• 한국산학기술학회논문지
• /
• 제6권6호
• /
• pp.473-477
• /
• 2005

본 연구에서는 폐유리를 여러 가지 조건으로 시편 1에서 5까지 발포실험을 하여 발포유리의 pH, 밀도, 열전도, 압축강도 그리고 흡음률을 측정하였다. 시편별 pore크기는 시편 1의 Pore가 가장 적게 발포되었고, 시편 5의 경우 pore크기가 시편 1보다 3배 이상 크게 발포되었다. pore크기가 시편 5에서 가장 크게 발포되었지만, 밀도가 낮은 것 외에는 압축강도와 흡음률의 결과가 최종목표에 미달하였고, 시편 1의 경우에는 밀도가 최종목표 $0.8g/cm^3$ 보다 우수한 $0.58g/cm^3$로 나타났고, 압축강도의 경우도 최종목표보다 높은 $22kg/cm^3$로 나타났으며, 흡음재로서의 흡음률은 시편 1의 경우 NRC 0.68로서 최종목표인 NRC 0.7에 근접하는 결과를 얻었다.

• Geomechanics and Engineering
• /
• 제3권2호
• /
• pp.83-108
• /
• 2011

The effect of non-plastic fines (silt) on liquefaction and pore pressure generation characteristics of saturated sands was studied through undrained stress controlled cyclic triaxial tests using cylindrical specimens of size 50 mm diameter and height 100 mm at different cyclic stress ratios and at a frequency of 0.1 Hz. The tests were carried out in the laboratory adopting various measures of sample density through various approaches namely gross void ratio approach, relative density approach, sand skeleton void ratio approach, and interfine void ratio approach. The limiting silt content and the relative density of a specimen were found to influence the undrained cyclic response of sand-silt mixtures to a great extent. Undrained cyclic response was observed to be independent of silt content at very high relative densities. However, the presence of fines significantly influenced this response of loose to medium dense specimens. Combined analyses of cyclic resistance have been done using the entire data collected from all the approaches.

• 한국세라믹학회지
• /
• 제47권5호
• /
• pp.365-372
• /
• 2010

This paper was to evaluate the influence of kiln process parameter(kiln angle, kiln rotating speed) of lightweight aggregate using waste glass and bottom ash with industrial by-products on thermal conductivity, density, water absorption, fracture load and porosity by response surface analysis. In the results of surface plot and contour plot, it has verified that kiln residence time of lightweight aggregate increase as kiln angle and rotating speed decreases. For this reason, pore size and quantity tend to increase by active reaction of forming agent. It seems to be that increase in pore size and quantity have caused decreasing density, fracture load and thermal conductivity, and increasing water absorption. In conclusion, optimization of kiln process parameter on thermal conductivity, density, water absorption, fracture load and porosity by response surface analysis are kiln angle 2.4646%, kiln rotating speed 40.7089 rpm.

• 자원리싸이클링
• /
• 제7권4호
• /
• pp.27-34
• /
• 1998

본 연구에서는 NiCuZn Ferrite(NCZF) 제조공정의 제어에 대하여 연구하였다. $700^{\circ}C$, 3시간 하소한 NCZF를 약 60시간 볼밀링하여 약 $0.5\mu\;extrm{m}$ 입자크기로 분쇄한 후 분무 건조하여 과립화하였다. NCZF의 충전율에 따른 겉보기 고화속도 및 초기투자율에 미치는 영향을 조사한 결과 다음과 같은 결과를 얻었다. 1. 성형압력 유지시간 1분에서 성형압력을 약 20~170 ㎫로 변화시켜 제조한 NCZF 토로이달 상의 출발시편은 성형압이 증가하면서 입자의 충전율은 48.6%에서 56.8%로 증가하였다. 2. 일정 소성온도에서 NCZF의 충전율이 높아질수록 고화속도가 높아지고, 일정 성형압력에서 소성온도가 높아질수록 NCZF의 겉보기 고화속도는 빨라졌다. NCZF의 충전율과 소성온도가 높고, 소성시간이 길어지면 bulk density는 증가하였다. 3. 고정된 조성에서 소성온도($875~925^{\circ}C$)와 소성시간(0~5시간)의 조합에 의해 제조된 NCZF의 초기투자율은 bulk density와 semi-log상에서 직선적인 비례관계를 가지며 NCZF입자의 충전율에 크게 의존하였다. NCZF입자의 충전율과 이들을 소성하였을 때의 bulk density를 알면 초기투자율을 예측할 수 있었다. log $\mu$i=$G1{\times}BD$+$G2{\times}충전율$+b(0), G1;0.8394, G2;-3.6233, (b);0.7053.

