• Title/Summary/Keyword: Physical characterization

Search Result 637, Processing Time 0.025 seconds

Characterization of Compacted and Pressureless Sintered Parts for Molybdenum Oxide Powder according to Hydrogen Reduction Temperature (수소 환원 온도에 따른 몰리브덴 산화물의 성형 및 상압소결특성 평가)

  • Jong Hoon Lee;Kun-Jae Lee
    • Journal of Powder Materials
    • /
    • v.31 no.4
    • /
    • pp.336-341
    • /
    • 2024
  • Molybdenum, valued for its high melting point and exceptional physical and chemical properties, is studied in diverse fields such as electronics, petrochemicals, and aviation. Among molybdenum oxides, molybdenum dioxide stands out for its higher electrical conductivity than other transition metal oxides due to its structural characteristics, exhibiting metallic properties. It is applied as pellets to gas sensors, semiconductors, and secondary batteries for its properties. Thus, research on molybdenum dioxide compaction and pressureless sintering is necessary, yet research on pressureless sintering is currently insufficient. This study synthesized MoO3 powder via solution combustion synthesis and reduced it using the 3% hydrogen/argon gas mixture to investigate the effect of reduction temperature on the powder. Additionally, the reduced powder was compacted and subjected to pressureless sintering with temperature as a variable. The density and the microstructure of brown parts were analyzed and discussed.

Elastic Imaging of Material Surface by Ultrasonic Atomic Force Microscopy (초음파 원자 현미경을 이용한 재료 표면의 탄성 이미지화)

  • Kim, C.S.;Park, Tae-Sung;Park, It-Keun;Lee, Seung-Seok;Lee, C.J.
    • Journal of the Korean Society for Nondestructive Testing
    • /
    • v.29 no.4
    • /
    • pp.293-298
    • /
    • 2009
  • The ultrasonic atomic force microscope(UAFM) has been developed in order to enhance the characterization technology for nano-scale surface combining ultrasonic property to atomic force microscope. This UAFM technique enables elasticity imaging due to the physical properties on the heterogeneous surface in addition to the novel topography of surface height in the nano-surface layer. In this study, the prototype UAFM system was constructed and applied to several materials, silicon deposited wafer, spherodized cold heading steel, and carbon fiber reinforced plastic specimen. Clear elastic contrast was successfully obtained using this developed prototype UAFM.

An Accurate Radio Channel Model for Wireless Sensor Networks Simulation

  • Alejandro Martfnez-Sala;Jose-Maria Molina-Garcia-Pardo;Esteban Egea-Lopez;Javier Vales-Alonso;Leandro Juan-Llacer;Joan Garcia-Haro
    • Journal of Communications and Networks
    • /
    • v.7 no.4
    • /
    • pp.401-407
    • /
    • 2005
  • Simulations are currently an essential tool to develop and test wireless sensor networks (WSNs) protocols and to analyze future WSNs applications performance. Researchers often simulate their proposals rather than deploying high-cost test-beds or develop complex mathematical analysis. However, simulation results rely on physical layer assumptions, which are not usually accurate enough to capture the real behavior of a WSN. Such an issue can lead to mistaken or questionable results. Besides, most of the envisioned applications for WSNs consider the nodes to be at the ground level. However, there is a lack of radio propagation characterization and validation by measurements with nodes at ground level for actual sensor hardware. In this paper, we propose to use a low-computational cost, two slope, log-normal path­loss near ground outdoor channel model at 868 MHz in WSN simulations. The model is validated by extensive real hardware measurements obtained in different scenarios. In addition, accurate model parameters are provided. This model is compared with the well-known one slope path-loss model. We demonstrate that the two slope log-normal model provides more accurate WSN simulations at almost the same computational cost as the single slope one. It is also shown that the radio propagation characterization heavily depends on the adjusted model parameters for a target deployment scenario: The model parameters have a considerable impact on the average number of neighbors and on the network connectivity.

