• 한국정보디스플레이학회:학술대회논문집
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• 2004.08a
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• pp.223-226
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• 2004

MgO thin films were deposited bye-beam evaporation on $SiO_2$/Si wafers for the application of a protective layer in alternating current plasma display panels (AC-PDPs). Three different MgO sources, single crystal, melted polycrystal and sintered polycrystal, were used to find out the change of the properties of MgO protective layer depending on the source type. The properties of MgO thin films such as density, orientation and surface morphology were influenced by the source type. MgO thin films deposited with the melted polycrystal source had the highest density with the highest (100) preferred orientation, whereas the films deposited with the sintered polycrystal source had the lowest density with less preferred orientation. Such a result seems to be originated from the different mobility of adatoms on the surface of the deposited MgO thin films. Different microstructures of MgO thin films deposited even in the same deposition condition were observed depending on the MgO source type, resulting in different discharge characteristics.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2008.10a
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• pp.130-133
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• 2008

The formability of DP steels can be affected by not only initial texture but also deformation texture evolved during plastic deformation. To investigate the evolution of deformation texture during deep drawing, deep drawing process for DP steels was carried out experimentally. A rate sensitive polycrystal model was used to predict texture evolution during deep drawing process. In order to evaluate the strain path during deep drawing, a steady state was assumed in the flange part of deep drawn cup. A rate sensitive polycrystal model successfully predicted the texture development in DP steels during deep drawing process. It was found that the final stable orientations were strongly dependent on the initial location in the blank.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2004.08a
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• pp.72-82
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• 2004

The deformation mechanism of hexagonal close-packed materials is quite complicate including slips and twins. A deformation mechanism, which accounts for both slip and twinning, was investigated for polycrystalline hop materials. The model was developed in a finite element polycrystal model formulated with initial strain method where the stiffness matrix in FEM is based on the elastic modulus. We predicted numerically the texture of Mg alloy(AZ31B) sheet by using FEM based on crystal plasticity theory. Also, we introduced the recrystallized texture employed the maximum energy release theory after rolling. From the numerical study, it was clarified that the shrink twin could not be the main mechanism for shortening of c-axis, because the lattice rotation due to twin rejects fur c-axis to become parallel to ND(normal direction of plate). It was showed that the deformation texture with the pyramidal slip gives the ring type pole figure having hole in the center.

• Transactions of Materials Processing
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• v.26 no.5
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• pp.286-292
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• 2017

Magnesium alloy shows strong anisotropy and asymmetric behavior in tension and compression curve, especially at room temperature. These characteristics limit the application of finite element method (FEM) which is based on conventional continuum mechanics. To accurately predict the material behavior of magnesium alloy at microstructural level, a methodology of fully coupled multiscale simulation is presented and a crystal plasticity model as a constitutive equation in the simulation of metal forming process is introduced in this study. The existing constitutive equation for rigid plastic FEM is modified to accommodate deviatoric stress component and its derivatives with respect to strain rate components. Viscoplastic self-consistent (VPSC) polycrystal model was selected as a constitutive model because it was regarded as the most robust model compared to Taylor model or Sachs model. Stiffness matrix and load vector were derived based on the new approach and implemented into $DEFORM^{TM}-3D$ via a user subroutine handling stiffness matrix at an elemental level. The application to extrusion and rolling process of pure magnesium is presented in this study to assess the validity of the proposed multiscale process.

• Korean Journal of Metals and Materials
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• v.48 no.7
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• pp.605-614
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• 2010

Conventional rolling (symmetric) and differential speed rolling (DSR) were both applied to AA1050 sheets at various velocity ratios, from 1 to 2 between the top and bottom rolls. An electron backscatter diffraction (EBSD) technique was used to measure texture inhomogeneity through the thickness direction. After the annealing process, the annealing texture of the DSR processed sheets was different from that of conventionally rolled sheets. The velocity ratio between the top and bottom rolls affected the texture inhomogeneity and macroscopic plastic strain ratio of the AA1050 sheets. A prediction for the macroscopic plastic strain ratio of AA1050 sheets was carried out using a visco-plastic self-consistent (VPSC) polycrystal model. The strain ratio directionality that was predicted using the VPSC polycrystal model was in good agreement with experimental results.

