• Title/Summary/Keyword: Porosity.

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Effect of soldering techniques and gapdistance on tensile strength of soldered Ni-Cr alloy joint

  • Lee, Sang-Yeob;Lee, Jong-Hyuk
    • The Journal of Advanced Prosthodontics
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    • v.2 no.4
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    • pp.117-121
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    • 2010
  • PURPOSE. The present study was intended to evaluate the effect of soldering techniques with infrared ray and gas torch under different gap distances (0.3 mm and 0.5 mm) on the tensile strength and surface porosity formation in Ni-Cr base metal alloy. MATERIALS AND METHODS. Thirty five dumbbell shaped Ni-Cr alloy specimens were prepared and assigned to 5 groups according to the soldering method and the gap distance. For the soldering methods, gas torch (G group) and infrared ray (IR group) were compared and each group was subdivided by corresponding gap distance (0.3 mm: G3 and IR3, 0.5 mm: G5, IR5). Specimens of the experimental groups were sectioned in the middle with a diamond disk and embedded in solder blocks according to the predetermined distance. As a control group, 7 specimens were prepared without sectioning or soldering. After the soldering procedure, a tensile strength test was performed using universal testing machine at a crosshead speed 1 mm/min. The proportions of porosity on the fractured surface were calculated on the images acquired through the scanning electronic microscope. RESULTS. Every specimen of G3, G5, IR3 and IR5 was fractured on the solder joint area. However, there was no significant difference between the test groups (P > .05). There was a negative correlation between porosity formation and tensile strength in all the specimens in the test groups (P < .05). CONCLUSION. There was no significant difference in ultimate tensile strength of joints and porosity formations between the gas-oxygen torch soldering and infrared ray soldering technique or between the gap distance of 0.3 mm and 0.5 mm.

Influence of porosity distribution on vibration analysis of GPLs-reinforcement sectorial plate

  • Jia, Anqiang;Liu, Haiyan;Ren, Lijian;Yun, Yingxia;Tahouneh, Vahid
    • Steel and Composite Structures
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    • v.35 no.1
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    • pp.111-127
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    • 2020
  • The goal of this study is to fill this apparent gap in the area about investigating the effect of porosity distributions on vibrational behavior of FG sectorial plates resting on a two-parameter elastic foundation. The response of the elastic medium is formulated by the Winkler/Pasternak model. The internal pores and graphene platelets (GPLs) are distributed in the matrix either uniformly or non-uniformly according to three different patterns. The model is proposed with material parameters varying in the thickness of plate to achieve graded distributions in both porosity and nanofillers. The elastic modulus of the nanocomposite is obtained by using Halpin-Tsai micromechanics model. The annular sector plate is assumed to be simply supported in the radial edges while any arbitrary boundary conditions are applied to the other two circular edges including simply supported, clamped and free. The 2-D differential quadrature method as an efficient and accurate numerical approach is used to discretize the governing equations and to implement the boundary conditions. The convergence of the method is demonstrated and to validate the results, comparisons are made between the present results and those reported by well-known references for special cases treated before, have confirmed accuracy and efficiency of the present approach. It is observed that the maximum vibration frequency obtained in the case of symmetric porosity and GPL distribution, while the minimum vibration frequency is obtained using uniform porosity distribution. Results show that for better understanding of mechanical behavior of nanocomposite plates, it is crucial to consider porosities inside the material structure.

Effect of Porosity on the High-Cycle Fatigue Behavior of Al-Si-Mg Casting Alloy (Al-Si-Mg계 주조용 알루미늄 합금의 고주기 피로 거동에 미치는 기공의 영향)

  • Lee, Young-Jae;Kang, Won-Guk;Euh, Kwang-Jun;Cho, Kyu-Sang;Lee, Kee-Ahn
    • Transactions of Materials Processing
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    • v.18 no.4
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    • pp.296-303
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    • 2009
  • The effect of porosity on the high-cycle fatigue properties of Al-Si-Mg casting aluminum alloys was investigated in this study. Microstructure examination, tensile and high-cycle fatigue test were conducted on both Al-Si-Mg casted (F) and heat-treated (T6) conditions. Porosity characteristics on the fracture surfaces of fatigue-tested samples were examined using SEM and image analysis. The microstructure observation results showed that eutectic Si particles were homogeneously dispersed in the matrix of the Al-Si-Mg casting alloys, but there were porosities formed as cast defects. The high-cycle fatigue results indicated that the fatigue strength of the 356-T6 alloy was higher than that of the 356-F alloys because of the significant reduction in volume fraction of pores by heat treatment. The SEM fractography results showed that porosity affected detrimental effect on the fatigue life: 80% of all tested samples fractured as a result of porosity which acted as the main crack initiation site. It was found that fatigue life decreased as the size of the surface pore increased. A comparison was made between surface pore and inner pore for its effect on the fatigue behavior. The results showed that the fatigue strength with the inner pores was higher than that of the surface pore.

