• Title/Summary/Keyword: Particle coating

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Preparation of Mg(OH)2 Dispersion and its Application to PET Non-woven Textile as Flame Retardant Coating (수산화마그네슘 분산상의 제조와 PET 부직포 섬유의 난연 코팅제 적용)

  • Lim, Hyung-Mi;Hyun, Mi-Kyung;Jeong, Sang-Ok;Lee, Dong-Jin;Lee, Seung-Ho
    • Journal of the Korean Ceramic Society
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    • v.48 no.6
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    • pp.537-542
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    • 2011
  • Magnesium hydroxide as a non-halogen flame retardant has increasing attention due to its non-toxicity, high decomposition temperature and smoke suppressant ability during combustion. For the application of magnesium hydroxide retardant to the textile by soaking and coating method, the prerequisite for the coating is a small particle size, stable dispersion, and adhesion to the textile. The dispersion of $Mg(OH)_2$ particles and stability of the coating was checked by monitoring the change of transmittance and backscattering by varying the types of dispersion agents, binder, solvent, and $Mg(OH)_2$ source, and their compositions in the coating. The $Mg(OH)_2$ dispersion coating was applied to PET(poly(ethylene terephthalate)) non-woven textile. The physical properties are characterized by surface morphology, amount of coating, particle dispersion, and adhesion test. The flame retardant $Mg(OH)_2$ coated textile has been compared by limited oxygen index(LOI) and thermal gravimetry and differential scanning calorimetry(TG-DSC). It was found that phosphorous additive may give synergistic effect on $Mg(OH)_2$ flame retardant coating to make the flame retardant PET non-woven textile.

Improvement of Coating Properties of Metal/diamond Composite Through Ni Coated Diamond in the Kinetic Spraying Process (저온 분사 공정에서 니켈이 코팅된 다이아몬드 적용을 통한 금속/다이아몬드 복합재료의 코팅성 향상)

  • Na, Hyun-Taek;Bae, Gyu-Yeol;Kang, Ki-Cheol;Kim, Hyung-Jun;Lee, Chang-Hee
    • Journal of the Korean institute of surface engineering
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    • v.41 no.6
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    • pp.255-263
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    • 2008
  • Generally, deposition mechanism of diamond particle is mainly embedding effect in the kinetic spray process. Accordingly, in spite of high cost, helium gas was employed as process gas to get high diamond fraction in the composite coating. In this study, the deposition behavior of bronze/diamond by kinetic spray process was compared using different process gas (helium and nitrogen). Bare (mean size of $5{\mu}m$, $20{\mu}m$) and nickel coated diamond (mean size of $26{\mu}m$) were deposited on Al 6061-T6 substrate with fixed process temperature and pressure. For comparison with experimental results, plastic deformation behavior of nickel layer was simulated by finite element analysis (using ABAQUS/Explicit 6.7-2). The size, broken ratio, and fraction of diamond in the composite coating were analyzed through scanning electron microscopy and image analysis method. The uniform distribution and deposition efficiency of diamond particles in the coating layer could be achieved by tailoring the physical properties of the feedstock.

A Study on Wear Characteristics of Piston Running Part (피스톤 런닝부의 소재에 따른 마모특성 연구)

  • Jang, J.H.;Yi, H.K.;Joo, B.D.;Lee, J.H.;Moon, Y.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2007.05a
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    • pp.375-378
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    • 2007
  • Abrasive wear between piston ring face and cylinder liner is an extremely unpredictable and hard-to-reproduce phenomenon that significantly decreases engine performance. Wear by abrasion are forms of wear caused by contact between a particle and solid material. Abrasive wear is the loss of material by the passage of hard particles over a surface. From the pin-on-disk test, particle dent test and scuffing test, abrasive wear characteristics of diesel engine cylinder liner-piston ring have been investigated. Pin-on-disk test results indicate that abrasive wear resistance is not simply related to the hardness of materials, but is influenced also by the microstructure, temperature, lubricity and micro- fracture properties. In particle dent test, dent resistance stress decreases with increasing temperature. From the scuffing test by using pin-on-disk tester, scuffing mechanisms for the soft coating and hard coating were proposed and experimentally confirmed.

