• Title/Summary/Keyword: Paraffin recovery

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Recovery of IGF-I Using Liquid Emulsion Membranes (액막법을 이용한 IGF-I 회수)

  • 최광수;문용일
    • Korean Journal of Animal Reproduction
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    • v.22 no.1
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    • pp.89-94
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    • 1998
  • A study was made to investigate the effects of concerning factors with IGF-I recovery on the final IGF-I concentration in the effluent and to establish recovery conditions of IGF-I using liquid emulsion membranes(LEM). D2EHPA was best carrier among Amberlite LA2, Aliquit 336 and D2EHPA for recovery rate of IGF-I. Recovery rate of IGF-I by D2EHPA volume in the oil phase was increased as increasing D2EHPA volume, and optimal volume of D2EHPA was 5% in this experiment. The recovery rate of IGF-I by D2EHPA was increased by the decreasing from pH 7 to pH 4 of external phase. Therefore, optimal pH value was 4.0. Optimal concentrations of sulfuric acid in internal phase, paraffin oil in oil phase and Span 80 for recovery rate of IGF-I were 0.1M, 2.0% and 5%, respectively, and optimal W/O rate was 2. These results suggested that optimal conditions for recovery of IGF-I were D2EHPA(5%) as carrier, pH 4.0, 0.1M sulfuric acid, 2% paraffin oil, 2.0 W/O rate and 5.0% Span 80.

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Recovery of Paraffin Components from Pyrolysis Oil Fraction of Waste Plastic by Batch Cocurrent 4 Stages Equilibrium Extraction (회분 병류 4단 평형추출에 의한 폐플라스틱 열분해유 유분 중의 파라핀 성분의 회수)

  • Kang, Ho-Cheol;Shin, Sung Soon;Kim, Doo Han;Kim, Su Jin
    • Applied Chemistry for Engineering
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    • v.29 no.5
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    • pp.630-634
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    • 2018
  • The recovery of paraffin components contained in the fraction as a part of improving the quality for the fraction of waste plastics pyrolysis oil (WPPO) was investigated by batch cocurrent 4 stages equilibrium extraction. The fraction at a distilling temperature of $120-350^{\circ}C$ recovered from WPPO by the simple distillation and a little water-added dimethylformamide (DMF) solution were used as a raw material and solvent, respectively. As the number of equilibrium extraction (n) and the carbon number of paraffin component increased, the concentration of paraffin component contained in the raffinate increased. The concentrations of $C_{12}$, $C_{14}$, $C16$ and $C_{18}$ paraffin components present in the raffinate recovered at n = 4 were about 1.2, 1.5, 1.6 and 1.8 times higher than those of using the raw materials, respectively. Recovery rates (residue rates present in raffinate) of paraffin components rapidly decreased with increasing n, and increased sharply with increasing the carbon number. Furthermore, it was possible to predict the recovery rates at n = 1 - 4 for all paraffin components ($C_7-C_{24}$) contained in the raw material. The raffinate recovered through this study is expected to be used as a renewable energy.

[Retracted]The effect of Massage and Paraffin on Cold Hypersensitivity Patient ([논문표절]수족냉증에 적용한 마사지와 파라핀의 효과)

  • Roh, Hyo-lyun
    • Proceedings of the Korea Contents Association Conference
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    • 2017.05a
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    • pp.101-102
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    • 2017
  • This study of purpose was to evaluate the changes in hands and feet temperature by applying massage and paraffin bath.. The subject of this study was 30 university healthy students. Subjects were divided into paraffin bath group and massages group. The digital infrared thermographic imaging was used for thermographic analysis. The visual analog scale was used for subjective information about the degree of cold sensitivity and cold stress test was used for analyzing the temperature recovery rate. After the interventions showed that temperature difference of the right hand and temperature difference of the left hand are less in the paraffin group than the massage group. When applied paraffin bath and massage to the cold hypersensitivity patient the massage group showed difference in the visual analog scale and the paraffin group showed difference in the temperature of the right hand, left hand, left foot and in the visual analog scale. Paraffin bath treatment seems to be useful to patients with cold hypersensitivity on hands and feet.

