• Title/Summary/Keyword: Post heat-treatment

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A Fatigue Toughness and Polymerization Shrinkage of Post-cure Heat Treated Composite Resins (광중합 복합레진에 대한 가열처리 피로내성 및 중합수축에 미치는 영향)

  • Oh, Won-Mann;Rhu, Sun-Youl;Son, Ho-Hyun;Okuda, Reiichi;Endo, Tastuo;Kudo, Yoshiyuki
    • Restorative Dentistry and Endodontics
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    • v.19 no.1
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    • pp.135-147
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    • 1994
  • This study was conducted to evaluate whether the fatigue toughness of visible light cured composite resins could be improved and how much percentage of polymerzation shrinkage could be affected by additional heat treatment. 7 materials were investigated for this study: P-50, Lite-fil CR inlay, Pekafil, Clearfil CR inlay, Clearfil photo posterior, Z -100 and Progress. Diametral tensile strengths and linear shrinkages of composite resins were taken under visible light cured and additional post-cure heated condition and compared each other. A fatigue toughness of above materials was evaluated by measuring diametral tensile strength after they were repeatedly loaded with 120kgf/$cm^2$ up to 3000 cycles. The results obtained were as follows : 1. When composite resins were cured just by visible light, Lite fil CR inlay, Z -100 and Progress showed respectively higher diametral tensile strength than the other materials. Clearfil CR inlay, Clearfil photo posterior and Progress exhibited strong fatigue toughness compared to P-50 and Pekafil. 2. Post-cure heat treated composite resins had higher diametral tensile strengths than visible light cured composite resins at fatigue toughness test as well as no fatigue toughness test. 3. When Composite resins were additionally polymerized by post-cure heat treatment, P-50 showed weak fatigue toughness, on the contrary, Clearfil CR inlay, Z-100, Progress showed strong one. 4. When composite resins were cured just by visible light, percentage of polymerization linear shrinkage was the lowerest in Clearfil CR inlay, followed by, in ascending order, Clearfil photo posterior, Lite-fil CR inlay, Progress, Pekafil, P-50, and Z-100. In the case of post- cure heat treated composite resins, percentage of linear shrinkage was the lowest in Clearfil photo posterior, followed by, in ascending order, Lite-til CR inlay, Clearfil CR inlay, Progress, P-50, Pekafil and Z-100. 5. Percentage of polymerization linear shrinkage was greater in the post-cure heat treated composite resins than in the visible light cured composite resins and linear shrinkage increased significantly in Pekafil, Clearfil CR inlay, and Clearfil photo posterior between at the visible light cured and at the post-cure heat treated condition. The above results is saying that additional post-cure heat treatment on the composite resins for posterior restoration is able to affect on improvement of strength and fatigue toughness and lead to increase polymerization of composite resins.

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Laser Hardening of Piston Ring Groove (피스톤 링그루브의 레이저 열처리)

  • Song, Y.K.;Suh, S.
    • Journal of the Korean Society for Heat Treatment
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    • v.10 no.3
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    • pp.165-171
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    • 1997
  • Laser hardening for the piston ring groove of ductile cast iron was tried. Mechanical and microstructural investigation for the hardened area indicated that the laser heating technique could replace conventional induction hardening process completely and further showed that post grinding process would be eliminated by minimizing bulging of heat treated area. In laser hardening, the volume increase caused by martensitic phase transformation proved to be less than $10{\mu}m$, which insures no post machining on the hardened surface. As expected, the depth of hardening was inversely proportional to the beam scanning velocity and the highest surface hardness was obtained at the beam velocity of 0.75m/min. Heat treatment using phosphate coating demonstrated quite comparable result to the case of graphite suscepter.

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Characterization of Live Fire Load in Buildings - Heat Release Characteristics of Typical Live Fire Load in Post Office Building - (건축물의 적재가연물 특성에 관한 연구 -우체국 적재가연물의 연소성상 -)

  • Nam, Dong-Gun;Yuji, Hasemi;SaKong, Seong-Ho;Jung, Jong-Jin
    • Proceedings of the Korea Institute of Fire Science and Engineering Conference
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    • 2008.04a
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    • pp.7-10
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    • 2008
  • Heat release characteristics of live fire load are an important parameter for performance oriented fire safety design of a building. While investigations have been carried out on the fire load and its burning behavior in office, residential and commercial buildings and so on, little effort has been paid for the rational treatment of fire load in post office buildings in Japan. In this report, burning behavior of typical combustible objects in post office buildings are studied by measuring heat release rates of plastic palettes with and without postal envelopes or packages and special containers loading numbers of palettes. The test results suggest that dynamic heat release rate is highly dependent on the condition of palettes especially if they load appropriate amount of postal envelopes or not.