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Flame Synthesis of Silica-Coated Iron Oxide Nanoparticles and Their Characterization

  • Jun, Kimin;Yang, Sangsun;Lee, Jeonghoon;Pikhitsa, Peter V.;Choi, Mansoo
    • Particle and aerosol research
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    • v.9 no.4
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    • pp.209-219
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    • 2013
  • We have used the modified diffusion flame burner to synthesize silica coated iron oxide nanoparticles having enhanced superparamagnetic property. Silica-encapsulated iron oxide particles were directly observed using a high resolution transmission electron microscope. From the energy dispersive X-ray spectroscopy (EDS) and zeta potential measurements, the iron oxide particles were found to be completely covered by a silica coating layer. X-ray photoelectron spectroscopy (XPS) and X-ray diffraction (XRD) measurements revealed that the iron oxide core consists of ${\gamma}-Fe_2O_3$ rather than ${\alpha}-Fe_2O_3$. Our magnetization measurements support this conclusion. Biocompatibility test of the silica-coated iron oxide nanoparticles is also conducted using the protein adsorption onto the coated particle.

Development of Ceramic Composite Membranes for Gas Separation: II. Preparation and Coating Characteristics of Nanoparticulate $TiO_2$ Sols (기체분리용 세라믹 복합분리막의 개발: II. 극미세 입자 $TiO_2$ 졸의 제조 및 코팅 특성)

  • 현상훈;박준수;최세영
    • Journal of the Korean Ceramic Society
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    • v.29 no.9
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    • pp.739-749
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    • 1992
  • The sols prepared by dialyzing solutions, in which the hydrolyzed precipitates of TEOT or directly Ti(OC3H7)4 were resolved, were the nanoparticulate sol with the average particle size less than 7 nm and the anatase crystal phase. In the pH range of 1.5 to 2.9, the particle size of the nanoparticulate TiO2 sols (0.09 mol/ι) increased gradually upto 15 nm~26nm with the increase of pH in the initial aging state but the sols were transparent all the time, and stable without growin any more after 30 days. When the slipcasted porous alumina tubes were coated by the sol-gel dipping method, the minimum particle size and the aging time for forming the coated gel layer at the given pH were optimized. For obtaining the very thin crack-free and reproducible membrane coating, the use of a nanoparticulate TiO2 sol (0.09 mol/ι) aged for about 30 dyas at pH=2.0 was found to be the best.

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Preparation of composite particles by Rapid Expansion of Supercritical fluid Solutions and Release behavior

  • Ryu, Han-Won;Kim, Jung-Hwan;Kim, Young-Do;Shin, Kun-Chul
    • Proceedings of the Korea Association of Crystal Growth Conference
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    • 1998.09a
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    • pp.117-121
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    • 1998
  • The Rapid Expansion of supercritical fluid Solutions (RESS) process was applied to particles coating. Experiments were conducted in a fluidized bed with an internal nozzle in the center of the reaction tube. Microcapsules (mean particle size : 49$\mu\textrm{m}$) prepared by spray drying method were used as the core particles. Supercritical CO2 solutions of paraffin were expanded through the nozzle in to the bed that was fluidized by air. Surface morphology prepared particles was observed by SEM. For the inspection of particle size change, particle size distributions were measured before and after coating. The releasing behavior of Mg2+ ions inspected by AA.

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Effect of Particle Dispersion on Physical Properties of Ni-CNT Composite Coatings (입자분산이 Ni-CNT 복합도금막의 특성에 미치는 영향)

  • Cheon, Young-Hoon;Bae, Kyoo-Sik
    • Journal of the Semiconductor & Display Technology
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    • v.10 no.2
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    • pp.91-95
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    • 2011
  • Ni-CNT(carbon nanotubes) composite coating is often used for the surface treatment of electronic/mechanical devices to improve the properties of the exisiting Ni electroplating. For this, the dispersion of CNT particle is a critical process. In this study, ball milling and additive called sodium dodecyl sulfate(SDS) are employed for dispersion. Electroplated Ni-CNT films were examined by SEM-EDX, AES, microhardness tester, 4-point probe and contact angle measurement to find the optimum dispersion conditions. Ni-CNT coatings formed by ball milling for 9 hrs and with addition of SDS 12 times of CNT contents showed the highest hardness, reasonable resistivity and non-stick characteristics.

