• 한국재료학회지
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• 제28권3호
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• pp.148-158
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• 2018

This study investigated the effect of the grinding media of a ball mill under various conditions on the raw material of copper powder during the milling process with a simulation of the discrete element method. Using the simulation of the three-dimensional motion of the grinding media in the stirred ball mill, we researched the grinding mechanism to calculate the force, kinetic energy, and medium velocity of the grinding media. The grinding behavior of the copper powder was investigated by scanning electron microscopy. We found that the particle size increased with an increasing rotation speed and milling time, and the particle morphology of the copper powder became more of a plate type. Nevertheless, the particle morphology slightly depended on the different grinding media of the ball mill. Moreover, the simulation results showed that rotation speed and ball size increased with the force and energy.

• 한국재료학회지
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• 제26권11호
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• pp.611-622
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• 2016

Particle morphology change and different experimental condition analysis during composite fabrication process by traditional ball milling with discrete element method (DEM) simulation were investigated. A simulation of the three dimensional motion of balls in a traditional ball mill for research on the grinding mechanism was carried out by DEM simulation. We studied the motion of the balls, the ball behavior energy and velocity; the forces acting on the balls were calculated using traditional ball milling as simulated by DEM. The effect of the operational variables such as the rotational speed, ball material and size on the flow velocity, collision force and total impact energy were analyzed. The results showed that increased rotation speed with interaction impact energy between balls and balls, balls and pots and walls and balls. The rotation speed increases with an increase of the impact energy. Experiments were conducted to quantify the grinding performance under the same conditions. Furthermore, the results showed that ball motion affects the particle morphology, which changed from irregular type to plate type with increasing rotation speed. The evolution was also found to depend on the impact energy increase of the grinding media. These findings are useful to understand and optimize the particle motion and grinding behavior of traditional ball mills.

• 한국연소학회:학술대회논문집
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• 한국연소학회 2006년도 제33회 KOSCO SYMPOSIUM 논문집
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• pp.196-201
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• 2006

Silica(SiO2) nanoparticles are used as additives in plastics and rubbers to improve mechanical, electrical, magnetic properties and optical material. Silica nanoparticles were synthesized by the gas phase thermal oxidation of several kinds of precursors in many types of reactor. Diffusion flame reactor has some advantages compared with other types of reactors. In this study, we investigated the generation of silica nanoparticles on the effect of residence time by tetraethylothosilicate(TEOS) in a turbulent diffusion flame reactor controlled by providing reactant flowrate and reactor geometry affect particle morphology, particle size and particle size distribution. To determine the flame residence time, flame length should be determined which was examined by ICCD image. Particle size, distribution and morphology were performed with TEM.

• 폴리머
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• 제25권5호
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• pp.744-753
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• 2001

내충격성 폴리스티렌 (HIPS)의 내충격성에 영향을 주는 중요한 요소 중의 하나는 분산된 고무상 입자의 크기 및 입도분포이다. 본 연구에서는 반응조건이 HIPS의 고무상 입자 크기 및 입도분포에 미치는 영향을 관찰하기 위하여 HIPS를 중합 제조한 다음 고무함량, 교반속도 및 전중합 시간에 따른 고무상 입도분포 및 형태구조를 고찰하였다. 입도분석기로 분석한 결과, 톨루엔을 분산용매로 사용한 경우 열처리 온도가 낮을수록, 열처리 시간이 짧을수록 팽윤의 영향으로 고무상의 평균 입자경이 커졌지만, MEK의 경우에는 열처리 과정이 없어도 보다 합당한 입도분포를 얻을 수 있었다. 고무함량이 증가함에 따라 고무상의 평균 입자경은 뚜렷하게 커졌지만 고무함량이 적은 경우에는 교반속도가 증가하여도 평균 입자경은 그다지 큰 변화를 나타내지 않았다. 하지만 교반속도가 커짐에 따라 고무상 내의 폴리스티렌 포획입자는 크기가 균일해짐을 확인하였다. 또한 전중합시간에 따른 입도분포의 변화를 고찰한 결과 전중합 시간이 길어질수록 보다 작은 입도분포를 얻을수 있었다.

• Tribology and Lubricants
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• 제12권3호
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• pp.72-78
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• 1996

This paper was undertaken to analyze the morphology of wear debris generated from lubricated moving machine surfaces by image processing. The lubricati, ng wear test was performed under different experimental conditions using the wear test device made in our laboratory and wear test specimen of the pin on disk type wear rubbed in paraffme series base oil, by varying applied load, sliding distance. The four parameters (50% volumetric diameter, aspect, roundness and reflectivity) to describe the morphology have been developed and outlined in the paper. A system using such techniques promises to obviate the need for subjective, human interpretation of particle morphology in machine condition monitoring, thus to overcome many of the difficulties with current methods and to facilitate wider use of wear particle analysis in machine condition monitoring.

• 한국정밀공학회:학술대회논문집
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• 한국정밀공학회 1996년도 춘계학술대회 논문집
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• pp.563-567
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• 1996

This paper was undertaken to analyze the morphology of wear debris generating from moving lubricated machine surfaces by image processing. The lubricating wear test was carried out under different experimentaal conditions using the wear test device was made in our laboritory and wear testing specimen of the pin on disk type wear rubbed in paraffine series base oil, byvarying applied load, sliding distance. The four parameters(50% volumetric diameter, aspect, roundness and reflectivity) to describe the morphology have been developed and are outlined in the paper. A system using such techniques promises to obviate the need for subjective, human interpretation of particle morphology in machine condition monitoring, thus overcoming many of the difficulties with current methods and facilitating wider use of wear particle analysis in machine condition monitoring.

