• Title/Summary/Keyword: Post-Heat treatment

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Microstructural changes of Al-Zn-Mg-Cu alloys containing Sc during hot extrusion and post heat treatments (Sc을 첨가한 Al-Zn-Mg-Cu 합금 압출재의 열처리에 따른 미세조직 변화)

  • 이혜경;서동우;이상용;이경환
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2003.10a
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    • pp.281-284
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    • 2003
  • The microstructural changes of Al-Zn-Mg-Cu alloy containing Sc during hot extrusion and post heat treatment is investigated. Two kinds of Al-Sc alloys with different alloying elements (B1, B2) are hot extruded to make I-shape bars at 380$^{\circ}C$, then the bars are solution treated at 480$^{\circ}C$ for 2hrs followed by artificial aging at 120$^{\circ}C$ for 24hrs. The interior microstructure of as extruded bar consists of elongated grains, however, fine equiaxed grains are mainly observed around surface. The microstructural gradient suggests that different restoration process can proceed during the hot extrusion. For B1 and B2, different grain growth behaviors are found around the surface during the post heat treatment. Rapid grain growth behavior around the surface is discussed related with the crystallographic orientation of the grain.

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Post-conditioning Periods and Seed Orientation Affects the Vigor of Cucurbit Seeds with Dry-heat Treatment (건열처리에 따른 박과채소종자의 활력 회복)

  • Choi, Byung-Soon;Lee, Jung-Myung;Choi, Geun-Won
    • Horticultural Science & Technology
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    • v.32 no.1
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    • pp.26-32
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    • 2014
  • We investigate the effect of post-conditioning periods and seed orientation on the vigor of cucurbit seeds with dry heat treatment (DHT). All the dry-heat treated seeds exhibited varying degree of seed vigor decreases. In general, pumpkin seeds showed less vigor decreases than the bottle gourd seeds. When the dry heat treated seeds were germinated after post-conditioning for 0, 30, and 120 days, the percentage of germination was enhanced by increasing the period of post-conditioning and the efficiency of post-conditioning differed by crop and cultivar. In both bottle gourd and pumpkin, the vigor of seeds placed in vertically upward and horizontal orientations was higher than that of the seeds placed in the vertically downward orientation. The results suggested that the vigor of dry-heat treated seeds could be improved by applying the proper post-conditioning and seed orientation.

Effect of the Ceragem Master Heat Bed for Posterior Neck Pain and Low Back Pain (항통 및 요배통 환자에서 세라젬 마스터 온열치료기의 효과)

  • Jang Jun-Hyuk;Kim Kyung-Ho;Kim Jang-Hyun
    • The Journal of Pediatrics of Korean Medicine
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    • v.14 no.2
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    • pp.133-140
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    • 2000
  • Purpose : Posterior Neck Pain and Back Pain are common diseases in human daily life. For reducting symptom and treatment of these diseases, many methods have been used and studied until now. The mechanisms of Ceragem Master Heat Bed(R)(Ceragem Co. Seoul, Korea) are infrared-heat therapy from natural nephrite and pressure therapy by up-down movement of natural nephrite ball. Through this study, authors would evaluate the clinical effectiveness of Ceragem Master Heat Bed(CMHB) on relieving posterior neck pain and back pain. Materials and methods : From 12-01-2000 to 01-13-2001, posterior neck pain and back pain patients were selected for experiment group(23patients) and control group(14patients). In both group, Visual Analog Scale(VAS) of pre-treatment stage is above 5 points. Experiment group were cared with acupuncture therapy, buhang therapy and CMHB. Control group were managed with only acupuncture therapy and buhang therapy. They were treated more than three times at least. At pre-treatment and post-treatment stage, we measured VAS for individual patients, and then compared effect of treatment in experiment group and in control group. Statistical analysis was preformed using SAS program. Results : In this study, a mean difference of VAS between pre-treatment and post-treatment stage was large in experiment(CMHB) group more than in control group(p〈0.01). Conclusion : Experiment(CMHB) group was more effective pain relief than control group in the treatment of posterior neck pain and back pain. CMHB was available for stimultaneous application of heat therapy and pressure massage together that gave another effects of mental stability and fatigue recovery. As the results of this study, CMHB could be used as a helpful treatment modality for posterior neck pain and back pain.

