• Bulletin of the Korean Chemical Society
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• 제29권6호
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• pp.1173-1178
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• 2008

A simple and sensitive high-performance liquid chromatographic method was developed for the simultaneous identification of enrofloxacin and its active metabolite ciprofloxacin in chicken muscle. Norflorxacin imprinted polymers synthesized in water-containing systems show high selectivity to enrofloxacin and ciprofloxacin in an aqueous environment. Using these water-compatible imprinted polymers as selective adsorbents in the solid-phase extraction of enrofloxacin and ciprofloxacin from chicken samples, the remaining biological matrix could be quickly washed out from the imprinted column while enrofloxacin and ciprofloxacin were selectively retained and enriched. Analytical separation was performed on a $C_{18}$ column using acetonitrile-water as a mobile phase and fluorescence detection. Good linearity was obtained from 0.8 to 500 ng/g (r > 0.998) with relative standard deviation of less than 3.9%. The mean recoveries of enrofloxacin and ciprofloxacin from chicken muscle were 80.6-94.5% and 77.8-91.8% at three different concentrations. The limits of determinations based on S/N=3 were 0.07 ng/g and 0.09 ng/g, which are below the maximum residue limits established in many countries.

• 한국주조공학회지
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• 제30권3호
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• pp.100-110
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• 2010

The solidification sequence and formation of intermetallic phase of Fe-rich Al-Si-Cu alloy were investigated by using real-time imaging of synchrotron X-ray radiation. Effects of cooling rate during uni-directional solidification on the resultant solidification behavior was also studied in a specially constructed vacuum chamber in the SPring-8 facility. The series of radiographic images were complementarily analyzed with conventional analysis of OM and SEM/EDX for phase identification. Detailed solidification sequence and formation mechanisms of various phases were discussed based on real-time image analysis. The growth rates of $\alpha$-AlFeMnSi and ${\beta}-Al_5FeSi$ were measured in order to understand the growth behavior of each phase. It is suggested that real-time imaging technique can be a powerful tool for the precise understanding of solidification behavior of various industrial materials.

• 전력전자학회논문지
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• 제16권2호
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• pp.191-198
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• 2011

본 논문에서는 영구자석 동기전동기 구동용 인버터 스위치에서 개방성 고장이 발생하여도 구동 성능을 유지하기 위한 고장진단 기법이 제안 되었다. 제안한 고장진단 기법은 확장형 칼만필터에 의해 실시간으로 추정된 고정자 저항이 개방성 고장발생 시 고장발생 위치에 따라서 다르게 추정되는 것을 이용하여 고장을 진단한다. 고장진단을 위한 제어 알고리즘을 별도의 하드웨어 구성없이 기존의 제어 프로그램에 추가함으로써 비용을 저감 시킬 수 있으며 추정된 고정자 저항은 상수 변동에 영향을 받는 제어기의 전동기 상수로 사용함으로써 제어 성능을 향상 시킬 수 있다. 제안한 고장진단 기법의 타당성은 시뮬레이션과 실험을 통하여 검증하였다.

• Journal of Electrical Engineering and Technology
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• 제12권5호
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• pp.1697-1708
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• 2017

This paper proposes an algorithm for the differential protection of an Indirect Symmetrical Phase Shift Transformer (ISPST) by considering the different behaviors of the compensated differential current under internal fault and magnetizing inrush conditions. In this algorithm, a criterion function is defined which is based on the difference of amplitude of the wavelet transformation over a specific frequency band. The function has been used for the discrimination between three phase magnetizing inrush and internal fault condition and requires less than a quarter cycle after disturbance. This method is independent of any coefficient or threshold values of wavelet transformation. The merit of this algorithm is demonstrated by the simulation of different faults in series and excitation unit and magnetizing inrush with varying switching conditions on ISPST using PSCAD/EMTDC. Due to unavailability of in-field large interconnected transformers for such a large number of destructive tests, the results are further verified by Real Time Digital Simulator (RSCAD/RTDS). The proposed algorithm has been compared with the conventional harmonic restraint based method that justifies the application of wavelet transform for differential protection of ISPST. The proposed algorithm has also been verified for different rating of ISPSTs and satisfactory results were obtained.