• 대한기계학회논문집B
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• 제26권5호
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• pp.710-715
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• 2002

The spherical nonagglomerated and uniform nanometer-size SiO$_2$particles are synthesized by the injection of TEOS vapor, irons and reaction gas in a furnace. Ions are generated by corona discharge and these ions charge SiO$_2$particles. As a result, spherical, nonagglomerated and ultrafine particles are generated in various conditions. Their morphology, charging portion and size distribution are examined by using TEM, ESP and SMPS. As the applied voltage of electrode changes from 0 to 5.0 kV, it is observed that the melon diameter of SiO$_2$particle decreases from 94 nm to 42 nm.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 1996년도 제23회 학술대회
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• pp.76-82
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• 1996

This paper was undertaken to analyze the morphology of wear debris generating from moving lubricated machine surfaces by image processing. The lubricating wear test was carried out under different experimental conditions using the wear test device was made in our laboritory and wear testing specimen of the pin on disk type wear rubbed in paraffine series base oil, by varying applied load, sliding distance. The four parameters(50% volumetric diameter, aspect, roundness and reflectivity) to describe the morphology have been developed and are outlined in the paper. A system using such techniques promises to obviate the need for subjective, human interpretation of particle morphology in machine condition monitoring, thus overcoming many of the difficulties with current methods and facilitating wider use of wear particle analysis in machine condition monitoring.

• Asian-Australasian Journal of Animal Sciences
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• 제20권11호
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• pp.1738-1745
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• 2007

A growth trial and a digestibility trial were conducted to examine the effect of feed particle size on the performance, nutrient digestibility, gastric ulceration and intestinal morphology in pigs fed barley-based diets. Barley was processed through a hammer mill to achieve four diets varying in particle size (average particle $size{\pm}standard $deviation): coarse ($1,100{\pm}2.19\;{\mu}m$), medium ($785{\pm}2.23\;{\mu}m$), fine ($434{\pm}1.70\;{\mu}m$) and mixed (1/3 of coarse, medium and fine) ($789{\pm}2.45\;{\mu}m$). Sixty-four entire male pigs were used in the growth trial and the diets were fed ad libitum between 31 kg and 87 kg live weight. Following slaughter, stomach and ileal tissues were scored for integrity (ulceration or damage) and histological measurements taken. Twenty-four entire male pigs were used in the digestibility trial, which involved total faecal collection. Over the entire growth phase, there were no differences (p>0.05) in average daily gain and feed conversion ratio between pigs fed diets of different particle size. Pigs fed the coarse and medium diets had lower (p<0.05) stomach ulceration scores (0.20 and 0.25, respectively, on a scale from 0 to 3) than those fed the mixed (0.69) or the fine diets (1.87). The stomachs of all animals fed the fine diet had lesions and stomach ulcerations were present only in this group. Pigs fed the fine diet had thicker (p<0.001) ileal epithelial cell layer with no differences (p>0.05) being observed for villous height or crypt depth. Faecal digestibility coefficients of neutral and acid detergent fibre were the highest (p<0.05) for the mixed diet, intermediate for the fine and coarse diets and the lowest for the medium diet. A similar numerical trend (p = 0.103) was observed for the apparent faecal energy digestibility coefficient. It is concluded that, with barley based diets, a variation in average particle size between $400{\mu}m$ and $1,100{\mu}m$ had no effect on pig performance but the fine dietary particle size affected the integrity of the stomach, as well as the structure of the small intestine, thus compromising overall gut health. Our data also demonstrate that changes in particle size distribution during the digestion process, rather than average particle size or particle size variation, are related to apparent faecal digestibility.

• Asian-Australasian Journal of Animal Sciences
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• 제22권1호
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• pp.107-112
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• 2009

This study was conducted to investigate the effect of feed particle size and feed form on growth performance, nutrient metabolizability and intestinal morphology in broiler chickens. This experiment was a 2${\times}$2 factorial arrangement including two feed particle sizes (fine and coarse) and two feed forms (mash and pellet). A total of two hundred and eighty eight day-old male Arbor Acre broilers were used in this six week experiment. Birds were randomly allotted to four dietary treatments with six replicates per treatment and twelve birds per replicate. The results showed that pelleting diets resulted in greater ADG (p<0.01), greater ADFI (p<0.01) and lower feed to gain ratio (F/G) (p<0.05) during starter, grower and overall period. Also, pelleting improved both apparent metabolizable energy (AME) (p<0.01) and the apparent metabolizability of crude protein (p<0.05) and organic matter (p<0.05) regardless of the phase. Reduction of feed particle size enhanced AME (p<0.05) during d 19 to 21. Increased villus height (p<0.05) and crypt depth ratio (p< 0.05) within duodenum, jejunum, and ileum were observed in birds fed the pellet diet compared with those given the mash diet. In conclusion, results indicated that feed pellets might enhance performance by improving nutrient metabolizability and digestive tract development.