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Statistical Properties of Vickers Hardness of Post Weld Heat Treated Friction Welded Parts in Alloy718 (Alloy718 마찰용접 후열처리재의 비커스 경도의 통계적 성질)

  • Kong, Yu-Sik;Kwon, Hyeok-Yong;Kim, Seon-Jin
    • Journal of Ocean Engineering and Technology
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    • v.23 no.6
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    • pp.105-110
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    • 2009
  • The objective of this paper is to investigate the statistical properties of Vickers hardness (HV) for friction welded parts in a Ni-based super alloy (Alloy718). In the case of post weld heat treatment (PWHT) parts, hardness tests were repeated for three different applied loads, 100, 200, and 300 g, with a duration time of 10 seconds. The arithmetic means of the Vickers hardness in heat affected zone (HAZ) materials were smaller than those of the base metal (BM) in all of the applied loads. The coefficient of variation (COV) for the BM and HAZ decreased by increasing the applied load. The probability distribution of the Vickers hardness followed the Weibull distribution well. The distribution of the Vickers hardness was not found to be symmetric. The shape parameter and scale parameter increased by increasing the applied load at both the BM and HAZ.

The influence of post weld heat treatment on mechanical properties of stainless steel weldment (스테인리스강 용접부의 기계적 성질에 미치는 후열처리의 영향)

  • 한종만;한기형;이은배;허만주;한용섭
    • Journal of Welding and Joining
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    • v.14 no.3
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    • pp.75-85
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    • 1996
  • In this paper the influence of postweld heat treatment on mechanical properties of SMAW and FCAW stainless steel weldments was examined and the obtained results are as follows ; (1) The amount of $\delta$-ferrite formed by SMAW and FCAW process decreased with increasing holding temperature and time in post weld heat treatment(PWHT), and it was found that the reduced ferrite was transformed into sigma phase after $800^{circ}C{\times}50hr$ PWHT. This sigma phase, even though it was very small, resulted in brittleness of dissimilar weldment between carbon steel and stainless steel in bending test, however in similar weldment between stainless steel and stainless steel was not occured. (2) The chemical composition of sigma phase was measured to 28-30%Cr, 7-9%Mo, 4-6Ni in 316L weldment, and also 35-37%Cr, 0.9-1.0Mo, 6-8%Ni in 309L weldment by EDS analysis.

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Effects of Post Annealing on the Properties of ZnO:Al Films Deposited by RF-Sputtering (RF-Sputtering 법을 이용한 ZnO:Al 박막의 후 열처리에 따른 특성 변화)

  • Lee, Jae-Hyeong;Lee, Dong-Jin
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.9
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    • pp.789-794
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    • 2008
  • Zinc oxide (ZnO) has been widely studied for its practical applications such as transparent conduction electrodes for flat panel displays and solar cells. Especially, ZnO films show good chemical stability against hydrogen plasma, absence of toxicity, abundance in nature, and then suitable for photovoltaic applications. However, the fabrication process of thin film solar cells require a high substrate temperature and/or post heat treatment. Therefore, the layers have to withstand high temperatures, requiring an excellent stability without degrading their electronic and optical properties. In this paper, we investigated the stability of zinc oxide (ZnO) films doped with aluminum and hydrogen. Doped ZnO films were prepared by r.f. magnetron sputter and followed by heat treatment at different temperatures and for various times.

Study for Heat Treatment Optimization of Titanium Hollow Casted Billet (타이타늄 중공마더빌렛 주조재의 열처리공정 최적화 연구)

  • Youn, Chang-Suk;Park, Yang-Kyun;Lee, Hyung-Wook;Lee, Dong-Geun
    • Journal of the Korean Society for Heat Treatment
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    • v.32 no.2
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    • pp.68-73
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    • 2019
  • ${\alpha}$-titanium alloy has a relatively low heat treatment characteristic and it is mainly subjected to heat treatment for residual stress, recovery or dynamic recrystallization. In this study, commercially pure titanium hollow castings was fabricated by gravity casting. Heat treatments were carried out at $750^{\circ}C$, $850^{\circ}C$ and $950^{\circ}C$ to investigate the effect of post-heat treatment on microstructure and mechanical properties. Beta-transus temperature ($T_{\beta}$) was about $913^{\circ}C$, and equiaxed microstructure was shown at temperature below $T_{\beta}$ and lath-type microstructure at temperature above $T_{\beta}$. Microstructure and mechanical properties did not show any significant difference in the direction of solidification for titanium hollow billet, so it can be seen that it was a well-made material for extrusion process. The optimum heat treatment condition of hollow billet castings for the seamless tube production was $850^{\circ}C$, 4 hr, FC, indicating a combination of equiaxed microstructure and appropriate mechanical properties.

