• 제목/요약/키워드: Phase response curve

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Determination of Fluorescent Whitening Agents in Paper Materials by Ion-Pair Reversed-Phase High-Performance Liquid Chromatography

  • Kim, Jeong Soo;Kim, Do Hwan;Kim, Keon
    • Bulletin of the Korean Chemical Society
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    • 제33권12호
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    • pp.3971-3976
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    • 2012
  • A simple method was developed for the analysis of seven stilbene-type fluorescent whitening agents (FWAs) in paper materials by ion-pair reversed-phase high-performance liquid chromatography with fluorescence detection. These stilbene-type FWAs included two disulfonate, two tetrasulfonate, and three hexasulfonate compounds. After optimization of chromatographic conditions, the FWAs were satisfactorily separated using a reversed-phase column (RP-18) with the following isocratic mobile phase: methanol-water (60:40) containing 17.5 mM TBABr and 10 mM citrate buffer (pH = 7.0). The calibration plot was linear in the range from 5 to 500 ng/mL for two disulfo-FWAs and from 1 to 500 ng/mL for the other five FWAs. Precision levels of the calibration curve as indicated by RSD of response factors were 1.2 and 8.1%. Limits of quantitation (LOQ) ranged from 1.2 to 11 ng/mL.

개선된 모델 축소 방법에 의한 범용적 제어기 설계 (Design of Generalized Controller by Improved Model Reduction)

  • 조준호;황형수
    • 전자공학회논문지SC
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    • 제44권5호
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    • pp.1-10
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    • 2007
  • 본 논문은 개선된 모델 축소 알고리즘을 이용하여 범용적 제어기 설계에 대해서 제안했다. 개선된 모델 축소 알고리즘은 모델의 과도상태와 정상상태 응답을 고려하여 주파수 영역에서 구하였다. 범용적 제어기 설계는 위상여유와 등 제동의 특성을 만족하는 PID 제어기와 2차 지연 모델에 대하여 촤적화 PID 제어기 설계에 대해서 제안 하였다. 시뮬레이션을 통하여 다양한 공정에 대하여 본 논문에서 제안한 방법을 적용하여, 모델축소 방법의 정확성 및 제어기 성능의 개선을 보였다.

Nonlinear response of complex fluids under LAOS(large amplitude oscillatory shear) flow

  • Ahn, Kyung-Hyun;Kyu Hyun;Nam, Jung-Gun;Manfred Wilhelm;Lee, Seung-Jong
    • Korea-Australia Rheology Journal
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    • 제15권2호
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    • pp.97-105
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    • 2003
  • In the previous paper (Hyun et al.,2002), we have investigated the shape of storage modulus (G') and loss modulus (G") of complex fluids under large amplitude oscillatory shear (LAOS) flow. As the strain amplitude increases, owever, the stress curve becomes distorted and some important information may be smothered during data processing. Thus we need to investigate the stress data more precisely and systematically. In this work, we have obtained the stress data using high performance ADC (analog digital converting) card, and investigated the nonlinear response of complex fluids, 4wt% xanthan gum (XG), 2 wt% PVA/ 1 wt% Borax, and 1 wt% hyaluronic acid (HA) solutions, using Fourier transformation (FT) rheology. Comparing the strain signals in time domain with FT parameters in frequency domain, we could illustrate the sensitivity and importance of FT rheology. Diverse and unique stress patterns were observed depending on the material system as well as flow environment. It was found that they are not the outcome of experimental deficiency like wall slip but characteristics of the material system. When nonlinear response of complex fluids is analyzed, the intensity and phase angle of higher harmonic contributions should be considered together, and the shape of the stress signal was found to be strongly dependent upon phase angle.ngle.

FFC Design for PI Flow Control System Designed by CDM

  • Oh, Kyu-Kwon;Yu, Kee-Ho
    • 제어로봇시스템학회:학술대회논문집
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    • 제어로봇시스템학회 2001년도 ICCAS
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    • pp.151.3-151
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    • 2001
  • A design of PI controller to be used to control the first-order lag plus dead time process, such as a flow process, by the coefficient diagram method (CDM) is investigated. The factor of the dead time of process is first approximated to be the first-order by the Pade approximation. The response of the flow control system designed by CDM satisfy both transient and steady state specifications. However, the transient response generally still has long rise time. In order to improve the speed of the system response, a feedforward controller (FFC) is added into the PI control system. The structure of the FFC is a phase lead structure with two designed parameters and one derivative time obtained from the reaction curve of the flow process ...