• 한국구조물진단유지관리공학회 논문집
• /
• 제24권5호
• /
• pp.143-149
• /
• 2020

본 연구에서는 금속 적층 제조로 출력한 격자 구조체의 내부 공극에 반응성 아크릴 화합물을 충진시켜, 밀도 제어가 가능한 밀실 복합 격자 구조체를 제작하는 것을 목표로 한다. 또한 본 격자 구조체를 건설분야에 적용하기 위하여 반응성 아클릴 화합물에 보통 포틀랜드 시멘트를 첨가함으로써 콘크리트와의 부착성능을 향상시킨 부착력 증진 반응성 아크릴 화합물을 검토하였다. 최종적으로 제조한 부착력 증진 반응성 아크릴 화합물을 격자 구조체 내부에 충진하여 밀도 제어형 기능성 복합 격자 구조체(Hybrid Lattice structure)의 비중, 흡수율 및 부착강도를 검토하였다. 그 결과, 밀도 제어 가능, 흡수율 1.0 % 이하 및 재령 1일 부착강도 1.78 MPa ~ 1.98 MPa의 결과물을 도출하였다.

• 한국재료학회지
• /
• 제31권2호
• /
• pp.108-114
• /
• 2021

In the manufacturing of bulk graphite, pores produced by vaporization and discharge of volatile materials in binders during carbonization reduce the density of bulk graphite, which adversely affects the electrical conductivity, strength and mechanical properties. Therefore, an impregnation process is introduced to fill the pores and increase the density of bulk graphite. In this study, bulk graphite is prepared by varying the viscosity of the impregnant. The microstructure of bulk graphite is observed. The flexural strength and electrical resistivity are measured. As the viscosity of the impregnants decreases and the number of impregnations increases, it is shown that the number of pores decreases. The density before impregnation is 1.62 g/㎤. The density increases to 1.67 g/㎤ and porosity decreases by 18.6 % after three impregnations using 5.1 cP impregnant, resulting in the best pore-filling effect. After three times of impregnation with a viscosity of 5.1 cP, the flexural strength increases by 55.2 % and the electrical resistivity decreases by 86.76 %. This shows that a slight increase in density due to the pore-filling effect improves the properties of bulk graphite.

• Geomechanics and Engineering
• /
• 제24권5호
• /
• pp.419-430
• /
• 2021

Investigation on the compressibility and shear strength of compacted loess is of great importance for the design and operation of engineering infrastructures in filling area. In this study, the mechanical behaviors of Yan'an compacted loess are investigated at various dry densities and water contents by conducting one dimensional compression and direct shear tests. And the elastic compressibility, plastic compressibility, yield stress and strength are obtained from the experiments. Results show that when water content increases, plastic compressibility parameter increases, but yield stress decreases. However, the increase of dry density leads to a decrease in plastic compressibility parameter but an increase in yield stress. In addition, elastic compressibility parameter is found to be a constant which is irrelevant to water content and dry density. As for strength, cohesion and internal friction angle is directly proportional to dry density, but inversely proportional to water content. Moreover, the mercury intrusion porosimetry (MIP) and scanning electron microscope (SEM) tests were also performed to observe the pore size distribution and microstructure of the specimens. Finally, by using results of MIP and SEM tests, the compressibility and strength behaviours of Yan'an compacted loess are explained from the perspective of pore-size distribution and microstructure.