DEEP-South: The Progress Report

  • Moon, Hong-Kyu;Kim, Myung-Jin;Park, Jintae;JeongAhn, Youngmin;Yang, Hongu;Lee, Hee-Jae;Kim, Dong-Heun;Roh, Dong-Goo;Choi, Young-Jun;Yim, Hong-Suh;Lee, Sang-Min;Kwak, SungWon
    • The Bulletin of The Korean Astronomical Society
    • /
    • v.43 no.1
    • /
    • pp.42.1-42.1
    • /
    • 2018
  • Deep Ecliptic Patrol of the Southern Sky (DEEP-South) observation is being made during the off-season for exoplanet survey, using Korea Microlensing Telescope Network (KMTNet). An optimal combination of its prime focus optics and the 0.3 billion pixel CCD provides a four square degrees field of view with 0.4 arcsec/pixel plate scale which is also best suited for small body studies. Normal operation of KMTNet started in October 2015, and a significant portion of the allocated telescope time for DEEP-South is dedicated to targeted observation, Opposition Census (OC), of near-Earth asteroids for physical and taxonomic characterization. This is effectively achieved through multiband, time series photometry using Johnson-Cousins BVRI filters. Uninterrupted monitoring of the southern sky with KMTNet is optimized for spin characterization of a broad spectrum of asteroids ranging from the near-Earth space to the main-belt, including binaries, asteroids with satellites, slow/fast- and non-principal axis-rotators, and thus is expected to facilitate the debiasing of previously reported lightcurve observations. Our software subsystem consists of an automated observation scheduler, a pipelined data processing system for differential photometry, and an easy-to-use lightcurve analysis toolkit. Lightcurves, spin periods and provisional determination of class of asteroids to which the lightcurve belongs will be presented, using the dataset from first year operation of KMTNet. Our new taxonomic classification scheme for asteroids will also be summarized.

  • PDF

Rapid Characterization and Prediction of Biomass Properties via Statistical Techniques

  • Cho, Hyun-Woo
    • Clean Technology
    • /
    • v.18 no.3
    • /
    • pp.265-271
    • /
    • 2012
  • The use of renewable energies has been required to diminish the dependency on fossil fuels. As one of clean energy sources biomass has been extensively studied because various biomass resources necessitated rapid characterization of their chemical and physical properties in an on-line or real-time basis. For such an analysis near-infrared (NIR) spectroscopy has been successfully applied because of its non-invasive and informative characteristics. In this work, the applicability of nonlinear chemometric techniques based on biomass near infrared (NIR) data is evaluated for the rapid prediction of ash/char contents in different types of biomass. The prediction results of various prediction models and the effect of using preprocessing methods for NIR data are compared using six types of biomass NIR data. The results showed that nonlinear prediction models yielded better prediction performance than linear ones. It also turned out that by adopting the use of proper preprocessing methods the performance of prediction of biomass properties improved.

CND41, a DNA-binding protein in chloroplast nucleoid, and its function

  • Sato, Fumihiko;Murakami, Shinya;Chatani, Hiroshi;Nakano, Takeshi
    • Proceedings of the Botanical Society of Korea Conference
    • /
    • 1999.07a
    • /
    • pp.51-56
    • /
    • 1999
  • Plastids, which are organelles unique to plant cells, bear their own genome that is organized into DNA-protein complexes (nucleoids). Regulation of gene expression in the plastid has been extensively investigated because this organelle plays an important role in photosynthesis. Few attempts, however, have been made to characterize the regulation of plastid gene expression at the chromosomal structure, using plastid nucleoids. In this report, we summarize the recent progress in the characterization of DNA-binding proteins in plastids, with special emphasis on CND41, a DNA binding protein, which we recently identified in the choloroplast nucleoids from photomixotrophically cultured tobacco cells. CND41 is a protein of 502 amino acids which consisted of a transit peptide of 120 amino acids and a mature protein of 382 amino acids. The N-terminal of the 'mature' protein has lysine-rich region which is essential for DNA-binding. CNA41 also showed significant identities to some aspartyl proteases. Protease activity of purified CND41 has been recently confirmed and characterized. On the other hand, characterization of accumulation of CND41 both in wild type and transgenic tobacco with reduced amount of CND41 suggests that CND41 is a negative regulator in chloroplast gene expression. Further investigation indicated that gene expression of CND41 is cell-specifically and developmentally regulated as well as sugar-induced expression. The reduction of CND41 expression in transgenic tobacco also brought the stunted plant growth due to the reduced cell length in stem. GA3 treatment on apical meristem reversed the dwarf phenotype in the transformants. Effects of CND41 expression on GA biosynthesis will be discussed.

  • PDF

Phase Error Accumulation Methodology for On-chip Cell Characterization (온 칩 셀 특성을 위한 위상 오차 축적 기법)

  • Kang, Chang-Soo;Im, In-Ho
    • 전자공학회논문지 IE
    • /
    • v.48 no.2
    • /
    • pp.6-11
    • /
    • 2011
  • This paper describes the design of new method of propagation delay measurement in micro and nanostructures during characterization of ASIC standard library cell. Providing more accuracy timing information about library cell (NOR, AND, XOR, etc.) to the design team we can improve a quality of timing analysis inside of ASIC design flow process. Also, this information could be very useful for semiconductor foundry team to make correction in technology process. By comparison of the propagation delay in the CMOS element and result of analog SPICE simulation, we can make assumptions about accuracy and quality of the transistor's parameters. Physical implementation of phase error accumulation method(PHEAM) can be easy integrated at the same chip as close as possible to the device under test(DUT). It was implemented as digital IP core for semiconductor manufacturing process($0.11{\mu}m$, GL130SB). Specialized method helps to observe the propagation time delay in one element of the standard-cell library with up-to picoseconds accuracy and less. Thus, the special useful solutions for VLSI schematic-to-parameters extraction (STPE), basic cell layout verification, design simulation and verification are announced.