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비선형 2자유도계의 비감쇠 강제진동 연구 (A Sudy on the Undamped Forced Vibration of Nonlinear Two-Degree-of-Freedom Systems)

  • 박철희;박선재;윤영석
    • 대한기계학회논문집
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    • 제12권2호
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    • pp.193-199
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    • 1988
  • 본 연구의 목적은 SCPA방법을 이용한 비선형 2자유도 비감쇠계의 해석을 통하여 응답곡선을 구하고, 그 응답곡선의 분기현상을 규명함에 있다. 결과의 비교를 위하여 4차의 Runge-Kutta방법을 이용한 수치실험을 수행하였다.

Finite Element Modeling and Nonlinear Analysis for Seismic Assessment of Off-Diagonal Steel Braced RC Frame

  • Ramin, Keyvan;Fereidoonfar, Mitra
    • International Journal of Concrete Structures and Materials
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    • 제9권1호
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    • pp.89-118
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    • 2015
  • The geometric nonlinearity of off-diagonal bracing system (ODBS) could be a complementary system to covering and extending the nonlinearity of reinforced concrete material. Finite element modeling is performed for flexural frame, x-braced frame and the ODBS braced frame system at the initial phase. Then the different models are investigated along various analyses. According to the experimental results of flexural and x-braced frame, the verification is done. Analytical assessments are performed in according to three dimensional finite element modeling. Nonlinear static analysis is considered to obtain performance level and seismic behaviour, and then the response modification factors calculated from each model's pushover curve. In the next phase, the evaluation of cracks observed in the finite element models, especially for RC members of all three systems is performed. The finite element assessment is performed on engendered cracks in ODBS braced frame for various time steps. The nonlinear dynamic time history analysis accomplished in different stories models for three records of Elcentro, Naghan and Tabas earthquake accelerograms. Dynamic analysis is performed after scaling accelerogram on each type of flexural frame, x-braced frame and ODBS braced frame one by one. The base-point on RC frame is considered to investigate proportional displacement under each record. Hysteresis curves are assessed along continuing this study. The equivalent viscous damping for ODBS system is estimated in according to references. Results in each section show the ODBS system has an acceptable seismic behaviour and their conclusions have been converged when the ODBS system is utilized in reinforced concrete frame.

국가수준 학업성취도 평가의 과학 문항 특성 분석 : 광학 내용을 중심으로 (Analysis on the Characteristics of National Assessment of Educational Achievement (NAEA) Items for Science Subject: With a Focus on Optics)

  • 이봉우;이인호
    • 한국과학교육학회지
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    • 제35권3호
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    • pp.465-475
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    • 2015
  • 본 연구의 목적은 과학과 국가수준 학업성취도 평가에서 물리의 광학 영역 문항의 평가 결과를 분석하고 답지 반응률 분포 곡선을 활용하여 중학생들의 반응 특성을 분석하는 것이다. 이를 위해서 2010년부터 2013년까지 중학생들을 대상으로 시행된 과학과 국가수준 학업성취도 평가의 물리 문항 중 광학 영역에 해당되는 10개 문항을 분석하였다. 분석 결과는 다음과 같다. 첫째, 학생들의 '광학' 영역의 성취수준은 다른 영역(역학, 전자기학)에 비해서는 높았다. 둘째, '빛' 영역에서 '상의 형성'과 관련되어 학생들이 낮은 성취수준을 보였으며, '파동' 영역에서는 '파동의 전파에서 위상의 변화'와 관련되어 낮은 성취수준을 나타내었다. 셋째, 학생들은 상황 의존적인 문제풀이 전략 및 결과를 보이고 있었다. 연구 결과를 바탕으로 광학 개념에 대한 교육과정 수준의 재검토, 기초학력 단계 학생들에 대한 추가적인 교수학습의 필요성, 실제적인 현상 및 상황 중심의 교수학습의 필요성 등의 제언을 논의하였다.