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Effect of heat treatment and mechanical stress on the dielectic strength of epoxy resin (열처리 및 기계적응력이 Epoxy resin의 절연강도에 미치는 영향)

  • 신중홍;박정후;김영식
    • Journal of Advanced Marine Engineering and Technology
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    • v.8 no.2
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    • pp.81-87
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    • 1984
  • The effect of heat treatment and mechanical stress on the dielectic strength of epoxy resin film is studied. The film with 30-210 .mu.m thickness are casted at room temperature for 8 hours and post cured at the range of temperature 60-180 .deg. C, and the heat setting time are two kind, ie, 2 and 10 hours. The samples are made with Stycast 1266 that the primary compound is diglycidyl ether of bisphenol A, and the hardner is denaturated polyamines. Under no mechanical stresses, the maximum dielectric strength of the sample is obtained for the sample heat treated for 2 hours at 150 .deg. C. However, the best dielectric strength characteristics under compressive stress is obtained for the sample heat treated at 90 .deg. C and 120 .deg. C. The dielectric strength of the sample are also affected significantly by the cooling velocity of the sample after post heat setting at given temperature.

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The Effects of Post-Treatments for Wet Spun PVDF on the Piezoelectric Property (습식방사 된 PVDF 섬유의 후 처리를 통한 결정구조의 변화)

  • Yu, Seung Mi;Oh, Hyun Ju;Hwang, Sang-Kyun;Chung, Yong Sik;Hwang, Hui Yun;Kim, Seong Su
    • Composites Research
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    • v.26 no.2
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    • pp.123-128
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    • 2013
  • The PVDF (polyvinylidene fluoride) fibers were prepared using the wet spinning processing. To improve ${\beta}$-phase crystalline which closely related piezoelectric property PVDF wet spun fibers conducted post treatment. Post treatment is consisted of heat stretching and annealing process. The heat stretching and annealing conditions were controlled by changing temperature between glass transition temperature and melting temperature. From these experimental data, the resulting crystal structure of the ${\beta}$-phase crystalline was confirmed by FT-IR and XRD experiments. From these analysis results, optimum stretching and annealing conditions of the wet spun PVDF fibers were founded to increase high ${\beta}$-phase crystalline. Furthermore results showed that thermal processing had a direct effect on modifying the crystalline microstructure and also confirmed that heat stretching and annealing could increase the degree of crystallinity and ${\beta}$-phase crystalline. Finally, piezoelectric constant ($d_{11}$) of the post heat treated PVDF fibers reinforced composite were measured to investigate the feasibility for the sensing materials.

Effect of Post-Weld Heat Treatment on the Mechanical Properties and Microstructure of P-No. 1 Carbon Steels (P-No. 1 탄소강의 기계적 특성과 미세조직에 미치는 용접후열처리의 영향)

  • Lee, Seung-Gun;Kang, Yongjoon;Kim, Gi-Dong;Kang, Sung-Sik
    • Journal of Welding and Joining
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    • v.35 no.1
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    • pp.26-33
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    • 2017
  • This study aims to investigate the suitability of requirement for post-weld heat treatment(PWHT) temperature when different P-No. materials are welded, which is defined by ASME Sec. III Code. For SA-516 Gr. 60 and SA-106 Gr. B carbon steels that are typical P-No. 1 material, simulated heat treatment were conducted for 8 h at $610^{\circ}C$, $650^{\circ}C$, $690^{\circ}C$, and $730^{\circ}C$, last two temperature falls in the temperature of PWHT for P-No. 5A low-alloy steels. Tensile and Charpy impact tests were performed for the heat-treated specimens, and then microstructure was analyzed by optical microscopy and scanning electron microscopy with energy-dispersive spectrometry. The Charpy impact properties deteriorated significantly mainly due to a large amount of cementite precipitation when the temperature of simulated heat treatment was $730^{\circ}C$. Therefore, when dissimilar metal welding is carried out for P-No. 1 carbon steel and different P-No. low alloy steel, the PWHT temperature should be carefully selected to avoid significant deterioration of impact properties for P-No. 1 carbon steel.

