• Proceedings of the KSME Conference
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• 2007.05b
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• pp.2142-2147
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• 2007

Experimental study was conducted to evaluate the performance of a miniature loop heat pipe (MLHP) with non-inverted meniscus type capillary structure. All parts of MLHP in this study were made of copper including the capillary structure and the distilled water was used as a working fluid of MLHP. The outer diameter of evaporator was 9 mm and its length was 119 mm. The effective pore size of the capillary structure was 30 micron and its porosity was 60%. The vapor transport line, the liquid transport line and the condenser were consisted of single 4.0 mm copper tube. The distance between the evaporator and the condenser region was 200 mm and the length of the loop was 969 mm. This MLHP was operated successfully at any orientation but the gravity highly influenced the thermal performance of the MLHP. The maximum thermal load was 130 watts at the bottom heat mode and the 20 watts at the top heat mode.

• Explosives and Blasting
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• v.29 no.2
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• pp.89-99
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• 2011

Recently on Jeju island there has been a lot of development and construction. However random distribution of porous basalt and clinker seam generated from volcanic activities often interrupt and greatly reduce efficiency of blasting necessary for construction. Three test blasts were operated to solve the inefficiency problem and results indicated that a powder factor of 0.40~0.45 $kg/cm^3$ is necessary to increase the efficiency of blasting. Also the blasting scheme should be concerned whether clinker seams exists in excavation levels or not.

• Proceedings of the Korea Concrete Institute Conference
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• 2001.05a
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• pp.935-940
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• 2001

This study search for absorbing sound and exhaust-gas which aims to manufacture continuous void by using clay and foam, the surface of materials is covered with $TiO_{2}$ powder as heat treatment. According to the results of the experiment, the increase of thickness of manufactured sound absorbing materials caused the increase of absorption rate in the range of low and middle sound and thus it can be an important factor of improving absorption rate. Sound absorbing materials could satisfy 70% of the average of sound absorption ratio in 7cm thickness. Also, the manufactured sound absorbing materials is covered with $TiO_{2}$ showed an excellency in the clarification of exhaust-gas under ultraviolet rays treatment when 70% of removal rate and about 10% of generation rate of $NO_{2}$ is settled by the flow of 2 $\ell$/min NO gas. Especially, manufactured sound absorbing materials could improve compressive strength of continuos porous concrete. in the case of 7% bubble addition, when the substitution rate of coagulator was 30% and 20%, compressive strength was 45kgf/$cm^{2}$ and 65kgf/$cm^{2}$ respectively. As the substitution rate of coagulator reducing, compressive strength increased after preforming burnt clay.

• New & Renewable Energy
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• v.3 no.1 s.9
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• pp.54-59
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• 2007

A sintering aid, $B_{2}O_{3}$ have been included into a $LiAlO_{2}$ electrolyte support by a tape casting method in order to reinforce mechanical strength of the support for molten carbonate fuel cells [MCFCs). Starting idea originates from the low melting point of $B_{2}O_{3}$ ($450^{\circ}C$), which can provide the low temperature consolidation of ceramic materials. The mechanical properties and the microstructure changes of the $B_{2}O_{3}$-included electrolyte support were examined by scanning electron microscope, mercury porosimetry, X-ray powder diffraction [XRD], high temperature differential scanning calorimeter and three-point bending strength measurement. The mechanical strength was clearly improved by addition of $B_{2}O_{3}$. The increase of mechanical strength results from the neck growth of a new $LiAlO_{2}$ phase between $LiAlO_{2}$ particles by the liquid phase sintering. Average pore size and porosity of the electrolyte support reinforced by addition of the sintering aid, $B_{2}O_{3}$, was $0.24{\mu}m$ and 59%, respectively which were suitable microstructure of a matrix for an application of MCFCs.

• Environmental Engineering Research
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• v.18 no.3
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• pp.163-168
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• 2013

In this study, an innovative media, iron mixed ceramic pellet (IMCP) has been developed for arsenic (As) removal from groundwater. A porous, solid-phase IMCP (2-3 mm) was manufactured by combining clay soil, rice bran, and Fe(0) powder at $600^{\circ}C$. Both the As(III) and As(V) adsorption characteristics of IMCP were studied in several batch experiments. Structural analysis of the IMCP was conducted using X-ray absorption fine structure (XAFS) analysis to understand the mechanism of As removal. The adsorption of As was found to be dependent on pH, and exhibited strong adsorption of both As(III) and As(V) at pH 5-7. The adsorption process was described to follow a pseudo-second-order reaction, and the adsorption rate of As(V) was greater than that of As(III). The adsorption data were fit well with both Freundlich and Langmuir isotherm models. The maximum adsorption capacities of As(III) and As(V) from the Langmuir isotherm were found to be 4.0 and 4.5 mg/g, respectively. Phosphorus in the water had an adverse effect on both As(III) and As(V) adsorption. Scanning electron microscopy results revealed that iron(III) oxides/hydroxides are aggregated on the surface of IMCP. XAFS analysis showed a partial oxidation of As(III) and adsorption of As(V) onto the iron oxide in the IMCP.

