were suggested to a hydroxy-glycyrrhizin which is added with hydroxy group (-OH) in the glycyrrhetic acid moiety and a reduced-glycyrrhizin which the position of 12 of the glycyrrhetic acid moiety is reduced. The purities of the standard materials were about 90%.

  • PDF

Development of a Special Program for Automatic Generation of Scoliotic Spine FE Model with a Normal Spine Model (정상 척추체 모델을 이용한 척추측만증 모델 자동 생성 프로그램 개발)

  • Ryu Han-Kyu;Kim Young-Eun
    • Journal of the Korean Society for Precision Engineering
    • /
    • v.23 no.3 s.180
    • /
    • pp.187-194
    • /
    • 2006
  • Unexpected postoperative changes, such as growth in rib hump and shoulder unbalance, have been occasionally reported after corrective surgery for scoliosis. However there has been neither experimental data fer explanation of these changes, nor the suggestion of optimal correction method. Therefore, the numerical study was designed to investigate the post-operative changes of vertebral rotation and rib cage deformation after the corrective surgery of scoliosis. A mathematical finite element model of normal spine including rib cage, sternum, both clavicles, and pelvis was developed with anatomical details. In this study, we also developed a special program which could convert a normal spine model to a desired scoliotic spine model automatically. A personalized skeletal deformity of scoliosis model was reconstructed with X-ray images of a scoliosis patient from the normal spine structures and rib cage model. The geometric mapping was performed by translating and rotating the spinal column with an amount analyzed from the digitized 12 built-in coordinate axes in each vertebral image. By utilizing this program, problems generated in mapping procedure such as facet joint overlapping, vertebral body deformity could be automatically resolved.