A Study on the Effect of Pre-treatment on the Formation of Nitriding Layer by Post Plasma (포스트 플라즈마를 이용한 질화의 질화층 형성에 미치는 전처리의 영향에 대한 연구)

  • Moon, Kyoung Il;Byun, Sang Mo;Cho, Yong Ki;Kim, Sang Gweon;Kim, Sung Wan
    • Journal of the Korean Society for Heat Treatment
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    • v.18 no.1
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    • pp.24-28
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    • 2005
  • New post plasma nitriding can achieve a high uniformity that have been difficult in DC nitriding and have a high productivity comparable to gas nitriding. However, it has not a enough high nitriding potential for a rapid nitriding, because surface activation or ion etching in the general plasma nitriding cannot be expected. Thus, in this study, the effects of pre-treatments with oxidation and reduction gas have been investigated to improve the nitriding kinetics of post plasma nitriding. An effective pre-treatment consisting of oxidation and reduction resulted in the increase of surface energy of STD 11. This induced the surface hardness and the effective nitriding depth of STD 11. It is thought that the increase of the surface energy and the surface area with pre-treatment promote the nucleation of nitriding layer.

A Study on the Post-Weld Heat Treatment Effect Affecting Corrosion Behavior and Mechanical Property of Welding Part of RE36 Steel for Marine Structure (해양구조물용 RE36강 용접부의 부식거동 및 기계적 특성에 미치는 용접후 열처리 효과에 관한 연구)

  • 김성종;문경만
    • Journal of Welding and Joining
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    • v.19 no.1
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    • pp.65-74
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    • 2001
  • A study on the corrosion behavior in case of As-welded and PWHT temperature 55$0^{\circ}C$ of welding part of RE36 steel for marine structure was investigated with parameters such as micro-Vickers hardness, corrosion potential measurement of weld metal(WM), base metal(BM) and heat affected zone(HAZ), both Al anode generating current and Al anode weight loss quantity under sacrificial anode cathodic protection conditions. And also we carried out slow strain rate test(SSRT) in order to research both limiting cathodic polarization potential for hydrogen embrittlement and optimum cathodic protection potential as well as mechanical properties by post-weld heat treatment(PWHT) effect. Hardness of HAZ was the highest among three parts(WM, BM and HAZ) and the highest galvanic corrosion susceptibility was HAZ. And the optimum cathodic polarization potential showing the best mechanical properties by SSRT method was from -770mV to -875mV(SCE). In analysis of SEM fractography, applied cathodic potential from -770mV to -875mV(SCE) it appeared dimple pattern with ductile fracture while it showed transgranular pattern (Q. C : quasicleavage) under -900mV(SCE). However it is suggested that limiting cathodic polarization potential indicating hydrogen embrittlement was under -900mV(SCE).

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Effect of process type and heat treatment conditions on warm hydroformability (온간액압성형특성에 미치는 압출제조공정과 열처리 조건의 영향)

  • Yi, H.K.;Kwon, S.O.;Park, H.K.;Yim, H.S.;Lee, Y.S.;Moon, Y.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.10a
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    • pp.132-135
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    • 2007
  • In this study, hydroformability and mechanical properties of pre- and post- heat treated Al6061 tubes at different extrusion type were investigated. For the investigation, as-extruded, full annealed and T6-treated Al6061 tubes at different extrusion type were prepared. To evaluate the hydroformability, uni-axial tensile test and free bulge test were performed at room temperature and $250^{\circ}C$. Also mechanical properties of hydroformed part at various pre- and post-heat treatments were estimated by tensile test. And the tensile test specimens were obtained from hexagonal prototype hydroformed tube at $250^{\circ}C$. As for the heat treatment, hydroformability of full annealed tube is 25% higher than that of extruded tube. The tensile strength and elongation were more than 330MPa and 12%, respectively, when hydroformed part was post-T6 treated after hydroforming of pre- full annealed tube. However, hydroformed part using T6 pre treated tube represents high strength and low elongation, 8%. Therefore, the T6 treatment after hydroforming for as-extruded tube is cost-effective. Hydroformability of Al6061 tube showed similar value for both extrusion types. But flow stress of seam tube showed $20{\sim}50MPa$ lower value.

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The Effect of Heat Treatment on Biological Response and Mutation Frequency of Gamma Irradiated Rice Seeds (수도종자의 방사선조사에 있어서 열처리의 효과)

  • Chang-Yawl Harn;J. L.Won;Kwang-Tae Choi
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.10
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    • pp.45-50
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    • 1971
  • For the purpose of finding out the effect of heat treatment on biological response and mutation rate, rice seeds were heat treated before and after gamma irradiation. 1. At a dose of 20 KR, pre-irradiation heat treatment showed reduced biological damage and increased mutation rate as compared with non-heat treatment. 2. Mutation frequency was increased in post-treatment of heat shock than in pre-irradiation heat treatment and non-heat treatment. 3. Pre-irradiation heat treatment at 6$0^{\circ}C$ for 30 minutes markedly reduced the biological damage and increased the mutation rate. 4. Mutation spectrum in heat treatment was different from non-treatment.

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