• Title/Summary/Keyword: Physiochemical Analysis

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Characterization of Electrospun Juniperus Chinensis Extracts Loaded PU Nanoweb (전기방사를 이용한 향나무 추출물 함유 PU 나노웹의 특성)

  • Kim, Jeong-Hwa;Lee, Jung Soon
    • Journal of the Korean Society of Clothing and Textiles
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    • v.41 no.1
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    • pp.131-140
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    • 2017
  • Uniform nanofibers of polyurethane with different content of Juniperus Chinensis extracts (JCE) were successfully prepared by the electrospinning method. We investigated physiochemical properties of prepared compound nanoweb according to various concentrations of Juniperus Chinensis extracts using a Fourier transform infrared (FT-IR) spectrometer, X-ray diffractometer (XRD), thermogravimeter (TGA), and differential scanning calorimeter (DSC). The antibacterial activity of the JCE loaded PU nanofiber was conducted using the disk diffusion test against Gram-positive and Gram-negative bacteria. JCE was induced in the infrared spectra in the absorption band of PU/JCE nanowebs at $3,300cm^{-1}$, $2,960cm^{-1}$, $1,400-1,600cm^{-1}$, and $1,050cm^{-1}$. Thermal stability decreased with increasing JCE content in the PU/JCE nanowebs. The DSC curve of the PU nanoweb shows an endotherm peak at $420^{\circ}C$; in addition, the peak also became smaller and broader with increasing JCE content. The diffraction intensities of PU observed at 2 theta of $20^{\circ}$ decreased with the increasing amount of JCE in the compound nanoweb. In addition, the crystal intensities of the compound nanowebs also decreased along with the JCE content. Structural analysis indicates that JCE and PU are miscible. Juniperus Chinensis incorporated PU nanofibers demonstrated excellent antibacterial properties against both Gram-positive and Gram-negative bacteria.

Quality Characteristics of Brown Rice Dasik Addition of White, Red and Black Ginseng Powder (백삼, 홍삼 및 흑삼 분말 첨가에 따른 현미다식의 품질 특성)

  • Kim, Ae-Jung;Han, Myung-Ryun;Joung, Kyung-Hee;Kang, Shin-Jeong
    • The Korean Journal of Food And Nutrition
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    • v.22 no.1
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    • pp.63-68
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    • 2009
  • Powders prepared from three different varieties Korean Ginsengs(white, red and black) are readily available ingredients and are consumed daily by many Korean as a functional food material. These variants of Ginsengs are known to exert a variety of physiological effects. Therefore, in this study, we assessed the physiochemical characteristics of Korean Ginseng Dasik prepared with different 3 types of Ginseng powder. We conducted a sensory evaluation analysis, and assessed the mechanical characteristics, Hunter's color values, and general compositions of 3 types of Korean Ginseng Dasik stored at room temperature(20$^{\circ}C$). The results of our sensory evaluation showed that there were significant differences in the color, taste and overall quality of the samples(p<0.05), but there were no significant differences in odor or texture. With regard to the mechanical properties of the samples, we noted significant differences in he Hardness, Cohesiveness, Gumminess and Chewiness of the samples(p<0.05), but no differences in springiness were detected. The luminance of the black Ginseng Dasik was significantly less than that of the red, white, and control samples(p<0.05), We noted significant differences in Hunter's b values, but no significant differences in Hunter's a values among the samples were detected. No significant differences in the general compositions of the samples were noted. In conclusion, red Ginseng Dasik among the samples evaluated herein, has the most commercial value.

Comparison of Physicochemical Properties and Malonyl Ginsenoside Contents between White and Red Ginseng (백삼 및 홍삼의 이화학적 특성 및 말로닐 진세노사이드 함량 비교)