Fabrication of porous nickel membrane for high precision gas filter (극청정 가스필터용 다공성 니켈 멤브레인의 제조)

  • Song, Han-Bok;Yang, Jae-Kyo;Seong, Ki-Hun;Seo, Dong-Moon;Kang, Du-Hong;Choa, Yong-Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.17 no.5
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    • pp.210-216
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    • 2007
  • Porous nickel membrane far high precision gas filter was prepared by in-situ reduced/sintered process of NiO with an addition of polymer(PMMA; polymethyl methacrylate). It showed that the porosity of Ni membrane was approximately 52%. It is similar to metal membrane which prepared using metal fiber as raw materials. The average pore diameter and porosity of Ni membrane increased as content of added polymer and decreased as elevating reduced/sintered temperature from $800^{\circ}C$ to $1000^{\circ}C$. Increase of porosity at $800^{\circ}C$ was associated with surface diffusion mechanism that leads to initial sintering, while decrease of porosity at $1000^{\circ}C$ was associated with lattice diffusion and grain boundary diffusion.

A Study on the Characteristic of Gas Pore Formation in Lost Foam Casting of Mg alloy;Comparison with Al alloy (마그네슘 합금의 소실모형주조 시 기포형성 특성에 관한 연구;알루미늄 합금과 비교)

  • Shin, Seung-Ryoul;Han, Sang-Won;Lee, Kyong-Whoan
    • Journal of Korea Foundry Society
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    • v.24 no.3
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    • pp.165-174
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    • 2004
  • The pore formation characteristic of Mg alloy during Lost Foam Casting(LFC) was investigated with reduced pressure test and real casting, which was compared with the results of previous work for Al alloy. Cast Mg alloys in LFC had much lower porosities in comparison with those of Al alloys. Also, the proper pouring temperature gave the minimum porosity like Al alloy although it was higher than that of Al alloys due to the worse fluidity of Mg alloy. The pore formation mechanism of Mg alloy in LFC was similar to that of AI alloy but the critical temperature showing the different mechanism is higher than that of Al alloy as much as $30{\sim}50^{\circ}C$. The result that Mg alloy in LFC had the lower porosity comparing with Al alloy was due to the extra solubility of hydrogen gas although the solubility of Al alloy was easily exceeded by the external sources like pyrolyzed polystyrene products. The mold evacuation gave the lower porosity due to the removal of polystyrene pyrolysis products, and reduced shrinkage defects. Also, there was a proper evacuation pressure that gave a porosity of almost 0vol%. But much higher vacuum degree than this proper pressure caused the severe entrapment of polymer pyrolysis products that gave the large porosity.

Numerical Analysis on the Heat Transfer and Pressure Drop Characteristics of a Channel with Pin-fin Structure (핀-휜 구조물을 삽입한 채널의 열전달 특성과 압력강하에 관한 수치해석)

  • Heo, Joo-Nyoung;Kim, Ji-Hoon;Son, Young-Seok;Shin, Jee-Young
    • Journal of Advanced Marine Engineering and Technology
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    • v.35 no.2
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    • pp.224-231
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    • 2011
  • Heating and/or cooling of the channel with pin-fin structure is a promising choice for the efficient heat transfer. Complex pin-fin structure shows highly irregular behavior like porous media. This study shows the numerical analysis on the characteristic of heat transfer and pressure drop of a channel with pin-fin structure. It predicts the experimental data quite well at the high porosity region with large diameter. Low porosity activates the rigorous flow disturbance and, consequently, the enhanced heat transfer. However, the concept of optimum design should be carefully reviewed because the pressure drop is also increased with decreasing porosity at low porosity region.

Pharmaceutical Potential of Gelatin as a pH-responsive Porogen for Manufacturing Porous Poly(d,l-lactic-co-glycolic acid) Microspheres

  • Kim, Hyun-Uk;Park, Hong-Il;Lee, Ju-Ho;Lee, Eun-Seong;Oh, Kyung-Taek;Yoon, Jeong-Hyun;Park, Eun-Seok;Lee, Kang-Choon;Youn, Yu-Seok
    • Journal of Pharmaceutical Investigation
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    • v.40 no.4
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    • pp.245-250
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    • 2010
  • Porous poly(lactic-co-glycolic acid) microspheres (PLGA MS) have been utilized as an inhalation delivery system and a matrix scaffold system for tissue engineering. Here, gelatin (type A) is introduced as an extractable pH-responsive porogen, which is capable of controlling the porosity and pore size of PLGA microspheres. Porous PLGA microspheres were prepared by a water-in-oil-in-water ($w_1/o/w_2$) double emulsification/solvent evaporation method. The surface morphology of these microspheres was examined by varying pH (2.0~11.0) of water phases, using scanning electron microscopy (SEM). Also, their porosity and pore size were monitored by altering acidification time (1~5 h) using a phosphoric acid solution. Results showed that the pore-forming capability of gelatin was optimized at pH 5.0, and that the surface pore-formation was not significantly observed at pHs of < 4.0 or > 8.0. This was attributable to the balance between gel-formation by electrostatic repulsion and dissolution of gelatin. The appropriate time-selection between PLGA hardening and gelatin-washing out was considered as a second significant factor to control the porosity. Delaying the acidification time to ~5 h after emulsification was clearly effective to make pores in the microspheres. This finding suggests that the porosity and pore size of porous microspheres using gelatin can be significantly controlled depending on water phase pH and gelatin-removal time. The results obtained in this study would provide valuable pharmaceutical information to prepare porous PLGA MS, which is required to control the porosity.