Effect of Hydrogen Ratio and Tin Addition on the Coke Formation of Platinum Catalyst for Propane Dehydrogenation Reaction (프로판 탈수소화 반응용 백금촉매의 코크 생성에 미치는 수소비와 주석첨가의 영향)

  • Kim, Soo Young;Kim, Ga Hee;Koh, Hyoung Lim
    • Clean Technology
    • /
    • v.22 no.2
    • /
    • pp.82-88
    • /
    • 2016
  • The loss of activity by coke is an important cause of catalyst deactivation during industrial operation. In this study, hydrogen ratio of reaction condition, which has influenced on coke formation over Pt-Sn catalyst, and regeneration of catalysts activity by coke burning, Pt sintering of coke burning as coke contents, effects of coke formation and deactivation with different Sn contents were confirmed. Pt-Sn-K catalyst supported on θ-alumina and γ-alumina was prepared progressively. Activity of regenerated catalyst for propane dehydrogenation was compared with fresh catalyst by coke burning, after propane dehydrogenation was carried out with different hydrogen ratio at 620 ℃ on fresh catalyst. Regenerated catalyst’s physical characterization such as BET, coke analysis and XRD was investigated. Through catalytic activity test and characterization, Sn contents of catalyst and hydrogen ratio in feed stream could affect coke formation on catalyst surface. Excessive coke makes loss of activity and Pt sintering during air regeneration process.

Detection and Characterization of a Lytic Pediococcus Bacteriophage from the Fermenting Cucumber Brine

  • Yoon, Sung-Sik;Baprangou-Poueys Roudolphe;Jr Fred Breidt;Fleming Henry P.
    • Journal of Microbiology and Biotechnology
    • /
    • v.17 no.2
    • /
    • pp.262-270
    • /
    • 2007
  • Of the twelve lytic bacteriophages recovered from five different fermenting cucumber tanks that were inoculated with Pediococcus sp. LA0281, a lytic phage, ${\phi}ps05$, was characterized in the present study. The plaques were mostly clear and round-shaped on the lawn of starter strain, indicating lytic phage. Overall appearance indicated that it belongs to the Siphoviridae family or Bradley's group B1, with a small isometric head and a flexible noncontractile tail with swollen base plate. The average size was found to be 51.2 nm in head diameter and 11.6 nm wide ${\times}$ 129.6 nm long for the tail. The single-step growth kinetics curve showed that the eclipse and the latent period were 29 min and 34 min, respectively, and an average burst size was calculated to be 12 particles per infective center. The optimum proliferating temperature ($35^{\circ}C$) was slightly lower than that of cell growth ($35\;to\;40^{\circ}C$). The structural proteins revealed by SDS-PAGE consisted of one main protein of 33 kDa and three minor proteins of 85, 58, and 52 kDa. The phage genome was a linear double-stranded DNA without cohesive ends. Based on the single and double digestion patterns obtained by EcoRI, HindIII, and SalI, the physical map was constructed. The overall size of the phage genome was estimated to be 24.1 kb. The present report describes the presence of a lytic phage active against a commercial starter culture Pediococcus sp. LA0281 in cucumber fermentation, and a preliminary study characterizes the phage on bacterial successions in the process of starter-added cucumber fermentation.

Infrared Imaging and a New Interpretation on the Reverse Contrast Images in GaAs Wafer (GaAs 웨이퍼의 적외선 영상기법 및 콘트라스트 반전 영상에 대한 새로운 해석)

  • Kang, Seong-jun
    • Journal of the Korea Institute of Information and Communication Engineering
    • /
    • v.20 no.11
    • /
    • pp.2085-2092
    • /
    • 2016
  • One of the most important properties of the IC substrate is that it should be uniform over large areas. Among the various physical approaches of wafer defect characterization, special attention is to be payed to the infrared techniques of inspection. In particular, a high spatial resolution, near infrared absorption method has been adopted to directly observe defects in semi-insulating GaAs. This technique, which relies on the mapping of infrared transmission, is both rapid and non-destructive. This method demonstrates in a direct way that the infrared images of GaAs crystals arise from defect absorption process. A new interpretation is presented for the observed reversal of contrast in the infrared absorption of nonuniformly distributed deep centers, related to EL2, in semi-insulating GaAs. The low temperature photoquenching experiment has demonstrated in a direct way that the contrast inverse images of GaAs wafers arise from both absorption and scattering mechanisms rather than charge re-distribution or local variation of bandgap.