광대역 첩 신호의 진폭 및 위상오차 분석을 통한 IRF 성능 분석 (IRF performance prediction by analyzing of amplitude and phase errors for the wideband Chirp signal)

  • 김동식;김종필;이종환
    • 한국항공우주학회지
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    • 제44권2호
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    • pp.131-138
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    • 2016
  • 본 논문에서는 SAR (Synthetic Aperture Radar)에 사용되는 광대역 첩 신호에 대한 IRF(Impulse Response Function) 성능을 분석하였다. 영상 레이더의 첩 신호에서 영상품질에 크게 영향을 주는 인자는 진폭과 위상으로 크게 분류할 수 있다. 이 값들을 2차 다항식 커브 피팅을 사용하여 선형, 직교, 랜덤 그리고 리플 이득으로 구분할 수 있다. 본 연구에서는 이러한 인자들에 의한 IRF 영향을 분석하고, PSLR(Peak Side Lobe Ratio) 및 ISLR(Integrated Side Lobe Ratio)의 규격을 만족하기 위한 RF 비선형성에 의한 오차 값들의 최소치를 제안하였다.

생리학적인 하중 조건에서 소 상완골 연골의 기계적 특성 (In Situ Mechanical Response of Bovine Humeral Head Articular Cartilage in a Physiological Loading Environment)

  • 박성훈
    • 한국정밀공학회지
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    • 제25권1호
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    • pp.145-150
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    • 2008
  • One of the unresolved questions in articular cartilage biomechanics is the magnitude of the dynamic modulus and tissue compressive strains under physiological loading conditions. The objective of this study was to characterize the dynamic modulus and compressive strain magnitudes of bovine articular cartilage at physiological compressive stress level and loading frequency. Four bovine calf shoulder joints (ages 2-4 months) were loaded in Instron testing system under load control, with a load amplitude up to 800 N and loading frequency of 1 Hz, resulting in peak engineering stress amplitude of ${\sim}5.8\;MPa$. The corresponding peak deformation of the articular layer reached ${\sim}27%$ of its thickness. The effective dynamic modulus determined from the slope of stress versus strain curve was ${\sim}23\;MPa$, and the phase angle difference between the applied stress and measured strain which is equivalent to the area of the hystresis loop in the stress-strain response was ${\sim}8.3^{\circ}$. These results are representative of the functional properties of articular cartilage in a physiological loading environment. This study provides novel experimental findings on the physiological strain magnitudes and dynamic modulus achieved in intact articular layers under cyclical loading conditions.

Sensing Characteristics of Uncoated Double Cladding Long-period Fiber Grating Based on Mode Transition and Dual-peak Resonance

  • Zhou, Yuan;Gu, Zheng Tian;Ling, Qiang
    • Current Optics and Photonics
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    • 제5권3호
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    • pp.243-249
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    • 2021
  • In this paper, the sensing characteristics of a double cladding fiber (DCF) long-period fiber grating (LPFG) to the surrounding refractive index (SRI) are studied. The outer cladding of the DCF plays the role of the overlay, thus, the mode transition (MT) phenomenon of DCF can be induced by etching the outer cladding radius instead of coating overlays. The response characteristics of the effective refractive index (ERI) of the cladding mode to the outer cladding radius are analyzed. It is found that in the MT range, the change rate of ERIs of cladding modes is relatively larger than that for other ranges. Further, based on the features of the mode transition region (MTR), the phase-matching curve of the 11th cladding mode is investigated, and the response of the DCF-LPFG to the SRI is characterized by the change of wavelength intervals between the dual peaks under different outer cladding radii. The numerical simulation results show that the SRI sensitivity is greatly improved, which is available to 3484.0 nm/RIU with the fitting degree 0.998 in the SRI range of 1.33-1.37. The proposed DCF-LPFG can provide new theoretical support for designing the DCF-LPFG refractive index sensor with excellent performances of sensitivity, linearity and structure.