  • Oh, Myeong Hwan;Park, Young Sik;Lee, Hwan;Kim, Na Young;Jang, Young Boo;Park, Ji Hun;Kwak, Jun Young;Park, Young Soon;Park, Jong Dae;Pyo, Mi Kyung
    • Korean Journal of Pharmacognosy
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    • v.47 no.1
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    • pp.84-91
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    • 2016
  • Korean ginseng (Panax ginseng C. A. Meyer) has been used as a traditional herbal medicine in East Asia and is very popular in the world, because of its health benefits. To comparison of pharmacological components and physiochemical properties between white and red ginseng from same body, we analyzed ginsenoside and malonyl ginsenoside, ash, crude lipid/protein, fatty acid, mineral contents, total/reducing sugar, and total phenolic and acidic polysaccharide contents. The general components did not show any significant difference between white and red ginseng. Whereas, the content of neutral ginsenoside $Rb_1$, $Rb_2$, Rc and Rd were higher in red ginseng than those of white ginseng. However, malonyl ginsenoside such as $m-Rb_1$, $m-Rb_2$, m-Rc and m-Rd in white ginseng were similar to neutral ginsenoside $Rb_1$, $Rb_2$, Rc and Rd in white ginseng and far higher than those of red ginseng. These results exhibit that malonyl ginsenosides were converted to neutral ginsenosides in steaming process for red ginseng. So, we suggest that malonyl ginsenoside are necessary to applies in ginsenoside analysis of Korean ginseng.

Processing Optimization and Antioxidant Activity of Chiffon Cake Prepared with Tomato Powder (토마토 분말 첨가 시폰 케이크의 제조조건 최적화 및 품질 특성)

  • Paik, Jaeeun;Kim, Soojeong;An, Hyunae;Joo, Nami
    • Journal of the Korean Dietetic Association
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    • v.19 no.1
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    • pp.1-13
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    • 2013
  • The purpose of this study was to determine the optimal mixing condition of tomato powder and sugar for producing chiffon cake. The experiment was designed according to the central composite design of response surface, which yielded ten experimental points, including two replicates. Physiochemical and sensory properties were measured, and theses values applied to mechanical models. A canonical form and perturbation plot showed the influence of each ingredient on the final product mixture. The results of the physiochemical analysis of each sample showed significant differences in sweetness (P<0.01), color L (P<0.001), color a (P<0.001), color b (P<0.05), hardness (P<0.05), and cohesiveness (P<0.01). The sensory measurements were significantly different in color (P<0.05), appearance (P<0.05), flavor (P<0.05), sweetness (P<0.01), moistness (P<0.05), and overall acceptability (P<0.05). The optimal formulation, calculated using the numerical and graphical method, was determined to be 59.27 g tomato powder and 285.66 g sugar. The sensory evaluation showed significantly higher preferences in the color, flavor, appearance, texture, sweetness, tenderness, moistness and overall quality of the optimized chiffon cake compared to the controlled chiffon cake. The optimized chiffon cake also showed a high antioxidative activity compared to the controlled chiffon cake. Our results show that chiffon cake prepared with tomato powder enhances sensory characteristics and antioxidative activity.

Principle Component Analysis on Electrokinetic Measurements for Amphoteric Fibers/Acid Dye System (앰포테릭섬유/산성염료계의 계면동전압 측정치에 대한 PCA)

  • Park, Byeong-Gi
    • Journal of Korean Society for Quality Management
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    • v.13 no.1
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    • pp.26-30
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    • 1985
  • In the light of the properties of colloids, in the surface of disperse phase and dispersion, there exist specific characters such as adsorption or electric double layer, which seems to play important roles in determining the physiochemical properties in the dyeing system. Nylon, wool and silk, the typical amphoteric fibers were dyed with Acid dye and various combinations were prepared by combining pH, temperature and dye concentration, in order to generate flowing electric potential which were measured by microviolt meter and specific conductivity meter. The results were transformed to Zeta potential by Helmholtz-Smoluchowski formular and to surface electric charge density by Suzawa formular, surface dye amount, and effective surface area of fibers, and these data were statistically analysed by principle component analysis.

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Synthesis of Spinel Phase ${LiMn_2}{O_4}$ and its Activation by Hydrogen Reduction (스피넬상 ${LiMn_2}{O_4}$의 합성과 수소환원에 의한 활성화)

  • 이동석;류대선;임병오;이풍헌
    • Journal of the Korean Ceramic Society
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    • v.37 no.6
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    • pp.564-568
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    • 2000
  • Spinel LiMn2O4 catalyst with submicron and single phase particles was synthesized at 48$0^{\circ}C$ for 12 hr in air by a sol-gel method. The spinel LiMn2O4 was deoxidized by hydrogen at various temperatures. Effects of physiochemical properties of the catalyst reduced by hydrogen were examined with X-ray diffractometer, thermogravimetric analysis and scanning electron microscope. The decomposition rate of carbon dioxide was measrued using the catalyst deosidized at 35$0^{\circ}C$.

