• Korean Journal of Metals and Materials
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• v.50 no.12
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• pp.931-937
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• 2012

The microstructure of Cu-15 wt%Ag composites fabricated by equal channel angular pressing (ECAP) with intermediate heat treatment at $320^{\circ}C$ was investigated by transmission electron microscopy (TEM) observations. Ag precipitates with a thickness of 20-40 nm were observed in the eutectic region of the Cu-15 wt%Ag composite solution treated at $700^{\circ}C$ before ECAP. The Cu matrix and Ag precipitates had a cube on cube orientation relationship. ECAPed composites exhibited ultrafine-grained microstructures with the shape and distribution dependent on the processing routes. For route A in which the sample was pressed without rotation between each pass, the Cu and Ag grains were elongated along the shear direction and many micro-twins were observed in elongated Cu grains as well as in Ag filaments. The steps were observed on coherent twin boundaries in Cu grains. For route Bc in which the sample was rotated by 90 degrees after each pass, a subgrain structure with misorientation of 2-4 degree by fragmentation of the large Cu grains were observed. For route C in which the sample was rotated by 180 degrees after each pass, the microstructure was similar to that of the route A sample. However, the thickness of the elongated grains along the shear direction was wider than that of the route A sample and the twin density was lower than the route A sample. It was found that more microtwins were formed in ECAPed Cu-15 wt%Ag than in the drawn sample. Grain boundaries were observed in relatively thick and long Ag filaments in Cu-15 wt%Ag ECAPed by route C, indicating the multi-crystalline nature of Ag filaments.

• Korean Journal of Metals and Materials
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• v.50 no.12
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• pp.913-920
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• 2012

In spite of some problems in processability and bondability, Au wires in the microelectronics industry are gradually being replaced by copper wires to reduce the cost of raw material. In this article, the effects of surface roughness enhanced capillaries on thermosonic Cu wire bonding were evaluated. The roughness-enhanced zirconia toughened alumina (ZTA) capillaries were fabricated via a thermal grooving technique. As a result, the shear bond strength of first bonds (ball bonds) bonded using the roughness-enhanced capillary was enhanced by 15% as compared with that of normal bonds due to more effective plastic deformation and flow of a Cu ball. In the pull-out test of second bonds (stitch bonds), processed at two limit conditions on combinations of process parameters, the bond strength of bonds formed using the roughness-enhanced capillary also resulted in values higher by 55.5% than that of normal bonds because of the increase in the bonding area, indicating the expansion of a processing window for Cu wire bonding. These results suggest that the adoption of roughness-enhanced capillaries is a promising approach for enhancing processability and bondability in Cu wire bonding.

• The Journal of Advanced Prosthodontics
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• v.14 no.5
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• pp.273-284
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• 2022

PURPOSE. Computer-aided design and manufacturing (CAD-CAM) of implant abutments has been shown to result in surface contamination from site-specific milling and fabrication processes. If not removed, these contaminants can have a potentially adverse effect and may trigger inflammatory responses of the peri-implant tissues. The aim of the present study was to evaluate the bacterial disinfection and cleaning efficacy of ultrasonic reprocessing in approved disinfectants to reduce the microbial load of CAD-CAM abutments. MATERIALS AND METHODS. Four different types of custom implant abutments (total N = 32) with eight specimens in each test group (type I to IV) were CAD-CAM manufactured. In two separate contamination experiments, specimens were contaminated with heparinized sheep blood alone and with heparinized sheep blood and the test bacterium Enterococcus faecium. Abutments in the test group were processed according to a three-stage ultrasonic protocol and assessed qualitatively and quantitatively by determination of residual protein. Ultrasonicated specimens contaminated with sheep blood and E. faecium were additionally eluted and the dilutions were incubated on agar plates for seven days. The determined bacterial counts were expressed as colony-forming units (CFU). RESULTS. Ultrasonic reprocessing resulted in a substantial decrease in residual bacterial protein to less than 80 ㎍ and a reduction in microbiota of more than 7 log levels of CFU for all abutment types, exceeding the effect required for disinfection. CONCLUSION. A three-stage ultrasonic cleaning and disinfection protocol results in effective bacterial decontamination. The procedure is reproducible and complies with the standardized reprocessing and disinfection specifications for one- or two-piece CAD-CAM implant abutments.