• 청정기술
• /
• 제29권4호
• /
• pp.249-254
• /
• 2023

본 연구에서는 제올라이트의 물리적 특성으로부터 기공율을 추정하는 연구를 수행하였다. 입자상 물질의 기공율 직접 측정의 어려움으로 본 연구에서는 여러 문헌에서 제시된 계산식에 제올라이트의 물리적 특성 측정값을 적용하여 기공율을 계산하였다. 이를 위해 제올라이트 3종-zeolite beta, zeolite Y, ZSM-5-에 대해 각각의 평균입자 크기 및 particle size distribution, 비표면적 및 기공특성을 측정하였으며, 가스와 액상을 이용한 진밀도, tap과 untapped를 적용한 겉보기 밀도를 측정하였다. 측정결과로부터 기공율을 계산하여 결과를 비교하고 기공율을 결정하는 주요 인자에 대해 평가하였다.

• Archives of Plastic Surgery
• /
• 제37권5호
• /
• pp.509-518
• /
• 2010

Purpose: Major drawbacks of conventional bone marrow stromal cells (BSCs) transplantation method are mainly caused by direct transplanted cell to host cell interactions. We hypothesized that separation of the transplanted cells by a microporous membrane might inhibit most of the potential adverse effects and induce superior effect. The purpose of the study is to determine the optimal condition of the microporous membrane. Methods: First, BSCs were placed in polyethylene terephthalate (PET) transwell inserts with 3, 8, or $12{\mu}m$ pore size, and cultured in 24 well culture plates. After 5 days, bottoms of the plates were observed for presence of attached BSCs in monolayer and cell numbers were evaluated. Second, BSCs were placed PET, polycarbonate (PCT), and mixed cellulose esters (MCE) transwell inserts with 3 and $8{\mu}m$ pore size, and cultured in 24 well culture plates. After 3 days, the supernatants of the media left in culture plate were analyzed for collagen, vascular endothelial growth factor (VEGF), platelet derived growth factor BB (PDGF-BB), and basic fibroblast growth factor (bFGF). Third, BSCs were placed in 15% and 70% of the PET membrane with $3{\mu}m$ pore size. All the experimental conditions and methods were same as the second study. Results: The optimal pore sizes to prevent BSC leakage were $3{\mu}m$ and $8{\mu}m$. The amounts of type I collagen and three growth factors tested did not show significant differences among PET, PCT, and MCE groups. However, the collagen, VEGF, and bFGF levels were much higher in the high (70%) density group than in the low (15%) density group. Conclusion: This study revealed that the optimal pore size of membrane to prevent direct BSC to recipient cell contact is in between $3{\mu}m$ and $8{\mu}m$. Membrane materials and pore sizes do not influence the collagen and growth factor passage through the membrane. The most striking factor for collagen and growth factor transport is pore density of the membrane.

• 대한치과기공학회지
• /
• 제29권1호
• /
• pp.23-34
• /
• 2007

The quantity of MgO in the Zirconia of 20wt% Frit has been varied and the sintering temperature has been differentiated to monitor the changes in the mechanical features. The rise of sintering temperature from 1100$^{\circ}C$ to 1300$^{\circ}C$ was followed by higher sintering density. And, at a sintering temperature, the increase of the quantity of MgO was followed by lower sintering density. The bending strength has been lowered as the quantity of MgO increases in the Zirconia of 20wt% Frit, which seems to be because the MgO functions as impurities degrading the mechanical features. In terms of micro-structure analysis, the pore has been greatly enlarged, while the density varied very little, when the MgO of 3wt% was added. The size of pore became smaller as the added quantity of MgO increased larger in the sequence of 5wt% and 7wt%. But, the pore-generating rate became higher as the added quantity of MgO increased in the sequence of 3wt%, 5wt% and 7wt%. Thus, it is possible to summarize that the small quantity of MgO, say, of 3wt%, promotes the grain growth, and the large quantity of MgO, say, of 7wt%, hinders the grain growth. Also, if the quantity of MgO exceeds some level, the MgO hinders substances from moving, which, ultimately, keeps blowholes from becoming enlarged or extinct, and makes pores small and dispersed in broad area. In conclusion, the study on the change in the size of pore shows that the larger the quantity of MgO is, the more the micro pores are, thereby degrading the mechanical features.