Evaluation of Microstructure and Mechanical Properties on Post-Weld Heat Treatment in the Heat Affected Zone of SA508 Gr.4N Ni-Mo-Cr Low Alloy Steel for Reactor Pressure Vessel (원자로압력용기용 SA508 Gr.4N Ni-Mo-Cr계 저합금강 용접열영향부의 용접후열처리에 따른 미세조직과 기계적 특성 평가)

  • Lee, Yoon-Sun;Kim, Min-Chul;Lee, Bong-Sang;Lee, Chang-Hee
    • Korean Journal of Metals and Materials
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    • v.47 no.3
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    • pp.139-146
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    • 2009
  • The heat-affected zone (HAZ) of SA508 Gr.4N Ni-Mo-Cr low alloy steel, which has higher Ni and Cr contents than SA508 Gr.3 Mn-Mo-Ni low alloy steel, was investigated on the microstructure and mechanical properties. The HAZ was categorized into seven characteristic zones (CGCG, FGCG, ICCG, SCCG, FGFG, ICIC and SCSC-HAZ) according to the peak temperature from the thermal cycle experienced during multi-pass welding. Post Weld Heat Treatment (PWHT) was conducted in the temperature range of $550{\sim}610^{\circ}C$ for 30 hours to evaluate the effect of PWHT conditions on the microstructure and mechanical properties. Before PWHT, CGHAZ and FGFGHAZ showed high yield strength (YS) ranging from 1000 to 1250 MPa, while YS of SCSCHAZ decreased from 607 MPa (observed for base metal) to 501 MPa. The Charpy impact energies of sub-HAZs fell below 100J at $-29^{\circ}C$, except in the SCSCHAZ. By applying PWHT to sub-HAZ specimens, YS decreased as the PWHT temperature increased. In the case of CGHAZs and FGFGHAZ heat-treated at $610^{\circ}C$, YS dropped drastically to the range of 654~686 MPa. From the Charpy impact test, the upper-shelf energy (USE) increased to approximately 250J and Index temperature ($T_{68J}$) decreased below $-50^{\circ}C$. Specifically, in FGFG, ICIC and SCSC-HAZ, $T_{68J}$ was below -110, which was lower than the case of base metal.

Effects of heat-treatment on the properties of ITO films on transparent polyimide substrates by RF magnetron sputtering (RF 마그네트론 스퍼터링법으로 투명 PI 기판에 증착된 ITO 박막의 특성에 미치는 열처리의 영향)

  • Kim, Hae-Chan;Cho, Hyun;Kim, Jin-Kon
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.30 no.1
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    • pp.12-16
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    • 2020
  • Indium tin oxide (ITO) films were prepared onto transparent polyimide (PI) substrates by RF magnetron sputtering at room temperature. The deposited ITO films were heat-treated at various temperatures (50, 100, 150, and 200℃). The effect of post heat-treatment temperature on structural, electrical and optical properties of ITO films were investigated. It was found that the as-deposited ITO films were amorphous and the degree of crystallinity and the grain size increased with an increasing heat-treatment temperature, which led to the increase in carrier concentration and mobility. The electrical resistivity of as-deposited ITO films was 2.73 × 10-3 Ω·cm. With the heat-treatment temperature increasing from 50 to 200℃, the electrical resistivity decreased from 2.93 × 10-3 to 1.21 × 10-4 Ω·cm. The average transmittance (400~800 nm) of the ITO deposited PI substrates was decreasing with post heat-treatment temperature and was above 81 % for the temperatures 50~150℃ and decreased considerably to 78 % at 200℃.

Effect of surface and heat treatment on the bond strength of veneering ceramics to zirconia(Y-TZP) (표면처리와 열처리가 전장도재와 지르코니아의 결합력에 미치는 영향)

  • Lee, Jung-Hwan;Ahn, Jae-Seok
    • Journal of Technologic Dentistry
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    • v.35 no.4
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    • pp.271-280
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    • 2013
  • Purpose: This study was to assess the effect of surface and heat treatment on the bond strength of veneering ceramics to zirconia. Methods: The specimens were divided into 7 groups according to surface treatment and heat treatment conditions prior to porcelain application. ten specimens from each group were subjected to a 3-point flexural test. In addition the influence of surface and heat treatment on surface roughness values and phase transformation of zirconia was evaluated. Statistical analysis was performed with one-way ANOVA and post hoc Tukey's test. Results: Bond strength ranged from $20.67{\pm}3.13MPa$ to $32.69{\pm}4.52$. Bond strength of surface treatment group was lower than that of control group but only $Al_2O_3$ sandblasting group was significant difference. Bond strength of heat treatment group was higher than that of surface treatment group but there was no statistical significance. Conclusion: Bond strength of veneering ceramics to zirconia was affected by surface and heat treatment.