• Composites Research
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• v.35 no.6
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• pp.469-476
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• 2022

In this paper, the microwave absorbing characteristics after the impact of the radar-absorbing structure (RAS) consisting of periodic pattern sheet (PPS) and glass fiber-reinforced plastic (GFRP) were experimentally investigated. The fabricated RAS effectively absorbed the microwave in the X-band (8.2-12.4 GHz). In order to induce the damage to the RAS, a low-velocity impact test with various impact energy of 15, 40, and 60 J was conducted. Afterward, the impact damage was observed by using visual inspection, non-destructive test, and image processing method. Moreover, the absorbing performance of intact and damaged RAS was measured by the free-space measurement system. The experiment results revealed that the delamination damage from the impact energy of 15 J did not considerably affect the microwave absorbing performance of the RAS. However, fiber breakage and penetration damage with a relatively large damaged area were occuured when the impact energy was increased up to 40 J and 60 J, and these failures significantly degraded the microwave absorbing characteristics of the RAS.

• Korean Journal of Materials Research
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• v.32 no.9
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• pp.391-395
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• 2022

Research is being actively conducted on the continuous thin plate casting method, which is used to manufacture magnesium alloy plate for plastic processing. This study applied a heat transfer solidification analysis method to the melt drag process. The heat transfer coefficient between the molten magnesium alloy metal and the roll in the thin plate manufacturing process using the melt drag method has not been clearly established until now, and the results were used to determine the temperature change. The estimated heat transfer coefficient for a roll speed of 30 m/min was 1.33 × 10⁵ W/m²·K, which was very large compared to the heat transfer coefficient used in the solidification analysis of general aluminum castings. The heat transfer coefficient between the molten metal and the roll estimated in the range of the roll speed of 5 to 90 m/min was 1.42 × 10⁵ to 8.95 × 10⁴ W/m²·K. The cooling rate was calculated using a method based on the results of deriving the temperature change of the molten metal and the roll, using the estimated heat transfer coefficient. The DAS was estimated from the relationship between the cooling rate and DAS, and compared with the experimental value. When the magnesium alloy is manufactured by the melt drag method, the cooling rate of the thin plate is in the range of about 1.4 × 10³ to 1.0 × 10⁴ K/s.

• Textile Coloration and Finishing
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• v.34 no.4
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• pp.241-249
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• 2022

As for military backpacks in Korea, utility backpack products equipped with various functions along with comfort and convenience are being developed. As a result, the volume and weight of the backpack increase, and many lightweight studies of the materials forming the backpack are being conducted. This study is a basic study on frame lightweight using fiber-reinforced composites to deal with aluminum, a back frame that maintains the shape of a backpack and provides stability when worn by combatants. As is known, only fiber-reinforced composites have sufficient light weight and mechanical properties, but the mechanical properties were reviewed by drilling holes to maximize the light weight. Tensile strength and flexural strength were measured by drilling 6mm, 12mm, 18mm, and 24mm holes, and the tensile strength and flexural strength were measured when 1, 3, 5, and 7 holes of 12mm were increased. As a result, even when the number of holes was increased, tensile strength did not change significantly, and the flexural strength showed to be higher in the case of 3 holes and 5 holes than in the case of 1 hole.

• Elastomers and Composites
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• v.59 no.2
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• pp.51-63
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• 2024

Polypropylene (PP) is a commodity plastic that is widely used owing to its cost-effectiveness, lightweight nature, easy processability, and outstanding chemical and thermomechanical characteristics. However, the imperative to address energy and environmental crises has spurred global initiatives toward a circular economy, necessitating sustainable alternatives to traditional fossil-fuel-derived plastics. In this study, we conducted a series of comparative investigations of bio-based polypropylene (bio-PP) blends with current PP of the same and different grades. An extrusion-based processing methodology was employed for the bio-PP composites. Talc was used as an active filler for the preparation of the composites. A comparative analysis with the current petroleum-based PP indicated that the thermal properties and tensile characteristics of the bio-PP blends and composites remained largely unaltered, signifying the feasibility of bio-PP as a potential substitute for the current PP. To achieve a higher Young's modulus, elongation at break (EAB), and melt flow index (MFI), we prepared different composites of PP of different grades and bio-PP with varying talc contents. Interestingly, at higher biomass contents, the composites exhibited higher MFI and EAB values with comparable Young's moduli. Notably, the impact strengths of the composites with various biomass and talc contents remained unaltered. In-depth investigations through surface analysis confirmed the uniform dispersion of talc within the composite matrix. Furthermore, the moldability of the bio-PP composites was substantiated by comprehensive rheological property assessments encompassing shear rate and shear viscosity. Thus, from these outcomes, the fabricated bio-PP-based composites could be an alternative to petroleum-based PP composites for sustainable automobile applications.

