• Proceedings of the Korean Society For Composite Materials Conference
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• 2005.04a
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• pp.265-268
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• 2005

A new method for measurement of the pore size in a nanohoneycomb structure using atomic force microscopy (AFM) was proposed. Porous type anodic aluminum oxide (AAO) was fabricated as a nanohoneycomb structure to measure the pore size. For measuring pore sizes from AFM images, a criterion was set in porous type AAO. The pore sizes from AFM images were compared with those from SEM images, and the results showed good agreement. The relationship between the pore size and widening time was found to be linear in the range of this study. It was understood as the synchronized effects of the impurity gradient in outer oxide of AAO, mechanical packing and mass transfer increase.

• Journal of the Korean Ceramic Society
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• v.45 no.11
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• pp.675-680
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• 2008

The effect of pore former content on both porosity and pore structure was investigated for porous sintered reaction-bonded silicon nitrides (SRBSNs). A spherical PMMA with $d_{50}=8{\mu}m$ was employed as a pore-former. Its amount ranged from 0 to 30 part. Porous SRBSNs were fabricated by post-sintering at various temperatures where the porosity was controlled at $12{\sim}52%$. The strong tendency of increasing porosity with PMMA content and decreasing porosity with sintering temperature was observed. Measured pore-channel diameter increased $(0.3{\rightarrow}1.1{\mu}m)$ with both PMMA content and sintering temperature.

• Proceedings of the Membrane Society of Korea Conference
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• 2001.10a
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• pp.39-50
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• 2001

The performance of membranes is governed their pore struture. Pore structures of porous materials can be determined by a number of techniques. However, The novel technique, capillary folw porometry has a number of advantages. In this technique, the sample is brought in contact with a liquid that fills the pores in the membrane spontaneously. Gas under pressure is used to force the liquid from the pores and increase gas flow. Gas flow rate measured as a function of gas pressure in wet and dry samples yield data on the largest pore size, the mean flow pore size, flow distribution and permeability. Pore characteristics of a number of membranes were measured using this technique. This technique did not require the use of any toxic material and the pressure employed was low. Capillary flow porometry is a suitable technique for measurement of the pore structure of many membranes.

• Journal of the Korean Ceramic Society
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• v.41 no.7
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• pp.497-502
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• 2004

A hybrid coextrusion and lamination process has been developed to fabricate macrochanneled bioceramic scaffolds. This process was mainly composed of three steps (i.e., coextrusion of thermoplastic compound, lamination, and thermal treatment), forming unique pore channels in dense bioceramic body. Pore channels were formed by removing carbon black material, while calcium phosphate or Tetragonal Zirconia Polycrystals (TZP) with a calcium phosphate coating layer were used as dense body. Two kinds of pore structures were fabricated; that is, the pore channels were formed in uni- or three-directional array. Such macrochanneled bioceramic scaffolds exhibited the precisely controlled pore structure (pore size, porosity, and interconnection), offering excellent mechanical properties and cellular responses.

• Bulletin of the Korean Chemical Society
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• v.30 no.7
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• pp.1559-1562
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• 2009

The influence of hot pressing on the pore structures of Nafion membranes was investigated by observing the Nafion before and after hot pressing with $^1H$ nuclear magnetic resonance (NMR) spectroscopy. The freezing point depression and chemical shift data of water in the Nafion indicated the presence of two different pore size ranges in Nafion. Hot pressing mainly reduced the sizes and number of the big pores. The reduction of water uptake and proton conductivity after hot pressing was explained by this variation of pore size and number. We demonstrated the potential application of chemical shift data and NMR cryoporometry experiments to measure the relative pore sizes, on a nano scale, and numbers.

• Architectural research
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• v.15 no.1
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• pp.53-58
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• 2013

High strength concrete is being used increasingly in mass structure projects. The purpose of this study is to investigate the influence of temperature during mixing, placing and curing on the strength development, hydration products and pore structures of high strength concrete in mass structures. The experiments were conducted with two different model walls, viz.: 1.5 m and 0.3 m under typical summer and winter weather conditions. The final part of this study deal with the clarification of the relationship between the long-term strength loss and the microstructure of the high strength concrete at high temperatures. Test results indicated that high elevated temperatures in mass concrete structures significantly accelerate the strength development of concrete at the early ages, while the long-term strength development is decreased. The long-term strength loss is caused by the decomposition of ettringite and increased the total porosity and amount of small pores.