• Korean Journal of Metals and Materials
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• v.47 no.5
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• pp.274-282
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• 2009

To investigate the evolution of deformation texture in dual phase (DP) steels during deep-drawing deformation, deep-drawing experiments were performed. Microtexture measurements were conducted using electron backscattered diffraction (EBSD) to analyze texture evolution. A rate-sensitive polycrystal model was used to predict texture evolution during deep-drawing deformation. In order to evaluate the strain path during deep-drawing deformation, a steady state was assumed in the flange part of a deep-drawn cup. A ratesensitive polycrystal model successfully predicted the texture evolution in DP steels during deep-drawing deformation. The final stable orientations were found to be strongly dependent on the initial location in the blank. Texture analysis revealed that the deep drawability of DP steels decreases as the true strain in the radial direction of the deep-drawn cup increases during deep-drawing deformation.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2009.11a
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• pp.124-124
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• 2009

We observed the changes of crystal structure of Rubrene (5,6,11,12-tetraphenylnaphthacene) polycrystal thin films at various in situ substrate temperature and process by scanning electron microscope(SEM), x-ray diffraction (XRD) and near-field microwave microprobe (NFMM). Amorphous rubrene thin film was initially obtained on 200 nm thick $SiO_2/Si$ substrate at 35 $^{\circ}C$ in a vacuum evaporation but in situ long time postannealing at the temperature 80 $^{\circ}C$ transformed the amorphous phase into crystalline. Four heating conditions are followed : (a) preheating (b) annealing (c) preheating, annealing (d) preheating, cooling(35 $^{\circ}C$), annealing. We have obtained the largest polycrystal disk in sample (c). But the highest crytallity and conductivity of the rubrene thin films were obtained in sample (d).

• Transactions of Materials Processing
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• v.17 no.7
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• pp.517-522
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• 2008

A visco-plastic self-consistent (VPSC) polycrystal model has been applied to simulate texture simulation and anisotropic properties of DP steels during deep drawing process. In order to evaluate the strain path during deep drawing, a steady state was assumed in the flange part of deep drawn cup. The final stable orientations were strongly dependent on the initial location in the blank. The evolution of anisotropy of DP steel sheets has been demonstrated through comparison of plastic strain rate vector at the different plastic strain levels.

• Electrical & Electronic Materials
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• v.9 no.3
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• pp.270-276
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• 1996

As methane concentration was varied, the textures of diamond films deposited on Si(100)substrate were observed by XRD,SEM and Raman spectroscope. As a result, $O_{2}$ plasma etching has been useful to observe microscopic structure of diamond films by SEM. The cross section of diamond films deposited on Si(100)substrate with 4% concentration of methane to hydrogen was a polycrystal like a pillar. The diamond crystal like a pillar has been oriented to (110)surface and the high quality diamond film with FWHM of Raman spectra being 3.8 $cm^{-1}$ / has been grown. As time goes by deposition time, the preferred orientation increases

• Journal of the Korean Institute of Telematics and Electronics
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• v.25 no.8
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• pp.966-971
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• 1988

AES was used to study oxygen adsorption due to the oxygen exposure at 300\ulcorner temperature and segregation of impurities due to annealing on polycrystal copper surface. The intensity of peak of CuM2, 3VV and CuL3 VV increased with annealing time and the peak of CKLL increased after Ar ion bombardment. The effect of oxygen adsorption on copper surface at 300\ulcorner was verified by the decreased of peak of CuM2, 3VV and CuL3 VV as oxygen exposure increase. The binding energy of copper atoms gradualy shifts from 0.7eV to 1.5eV of copper atoms gradually shifts from 0.7eV to 1.5eV after a oxygen exposure. After the oxygen exposure, the width at half the height of CuM2, 3VV is larger 2V*C/S by the effect of chemical liaison of the copper aton with oxygen atom.