• BioChip Journal
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• v.16
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• pp.82-98
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• 2020

We report a quantitative and systematic method for determining 3D-printing and surface-treatment conditions that can help improve the optical quality of direct-printed microfluidic devices. Digital light processing (DLP)-stereolithography (SLA) printing was extensively studied in microfluidics owing to the rapid, one-step, cleanroom-free, maskless, and high-definition microfabrication of 3D-microfluidic devices. However, optical imaging or detection for bioassays in DLP-SLA-printed microfluidic devices are limited by the translucence of photopolymerized resins. Various approaches, including mechanical abrasions, chemical etching, polymer coatings, and printing on transparent glass/plastic slides, were proposed to address this limitation. However, the effects of these methods have not been analyzed quantitatively or systematically. For the first time, we propose quantitative and methodological determination of 3D-printing and surface-treatment conditions, based on optical-resolution analysis using USAF 1951 resolution test targets and a fluorescence microbead slide through 3D-printed coverslip chips. The key printing parameters (resin type, build orientation, layer thickness, and layer offset) and surface-treatment parameters (grit number for sanding, polishing time with alumina slurry, and type of refractive-index-matching coatings) were determined in a step-wise manner. As a result, we achieved marked improvements in resolution (from 80.6 to 645.1 lp/mm) and contrast (from 3.30 to 27.63% for 645.1 lp/mm resolution). Furthermore, images of the fluorescence microbeads were qualitatively analyzed to evaluate the proposed 3D-printing and surface-treatment approach for fluorescence imaging applications. Finally, the proposed method was validated by fabricating an acoustic micromixer chip and fluorescently visualizing cavitation microstreaming that emanated from an oscillating bubble captured inside the chip. We expect that our approach for enhancing optical quality will be widely used in the rapid manufacturing of 3D-microfluidic chips for optical assays.

• Food Science and Preservation
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• v.15 no.6
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• pp.847-851
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• 2008

The handling and processing of agricultural products in Korea is done manually. Small plastic boxes, nets, and corrugated cardboard boxes are used as containers during harvesting, sorting and other product handling operations. However, these practices are labor-intensive, time-consuming, require various kinds of packing materials, and are expensive because of high operating costs. To overcome these problems, the use of pallet bins with pre-cooling and storage features for handling and processing bulk farm products was investigated. The airflow resistances through bulk potato, onion and mandarin stocks were measured, and the pallet bins and a pressure pre-cooling device were manufactured. The opening ratio, bed depth and airflow rate through bulk potato, onion and mandarin in the pallet bin were defined with regression equations. The cooling rates of bulk potato, onion and mandarin were 0.8C/h ($21.7{\rightarrow}0C$, 14.5 h), 0.4C/h ($15.4{\rightarrow}.0C$, 32.2 h) and 0.7C/h ($13.7{\rightarrow}C$, 18.8 h), respectively, with the pressure pre-cooling system. Temperature deviances for storage of bulk potato, onion and mandarin were 0.12C, 0.12C and 0.17C, respectively.

• Korean Journal of Fisheries and Aquatic Sciences
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• v.17 no.6
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• pp.499-505
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• 1984

For the purpose of obtaining basic data which can be applied to processing of retort pouched shell-fishes, retort pouched seasoned baby clam was prepared. After sand and mud were removed, and then steamed baby clams were shucked. Baby clam meats were seasoned with the mixed seasoning powder containing $3\%$ of sugar, $2.5\%$ of salt, $12\%$ of sorbitol, $0.5\%$ of monosodium glutamate and $10\%$ of smoke flavor, and then dried at $35-40^{\circ}C$ for 3 hours. After dried, the meats were vacuum packed in plastic film bag (polyester/nylon/unoriented polyproylene; $12{\mu}m/15{\mu}m/50{\mu}m,\;15{\times}17cm$), and sterilized for 12 minutes in a hot water circulating sterilzer at $120^{\circ}C$, The factors such as pH, VBN, moisture content water activity, color value (L, a, b), texture, TBA value and viable bacterial count of products were determined during storage at room temperture ($20{\pm}3^{\circ}C$). The results showed that the product could be preserved in a good condition for 120 days at $20{\pm}3^{\circ}C$. Judging from the scores of sensory evaluation on flavor, the product added smoke flavor as seasoning was the most desirable.