• The Journal of Engineering Geology
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• v.20 no.4
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• pp.461-465
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• 2010

Weathering and permeability in rocks play a very important role in underground disposal of radioactive waste and their long-term management as well as stability security of rock structures. Weathering and permeability of rocks are largely controlled by the characters of inner structures of rocks. In other words, weathering rate can be accelerated depending on the quantity of pore and microcrack in rocks. Quantitative evaluation of inner structures of rocks can serve as a tool that can assess the degree of weathering of rocks. Therefore it can be said that the understanding of three dimensional distribution of the inner structure of rocks is important for long-term management of rock structures. This study was performed to analyze three dimensional distribution of pore in rocks using Micro Focus X-ray CT on fresh granite and weathered granite from Korea. Results of the analysis clearly show distribution of pore and porosity of the inner rock.

• Computers and Concrete
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• v.17 no.1
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• pp.107-127
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• 2016

Concrete is a heterogeneous material containing many weaknesses such as micro-cracks, pores and grain boundaries. The crack growth mechanism and failure behavior of concrete structures depend on the plastic deformation created by these weaknesses. In this article the non-linear finite element method is used to analyze the effect of presence of micro pore near a crack tip on both of the characteristics of crack tip plastic zone (its shape and size) and crack growth properties (such as crack growth length and crack initiation angle) under pure shear loading. The FE Code Franc2D/L is used to carry out these objectives. The effects of the crack-pore configurations and the spacing between micro pore and pre-excising crack tip on the characteristics of crack tip plastic zone and crack growth properties is highlighted. Based on the obtained results, the relative distance between the crack tip and the micro pore affects in very significant way the shape and the size of the crack tip plastic zone. Furthermore, crack growth length and crack initiation angle are mostly influenced by size and shape of plastic zone ahead of crack tip. Also the effects of pore decrease on the crack tip by variation of pore situation from linear to perpendicular configuration. The critical position for a micro pore is in front of the crack tip.

• YAKHAK HOEJI
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• v.29 no.4
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• pp.176-182
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• 1985

As a part of the studies on adsorptive properties of Korean halloysite clays, Hadong white clays of premium grade were examined for geometric pore structured by mercury porosimetry and for specific surface areas by nitrogen adsorption according to the BET procedure. Three size fractions of the native clay sample were derived from passage BS #100, #200 and #325 meshes, respectively. Several parameters lhus observed in relation to the pore structures are shown below: 1. The size fraction of BS #100, #200 and #325 show internal pore volumes of 25.3, 30.2 and $35.0m^2g^{-1}$, respectively. 2. In the distribution curves of the cumulative pore volume against pore diameter, it has been shown that the larticle sizes, the steeper the distribution over the larger ranges of pore diameters. The converse is true the smaller particles. 3. Internal pore areas increase with decrease in pore sizes. It follows that the pores having diameters of $\leq$0.1$\mu\textrm{m}$ are responsible for more than 90% of the total pore area. 4. The behaviour of nitrogen adsorption can be best described by BET type IV isotherm. Further, the hysteresis loops of the adsorptiondesorption curves become narrower with decresing particle sizes. 5. The specific surface areas observed for the fractions of BS #100, BS #200 and BS #325 are 34.6, 35.4 and 43.2m $^2g^{-1}$, respectively. and the calcined clay of BS #325 has a specific surface area near $30.4m^2g^{-1}$.

• Archives of Metallurgy and Materials
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• v.67 no.4
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• pp.1547-1550
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• 2022

In this study, a flake-shaped metal powder was coated on a tube shaped pre-sintered 316L stainless steel support using a wet powder spraying process to fabricate a double pore structure, and the pore characteristics were analyzed according to coating time and tube rotation speed. The thickness of the coated layer was checked via optical microscopy, and porosity was measured using image analysis software. Air permeability was measured using a capillary flow porometer. As a result of the experiment, the optimal rotation speed of the support tube was established as 200 rpm. When the rotation speed was fixed, the coating thickness and the coating amount of the double pore structure increased as the coating time increased. The porosity of the double pore structure was increased due to the irregular arrangement of the flake-shaped powder. The air permeability of the double pore structure decreased with increasing fine pore layer thickness.