Effect of the Inner Side Dielectric Coating of the Tank on the Particle Movement for Improving of GIS Insulation Reliability (GIS 절연 신뢰성 향상을 위한 탱크 내면 코팅이 파티클 거동에 미치는 영향)

  • Lee, Bang-Wook;Koo, Ja-Yoon;Kim, Min-Kyu;Kim, Ik-Soo
    • Proceedings of the KIEE Conference
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    • 1996.11a
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    • pp.267-269
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    • 1996
  • In this work, the influence of wire type conducting particles on the insulation reliability of GIS has been systematically investigated when outer electrode was dielectric coated by epoxy resin. For this purpose, coaxial cylinder-type electrode was adopted in 362 kV chamber and various size of Cu conducting particle was used and different gas pressure was applied. To prove the coating effect on the gas insulation, different thickness of epoxy coated outer electrode have been considered and the lift-off voltage and flashover voltage have been analyzed. The results show that the dielectric coated electrode has an remarkable influence on the reducing particle behavior in GIS system and enhancing the GIS insulation reliability.

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Influence of nano-structured alumina coating treatment on shear bond strength between zirconia ceramic and resin cement (나노구조 알루미나 코팅 처리가 지르코니아 도재와 레진 시멘트 사이 전단 결합강도에 미치는 영향)

  • Kim, Dong-Woon;Lee, Jung-Jin;Kim, Kyoung-A;Seo, Jae-Min
    • The Journal of Korean Academy of Prosthodontics
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    • v.54 no.4
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    • pp.354-363
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    • 2016
  • Purpose: The aim of this study was to investigate whether the application of nano-structured alumina coating to the surface of Y-TZP could enhance the bond strength with resin cement. Materials and methods: A total of 80 zirconia plates were prepared and divided into four groups. : 1) airborne particle abrasion treatment (A) : 2) Rocatec treatment after airborne particle abrasion (R) : 3) nano-structured alumina coating treatment after polishing (PC) and 4) nano-structured alumina coating after airborne particle abrasion (AC). Alumina coating was formed by the hydrolysis of aluminium nitride (AlN) powder and heat treatment at $900^{\circ}C$. Coating patterns were observed with FE-SEM. Resin block was bonded to treated zirconia ceramics using resin cement. The shear bond strengths were measured before and after thermocycling. Results: The FE-SEM images show a dense and uniform nano-structured alumina coating structure, which enhances shear bond strength by increasing micro mechanical interlocking to resin cement. PC and AC groups showed higher shear bond strengths than A and R groups before and after thermocycling. A and R groups displayed significant drops in shear bond strength after thermocycling. However, PC and AC groups did not show any meaningful decreases in shear bond strength after thermocycling. Conclusion: Treatment of Y-TZP ceramics with nano-structured alumina coating could significantly increase their shear bond strength.

A Study on High Temperature Particles-Erosion of Hard Coatings (경질 코팅의 고온 입자침식 현상 연구)

  • 이의열;김종하
    • Journal of the Korean institute of surface engineering
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    • v.36 no.4
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    • pp.291-295
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    • 2003
  • Many steam turbine components encounter solid particle erosion damage. It has been reported that particle erosion damage is caused by oxide scale exfoliation from boiler tubes. One of the most effective solutions to combat the erosion damage is the application of erosion resistant coatings on the turbine components. In this study, particle erosion resistance for various hard coatings such as nitride, Cr carbide and boride coatings was evaluated under the simulated erosion conditions of steam turbines. Based on the particle erosion tests, the boride coating was found to be more superior to others.