Physical Properties of Grain (곡물(糓物)의 물리적(物理的) 특성(特性)에 관(關)한 연구(硏究))

  • Kim, Man Soo;Koh, Hak Kyun
    • Journal of Biosystems Engineering
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    • v.6 no.1
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    • pp.73-82
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    • 1981
  • The physical properties of grain are very important for the design of handling, sorting, processing, and storage system. On the physical properties of grain, volume, bulk density, true density, specific gravity, and porosity arc the major factors affecting the thermal properties of grain. This study was conducted to determine experimentally the above physical properties of rough rice (3 Japonica-type, 3 Indica-type) and barley (covered, naked) as a function of moisture content ranged from about 10% to 25% (w.b). The results of this study are summarized as follows; 1. The volume of grain kernel increased with moisture content for both rice and barley. The volume of those grain kernel was in the range of $2.2068{\times}10^{-8}{\sim}3.3960{\times}10^{-8}m^3$ at the moisture content of 14%. 2. The bulk density of rice increased linearly with moisture content for Japonica-type rough rice and quadratically for Indica-type rough rice, but the bulk density of barley decreased linearly with moisture content. The bulk density of the grain was in the range of 501.14~689.13kg/$m^3$ at the moisture content of 14%. 3. The true density of whole grain decreased linearly with moisture content, and was in the range of 1019.49~1139.75kg/$m^3$ at the moisture content of 14%. 4. The porosity of rice decreased linearly with moisture content for Japonica-type rough rice and quadratically for Indica-type rough rice, but the porosity of barley increased linearly with moisture content. The porosity of the grain was in the range of 39.51~50.83% at the moisture content of 14%. 5. The regression equations of the physical properties such as volume, bulk density, true density, and porosity of the grain were determined as a function of moisture content.

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Fabrication of Porous SiC Ceramics by Partial Sintering and their Properties (부분소결공정에 의한 다공질 탄화규소 세라믹스의 제조 및 특성)

  • 김신한;김영욱;윤중열;김해두
    • Journal of the Korean Ceramic Society
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    • v.41 no.7
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    • pp.541-547
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    • 2004
  • Addition of large particles restrains densification by small particles in mixed particle systems. In the present study, large SiC whiskers or particles were introduced into small particles for restraining densification and the mixtures were sintered using yttrium aluminum garnet (Y$_3$A1$\sub$5/O$\sub$12/, YAG) as a sintering additive. By controlling the content of large SiC whiskers or particles and the applied pressure during sintering, porous SiC ceramics, with a porosity ranging from 0.3% to 39%, were fabricated. Porosity increased with increasing the content of restraining materials. SiC whiskers were more effective than large SiC partcles for restraining densification. Permeability of the porous SiC ceramics increased with increasing the porosity. Flexural strength decreased with increasing porosity. A noticeable increase in strain to failure was observed in the porous ceramics with a porosity ranging from 18% to 39%.

Effect of Porosity on the High-Cycle Fatigue Behavior of Al-Si-Mg Casting Alloy (Al-Si-Mg계 주조용 알루미늄 합금의 고주기 피로 거동에 미치는 기공의 영향)

  • Lee, Young-Jae;Kang, Won-Guk;Euh, Kwang-Jun;Cho, Kyu-Sang;Lee, Kee-Ahn
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.05a
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    • pp.350-352
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    • 2009
  • The effect of porosity on the high-cycle fatigue properties of Al-Si-Mg casting aluminum alloys was investigated in this study. Microstructure examination, tensile and high-cycle fatigue test were conducted on both Al-Si-Mg casted (F) and heat-treated (T6) conditions. Porosity characteristics on the fracture surfaces of fatigue-tested samples were examined using SEM and image analysis. The microstructure observation results showed that eutectic Si particles were homogeneously dispersed in the matrix of the Al-Si-Mg casting alloys, but there were porosities formed as cast defects. The high-cycle fatigue results indicated that the fatigue strength of the 356-T6 alloy was higher than that of the 356-F alloys because of the significant reduction in volume fraction of pores by heat treatment. The SEM fractography results showed that porosity affected detrimental effect on the fatigue life: 80% of all tested samples fractured as a result of porosity which acted as the main crack initiation site. It was found that fatigue life decreased as the size of the surface pore increased. A comparison was made between surface pore and inner pore fur its effect on the fatigue behavior. The results showed that the fatigue strength with the inner pores was higher than that of the surface pore.

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