• Bulletin of the Korean Chemical Society
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• v.35 no.6
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• pp.1784-1788
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• 2014

The present study suggests a novel method to produce raspberry-like microparticles containing diverse functional materials inside. The raspberry-like microparticles were produced from a random assembly of uniformly-sized poly(methyl methacrylate) (PMMA) nanoparticles via electrospraying. The solution containing the PMMA nanoparticles were supplied through the inner nozzle and compressed air was emitted through the outer nozzle. The air supply helped fast evaporation of acetone, so it enabled copious amount of microparticles as dry powder. The microparticles were highly porous both on the surface and interiors, hence various materials with a function of UV-blocking ($TiO_2$ nanoparticles and methoxyphenyl triazine) or anti-aging (ethyl(4-(2,3-dihydro-1H-indene-5-carboxyamido) benzoate)) were loaded in large amount (17 wt % versus PMMA). The surface and interior structures of the microparticles were dependent on the characteristics of functional materials. The results clearly suggest that the process to prepare the raspberry-like microparticles can be an excellent approach to generate functional microstructures.

• Journal of the Korean Ceramic Society
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• v.48 no.6
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• pp.595-599
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• 2011

ALC(Autoclaved Lightweight Concrete) is produced using quartz sand, lime and cement and water. And aluminum powder is used for blowing agent. ALC is manufactured by autoclave chamber under high-temperature and high-pressure. Generally, ALC is 1/4 levels lighter than concrete and mortar, because it has a lot of pores. So density of ALC is about 0.45~0.65 g/$cm^3$. But, ALC has a weakness, typically low strength, with its porous structure. So, it is necessary to excellent strength properties for extensive apply of ALC materials in high porosity. In this study, melamine resin was used to improve the strength characteristics of ALC materials. We performed compressive and bending strength measurements. Compressive strength of ALC with 2% melamine resin increased 26.88% than 'melamine-free' ALC. Also we performed functionality evaluation such as thermal conductivity, sound absorption, and flame-resistance.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2003.04a
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• pp.155-159
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• 2003

The preparation and luminescence characterization of yttrium oxide doped with trivalent europium phosphors by sol-gel method have been investigated. Aqueous metal nitrate solution was mixed with EDTA which was chosen by the most suitable material of sol-gel formation one of appled various chelating agents. we noticed that the samples when are heated with EDTA at a temperature of $100^{\circ}C$ for 1hrs, produced brownish and crisp powders due to condensation reaction on decomposition, dehydration and formation of sol-gel. Hence, when the powder pre-heated was then heated at $1200^{\circ}C$ for 3hrs in atmosphere, the luminescence characterization of resultant $Y_{2}O_{3}:Eu^{3+}$ phosphor was enhanced upto maximum 30% significantly than conventional method through increasing porous region and decreasing particle sizes.

• Membrane and Water Treatment
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• v.7 no.6
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• pp.495-505
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• 2016

Mesoporous MCM-41 was deposited on an inexpensive disk shaped ceramic support through hydrothermal technique for ultrafiltration of $Fe^{3+}$ from aqueous solution. The ceramic support was fabricated using uni-axial compaction technique followed by sintering at $950^{\circ}C$. The characteristics of MCM-41 powder as well as the composite membrane were examined by X-ray diffraction (XRD), thermogravimetric analysis (TGA), field emission scanning electron microscope (FESEM), porosity and pure water permeation test. The XRD result revealed the good crystallinity and well-resolved hexagonally arranged pore geometry of MCM-41. TGA profile of synthesized MCM-41 zeolite displayed the three different stepwise mechanisms for the removal of organic template. The formation of MCM-41 on the porous support was verified by FESEM analysis. The characterization results clearly indicated that the accumulation of MCM-41 by repeated coating on the ceramic disk directs to reduce the porosity and pore size from 47% to 23% and 1.0 to $0.173{\mu}m$, respectively. Moreover, the potential of the fabricated MCM-41 membrane was investigated by ultrafiltration of $Fe^{3+}$ from aqueous stream at various influencing parameters such as applied pressure, initial feed concentration and pH of solution. The maximum rejection 85% was obtained at applied pressure of 276 kPa and the initial feed concentration of 250 ppm at pH 2.

• Preventive Nutrition and Food Science
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• v.20 no.2
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• pp.143-147
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• 2015

Systematic study of how different drying methods, namely hot-air drying, vacuum-drying, and freeze-drying, affect color, browning index, degree of rehydration, water solubility, and vitamin C content is critical for utilizing pine needle powders (PNP) as a novel ingredient in functional foods. Samples prepared by vacuum-drying showed a significantly higher $L^*$-value, whereas higher $a^*$- and $b^*$-values were detected in the hot-air dried samples (P<0.05). The browning index was significantly higher in samples prepared by vacuum-drying compared to samples prepared by freeze-drying (P<0.05). Freeze-dried PNP exhibited a significantly higher degree of rehydration than hot-air dried samples (P<0.05). Water solubilities of freeze-dried and hot-air dried samples were significantly higher than that of vacuum-dried sample (P<0.05). Vitamin C was less destroyed during freeze-drying compared to hot-air or vacuum-drying (P<0.05). Freeze-dried samples displayed a clear porous structure and appeared to have a bigger space, whereas hot-air dried samples showed lower porosity than vacuum and freeze-dried samples.