• 대한기계학회논문집B
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• 제31권5호
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• pp.435-447
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• 2007

Recently, as MEMS and NEMS devices have been widely used in the various engineering applications, the characteristics of nanoscale systems are investigated in the limelight. However, as opposed to a macroscale system, the identification of the state of nanoscale systems is extremely hard because they can include only the order of $10^3{\sim}10^5$ molecules, which requires highly expensive and accurate experimental apparatus for an investigation. This limitations make the study on nanoscale system use computer simulations. Therefore, it is strongly required to identify the state of nanoscale system simulated in computer simulation. In this molecular dynamics(MD) study, we suggest that the potential energy of individual molecule can be used as criterion for defining the state of clusters or nanoscale systems. In addition, we compared the phase state from the potential energy with one from the radial distribution function(RDF) for verification. The comparison showed that the intermolecular potential energy can be used as a criteria distinguishing the phase state of nanoscale systems.

• 대한기계학회논문집
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• 제14권5호
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• pp.1290-1299
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• 1990

본 연구에서는 이러한 개념을 확장하여 직경이 26nm와 38nm인 두 개의 수평관 내 기액 2상유동에서 오리피스의 차압교란치의 확률밀도함수, 자기상관함수와 파워 스 펙트럼 밀도함수를 구하여 유동양식에 따른 이 들 통계치의 특성을 구명하였다. 본 연구에서 다룬 유동양식은 기포, 플러그, 슬러그, 성층, 파상, 환상, pseudo-slug 유 동이다. 이 결과 차압교란치의 통계적 해석을 통한 유동양식 판별법이 매우 유용하 다는 사실을 밝혔으며, 또 본 판별법을 관내 압력강하치의 통계적 해석을 통하여 유동 양식을 구분한 타 연구자들의 방법과 비교 분석하였다.

• 한국정밀공학회지
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• 제24권3호
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• pp.124-133
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• 2007

Active vibration isolation systems need the following performance specifications which are different from those of existing positioning systems: usage of seismic sensors, strict suppression of phase lead/lag in signal processing for sensors and actuators, excellent control in low frequency range and so on. In consideration of such specifications, a 3-DOF precision stage for vibration isolation is designed and modeled based on the physical characteristics. Then the major parameters such as spring constants and damping coefficients are valued by the system identification method using empirical transfer function. Finite element analysis is used as a verification and simulation tool throughout this research. This paper lays the foundation for the future research on the control of the active vibration isolation system.

• 한국통신학회논문지
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• 제38B권2호
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• pp.115-121
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• 2013

LED-ID (Light Emitting Diode-Identification) network is envisioned to be the next generation indoor wireless communication medium by which simultaneously high speed data transmission, identification, and illumination are possible. In spite of being extremely promising, it suffers from much impairment. Signals having different propagation paths can suffer from delays, and phase shifts which will eventually result interference. The probability of interference is also increased when communication links are established between a tag and several readers. Therefore it is necessary to reduce the interference in LED-ID network to ensure quality of service. It is possible to avoid interference by knowing the information about readers prior to assign the available spectrum. In this paper, we have proposed dynamic spectrum decision using cognitive radio concept. The simulation results justify that the proposed scheme is better than the conventional scheme.

• 분석과학
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• 제26권6호
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• pp.357-363
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• 2013

Selenium-containing proteins were separated from selenium-enriched yeast (SEY) using Trizol$^{(R)}$ reagent followed by anion exchange (AE) chromatography. This method is simpler and less time consuming than electrophoresis. Five selenium containing proteins were identified by on-line AE HPLC-ICP/MS (high performance liquid chromatography-inductively coupled plasma/mass spectrometry). Each protein was enzymatically hydrolyzed to seleno-amino acids and separated with RP (reverse phase) HPLC for the identification of selenoproteins.

• 산업기술연구
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• 제21권B호
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• pp.125-132
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• 2001

Heat dissipation technology using flow resonant phenomenon is a kind of new concept in heat transfer area. A vibration exciter is needed to generate air turbulence which has the natural shedding frequency of heat system. A mechanical vibrating device for the air flow oscillation is introduced, which is driven by a moving coil actuator. An analytical dynamic model for this mechanical vibration exciter is presented and its' validity is verified by the comparison with experimental data. Values of some unknown system parameters in the analytic model are estimated through the system identification approach. Based on this mathematical model, the vibration exciter using strain displacement estimator is developed. And in the experiment, the feedback control is used. During the experimental verification phase, it turns out the high modal resonant characteristics of vibrating plate are the major barrier against obtaining a high bandwidth vibration exciter.