• 박물관보존과학
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• 제9권
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• pp.1-15
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• 2008

국립중앙박물관에 소장되어 있는 신안 해저 출토 유물인 경덕진 백자 중'복소법(覆燒法)'으로 제작되어 구연부에 유약이 시유되지 않은 부분에 금속 테두리(金屬釦)를 덧씌운 '청백자인각화훼문은구완' 4점과 '백자은구대접' 1점에 대해 구연에 주사전자현미경(SEM)으로 단면과 미세 구조를 관찰하였고, 성분 분석은 에너지분산형분석기(EDS)의 반사전자상(BEI)으로 측정한 결과, 금속 테두리는 은(銀)이 아닌 주석 재질임을 알 수 있었다. 또한 구연부에 금속 테두리를 접합 방법을 알아 보기 위해 퓨리어변환 적외선 분석기(FT-IR)로 조사해 본 결과, 접합 재료는 옻 성분을 사용하여 고정하였음을 알 수 있었다.

• The Journal of Advanced Prosthodontics
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• 제3권4호
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• pp.196-203
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• 2011

PURPOSE. This study evaluated marginal fit of glass infiltrated alumina cores fabricated using two techniques and their marginal stability after firing cycles of veneering porcelain. MATERIALS AND METHODS. Fifteen standardized all-ceramic crowns were fabricated on a metal die using each technique: slip cast technique of VITA In-Ceram sprint Alumina (Group A as control) and plastic foil matrix technique of Turkom-Cera fused alumina core system (Group B). Copings were compared between groups and within groups at coping stage and after firing each layer of veneering porcelain. A device was used to standardize seating of copings on the metal die and positioning of the specimens under the microscope after each stage of fabrication. The specimens were not cemented and marginal gap was measured using an image analyzing software (Imagepro Express) on the photographs captured under an optical microscope. Two tailed unpaired 't test' was used to compare marginal gaps in two groups and one way ANOVA was used to analyze marginal distortion within each group at 95% confidence interval. RESULTS. The marginal gap was smaller at the coping stage in group B ($60+30{\mu}M$) than group A ($81+21{\mu}M$) with statistical significance. After firing of veneering porcelain the difference was insignificant. At the final stage, both groups exhibited lower mean marginal gaps than at the initial coping stage with the difference of $11.75{\mu}M$ for group A and $11.94{\mu}M$ for group B, but it was statistically insignificant due to high value of standard deviation. CONCLUSION. Within the limitations of this study, it was concluded that both techniques produced copings with comparable and acceptable marginal fit and marginal stability on firing veneering porcelain.

• The Journal of Advanced Prosthodontics
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• 제6권5호
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• pp.387-394
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• 2014

PURPOSE. Topographic analysis of treated ceramics provides qualitative information regarding the surface texture affecting the micromechanical retention and locking of resin-ceramics. This study aims to compare the surface microstructure following different surface treatments of feldspathic porcelain. MATERIALS AND METHODS. This in-vitro study was conducted on 72 porcelain discs randomly divided into 12 groups (n=6). In 9 groups, feldspathic surfaces were subjected to sandblasting at 2, 3 or 4 bar pressure for 5, 10 or 15 seconds with $50{\mu}m$ alumina particles at a 5 mm distance. In group 10, 9.5% hydrofluoric acid (HF) gel was applied for 120 seconds. In group 11, specimens were sandblasted at 3 bar pressure for 10 seconds and then conditioned with HF. In group 12, specimens were first treated with HF and then sandblasted at 3 bar pressure for 10 seconds. All specimens were then evaluated under scanning electron microscopy (SEM) at different magnifications. RESULTS. SEM images of HF treated specimens revealed deep porosities of variable sizes; whereas, the sandblasted surfaces were more homogenous and had sharper peaks. Increasing the pressure and duration of sandblasting increased the surface roughness. SEM images of the two combined techniques showed that in group 11 (sandblasted first), HF caused deeper porosities; whereas in group 12 (treated with HF first) sandblasting caused irregularities with less homogeneity. CONCLUSION. All surface treatments increased the surface area and caused porous surfaces. In groups subjected to HF, the porosities were deeper than those in sandblasted only groups.

• 한국세라믹학회지
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• 제42권2호
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• pp.99-103
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• 2005

현재 국내에서 많은 양의 도자기 폐기물이 발생하고 있으며, 이들 폐기물은 경제적 이득과 환경 보전의 차원에서 재활용하는 방안이 모색되어져야 한다. 따라서, 본 연구에서는 도자기 폐기물을 콘크리트용 골재로 이용하여 폐도자기의 재활용성을 검증하고자 하였다. 폐도자기 재활용 골재(recycled aggregate)의 품질을 부순 골재(crushed aggregate)와 비교 분석하였으며, 부순 골재 단독 콘크리트와 재활용 골재가 비례대로 치환된 콘크리트의 물리적 특성을 비교 분석하였다. 실험 결과 재활용 폐도자기의 비율이 $10\%,\;20\%$, 그리고 $30\%$까지는 압축강도에 작은 영향을 미쳤지만, 재활용 폐도자기의 비율이 $30\%$ 이상 증가할수록 압축강도는 급격히 감소하였으며, 홉수율은 증가하였다. 실험 결과에 따르면, 일정한 압축강도를 지니는 폐도자기 재활용 콘크리트의 제조를 위해서 대체 가능한 재활용 골재의 최대 함량은 $30\%$임을 확인 할 수 있었다.