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Purification and Properties of Biosurfactant from Pseudomonas aeruginosa KK-7 (Pseudomonas aeruginosa가 생산하는 biosurfactant의 분리 및 특성)

  • 김대원;김민주;강상모
    • Microbiology and Biotechnology Letters
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    • v.23 no.3
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    • pp.337-345
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    • 1995
  • Biosurfactants produced by Pseudomonas aeroginosa KK-7 were purified and their properties were studied. The bacterial surfactant was seperated into two sorts of biosufactants (Type I, 11) by silica gel column chromatograpgy. On the basis of physiochemical analysis, Type I was found to be mixture of two glycolipids with M.W. 800, and Type II was peptide with M.W. 1300. The Type 11 biosurfactant was compose of glutamic acid, proline, glycine, leucine, histidine. The crude extract was used to dertermine some properties as a surfactant. The biosurfactant had the properties as stronger emulsification agent and a stronger stabilizing agent emulsion than any other surfactants tested.

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Effects of Adding Sugars and Lipids on Characteristics of Cooked Rice (당류 및 유지류 첨가가 밥의 특성에 미치는 영향)

  • 권혜진;김영아
    • Korean journal of food and cookery science
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    • v.15 no.2
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    • pp.163-170
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    • 1999
  • To investigate the effect of adding sugars and lipids on characteristics of cooked rice, the solubility, swelling power, blue value, amylogram and sensory evaluation characteristics of cooked rices with 0.5, 1.0, 1.5, 2.0% level of sugars and lipids additives were measured. The solubility, swelling power and blue value of cooked rice with sugars were increased as the more sugars were added. Those parameters of the cooked rice with isomalto oligosaccharide were higher than sucrose. The solubility decreased as the more lipids were added. The swelling power decreased as the more lipids were added. As the result of amylograph analysis, addition of isomalto oligosaccharide accelerates the gelatinization and retards the retrogradation. In sensory evaluation, the cooked rice with 0.5% level of sucrose and isomalto oligosaccharide were showed better acceptability than the others. In conclusion, the additions of sugars and lipids affect characteristics of cooked rice. Especially, the cooked rice with 0.5% isomalto oligosaccharide was showed the best physiochemical and sensory properties.

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Molecular Differentiation of Panax Species by RAPD Analysis

  • Shim, Young-Hun;Choi, Jung-Ho;Park, Chan-Dong;Lim, Chul-Joo;Cho, Jung-Hee;Kim, Hong-Jin
    • Archives of Pharmacal Research
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    • v.26 no.8
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    • pp.601-605
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    • 2003
  • Traditional taxonomic methods used for the identification and differentiation of ginsengs rely primarily on morphological observations or physiochemical methods, which cannot be used efficiently when only powdered forms or shredded material is available. Randomly amplified polymorphic DNA (RAPD) was used to determine the unique DNA profiles that are characteristic not only of the genus Panax but also of various Panax subgroups collected from five different countries. RAPD results of OP-5A primer showed a specific single band that is characteristic of all ginseng samples. RAPD results of OP-13B primer demonstrated that OP-13B primer could be used as a unique RAPD marker to differentiate Panax species. These results support that this approach could be applied to distinguish Korean Ginseng (Panax ginseng) from others at the molecular level.

Qualities of Soybean Dasik with Added Saltwort (Salicornia herbacea L.) Powder (함초 분말을 첨가한 콩다식의 품질특성)

  • Kim, Myung-Hee;Hong, Geum-Ju
    • Journal of the Korean Society of Food Culture
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    • v.26 no.5
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    • pp.501-505
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    • 2011
  • Soybean powder is a readily-available food ingredient. Furthermore, saltwort powder is an herb with various physiological effects. Therefore, in this study we examined the physiochemical characteristics of soybean dasik prepared with 0, 4, 8, and 12% saltwort powder. We measured Hunter's color values, mechanical characteristics, and sensory qualities. The result of each analysis is as follows. There were not significant differences between the moisture content of the control group and the groups with saltwort powder. The ash content increased while the fat and protein content decreased as the ratio of saltwort powder increased (p<0.001). In the analysis of color differences, the L, a, and b values decreased as the ratio of saltwort powder increased (p<0.001). The hardness (p<0.001) of the groups increased as the ratio of saltwort powder increased, but adhesiveness decreased. Sensory evaluation data showed that softness, hardness, and chewiness decreased while color increased as the ratio of saltwort powder increased. Finally, aroma, sweet taste, nutty taste, and overall acceptability was shown to be best for the 4% addition group.