• 대한치과보철학회지
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• 제29권2호
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• pp.195-209
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• 1991

When the porcelain fused to metal restorations were fractured at the metal interface, various techniques and materials for intraoral porcelain repair have been suggested. The purpose of this study was to investigate the effect of metal surface treatment method and water storage on the shear bond strength of four porcelain repair systems. : Clearfil(Kuraray), All-bond(Bisco), Superbond C & B(Sun Medical), Panavia OP(Kuraray). After the metal surfaces of the specimens were sandblasted by aluminum oxide or roughened by diamond point, they were stored in double deionized water(24 Hr., $37^{\circ}C$) and thermocycling was performed(24 Hr., 1024 cycles), and again half of specimes were stored in water bath(2 Months, $37^{\circ}C$). Mean shear bond strength and mode of failure were recorded. The results of this study were obtained as follows : 1. Differences were observed between the sandblasted and diamond - treated specimens in Clearfil, All-bond, and Superbond. No statistically significant differences were observed in Panavia. 2. The 2-month storage time significantly affected the bond strength of All-bond and Superbond. No statistically significant differences were observed in Clearfil and Panavia. 3. The failures were observed at the interface between opaque resin and the metal in Clearfil and All-bond. 4. The failures were observed at the interface between opaque resin and veneered resin in Panavia. The failures were observed at the interface between opaque resin and veneered resin in Superbond, but 40% of them were fractured at the interface between the metal and opaque resin after 2-month storage time.

• KSBB Journal
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• 제15권2호
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• pp.208-213
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• 2000

백자, 청자 및 일반 자기 제조용 점토인 3종류의 점토(백토, 청토, 황토)를 철환원 미생물을 이용한 숙성과정을 통해 점토의 개질을 수행하였다. 철환원 미생물을 이용한 숙성기간 동안 점토 종류에 따른 철환원 및 용출특성과 숙성된 점토들의 물성 변화를 조사하였다. 숙성기간동안 점토의 철용출량은 점토의 종류에 관계없이 탄소원인 sucrose의 첨가량이 증가할수록 증가하였지만, 총 철용출량과 용출속도는 점토의 종류에 의존하였다. 숙성점토는 원료물질과 비교하여 sucrose 의 첨가량이 증가함에 따라 수축을 변화없이 강도와 색도가 향상되었다. 점토의 색도는 점토의 종류에 많은 영향을 받았으며, 점토의 숙성과정은 색도 중 적색도가 가장 많이 감소하는 효과를 제공하였다. 숙성점토의 물리적 특성과 탈철양을 고려할 때, 점토 중에 함유된 철환원을 전자공여체로 제공되는 sucrose의 최적 첨가량은 4wt% 임을 확인하였다.

• 한국건축시공학회지
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• 제14권3호
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• pp.237-243
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• 2014

지구온난화 현상으로 인해 환경 문제가 심각하며, 또한, 시멘트의 원료인 석회석과 골재의 무분별한 채취로 인한 환경파괴와 자원고갈의 심각성이 강조되고 있는 상황에서 문제점을 줄이려는 노력이 지속되고 있는 실정이다. 따라서, 본 연구에서는 천연골재 대체재인 폐자기를 혼합하여 적용시켰다. 또한, 시멘트 대체재로써 마그네시아 인산염 복합체와 플라이애시를 혼입하여 그에 따른 인조석재의 특성을 알아보고자 한다. 실험결과, 폐유리 혼합비율 60% 및 폐자기 혼합비율 70%가 인조석재의 전반적인 실험에서 가장 우수한 것으로 판단되며, 인조석재의 기초적인 자료로 활용할 수 있을 것으로 기대된다.

• 대한치과의사협회지
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• 제27권6호통권241호
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• pp.509-514
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• 1989

국소의치나 총의치에 사용하는 인공치는 대부분 도재치(porcelain teeth)와 레진치(resin teeth, plastic teeth)이다. 도재치나 레진치 모두 자연치아와 유사한 색조를 갖고 있어 자연감을 나타내기 때문이다. 인공치의 대표적인 도재치와 레진치에 대하여 이공학적 측면, 임상측면, 기공측면에서 재료학적 고찰을 한다.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2006년도 추계학술대회 논문집 Vol.19
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• pp.326-327
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• 2006

The paper describes the development of arrester for 154kV class power station and substation. The arrester employs silicone insulating materials for Its housing, instead of the conventional porcelain housing. The sealing integrity is related to safe operation of surge arrester, the prime failure reason of porcelain housed arresters is moisture ingress. In this paper, the sealing integrity of polymeric surge arresters for ultra high voltage is investigated with moisture ingress test. The diagnostic techniques are discusses, including watt loss, partial discharge, AC leakage current, 1mA DC voltage and residual voltage.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2008년도 제39회 하계학술대회
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• pp.462-463
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• 2008

36,000lbs porcelain insulators (D-1995, D-1997, D-2002) investigated mechanical and electrical qualities, which were installed in the Korea 154kV transmission lines. This paper assessed Weibull distribution function, quality index, and uniformity index to forecast the remaining life expectancies of insulators. Applying Weibull distribution function on year lapse change test, electro-mechanical failing load test, and HRB values confirmed a significant degree of correlation. Statistically calculating the life expectancy through quality indices for aging and new products and uniformity indices that are associated with uniformity of insulation materials revealed.