Quality Improvement of Pyrolysis Oil Fraction of Waste Plastic by Dimethylformamide Extraction (디메틸포름아마이드 추출에 의한 폐플라스틱 열분해유 유분의 품질향상)

  • Kim, Su Jin
    • Applied Chemistry for Engineering
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    • v.30 no.2
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    • pp.155-159
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    • 2019
  • As a part of improving the quality for the fraction of the waste plastics pyrolysis oil (WPPO), the recovery of paraffin components contained in the fraction was investigated by dimethylformamide (DMF) equilibrium extraction. The fraction of a distilling temperature of $120{\sim}350^{\circ}C$ recovered from WPPO by the simple distillation and the aqueous solution of DMF were used as a raw material and solvent, respectively. The concentrations of paraffin components ($C_{12}$, $C_{14}$, $C_{16}$ and $C_{18}$) contained in the raffinate decreased by increasing the mass fraction of water in the solvent at an initial state ($y_{w,0}$), whereas, the concentrations of paraffin components contained in the raffinate increased by increasing the mass ratio of the solvent to the feed at an initial state $(S/F)_0$. The concentrations of $C_{12}$, $C_{14}$, $C_{16}$ and $C_{18}$ paraffin components present in the raffinate recovered at $(S/F)_0=10$ were about 1.37, 2.0, 2.46 and 3.16 times higher than those of the raw materials, respectively. Recovery rates (residue rates present in raffinate) of paraffin components rapidly increased with increasing $y_{w,0}$, and decreasing $(S/F)_0$. The raffinate recovered through this study was expected to be used as a renewable energy.

Heat transfer characteristics of Triple-Tube Type Latent Heat Storage Tank (3중관 튜브형 잠열 축열조에서의 열전달 특성 연구)

  • Lee, W.K.;Han, G.Y.;Kang, Y.H.
    • Journal of the Korean Solar Energy Society
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    • v.21 no.1
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    • pp.71-82
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    • 2001
  • The heat transfer experiment in a latent heat storage tank as a solar energy storage system for the hot water supply was carried out. The latent heat storage tank was consisted of triple - tube type ; Outer shell for hot water from solar collector, PCM storage vessel in the middle of the tank and inside tube for hot water recovery. The heat storage tank has the dimension of 60 cm long and 34 cm outside diameter. Paraffin wax(m.p = 55.4C) and sodium acetate trihydrate(m.p = 58 C) were employed as the PCM this study. Experimental variables were inlet temperature and flow rate of the hot water for heat storage stage and cold water for heat recovery stage. Temperature profiles, heat transfer coefficient and the efficiency of heat storage$(Q/Q_{max})$ and heat recovery $(Q/Q_{max})$ were determined for the paraffin wax and inorganic salt respectively.

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Heat transfer characteristics of Immersed Coil Type Latent Heat Storage Tank (내부코일형 잠열 축열조에서의 열전달 특성 연구)

  • Lee, W.K.;Han, G.Y.;Kang, Y.H.
    • Journal of the Korean Solar Energy Society
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    • v.21 no.1
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    • pp.83-91
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    • 2001
  • The heat transfer experiment in a pilot scale latent heat storage tank as a solar energy storage system for the hot water supply was carried out. The latent heat storage tank was consisted of three parts; Outer shell for hot water from solar collector, PCM storage vessel in the middle of the tank and immersed coil in the PCM vessel for hot water recovery. The heat storage tank has the dimension of 115 cm in height and 32 cm outside diameter. Paraffin wax (m.p = 55.4C) and sodium acetate trihydrate (m.p = 58 C) were employed as the PCM this study. Experimental variables were inlet temperature and flow rate of the hot water for heat storage stage and cold water for heat recovery stage. Temperature profiles, heat transfer coefficient and the efficiency of heat storage $(Q/Q_{max})$ and heat recovery $(Q/Q_{max})$ were determined for the paraffin wax and inorganic salt respectively.

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Determination of Liquid Paraffins in Foods by Using GC-FID (GC-FID를 이용한 식품 중 유동파라핀 함량 분석)

  • Park, Se-Jong;Choi, Jae-Chun;Lim, Ho-Soo;Jang, Su-Jin;Kim, So-Hee;Kim, Meehye
    • Korean Journal of Food Science and Technology
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    • v.45 no.5
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    • pp.545-549
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    • 2013
  • Liquid paraffin is a mixture of heavier alkanes derived from petroleum. It can be used as a lubricant in processing machinery, as a coating agent, or as a releasing agent. The purpose of this study was to analyze liquid paraffins in foods by using a gas chromatography-flame ionized detector (GC-FID). Liquid paraffin was extracted from the food samples using n-hexane. Non-polar aromatic or olefinic co-extractives were removed by alkaline permanganate oxidation followed by clean up on an aluminium oxide SPE cartridge before the GC-FID analysis. The results of recovery tests were 91.5-103.2%. Based on this optimized method, we investigated the amount of liquid paraffin in various food samples purchased from domestic markets. The levels of liquid paraffin in bread were $95.5{\pm}156.0$ mg/kg (0.008%), those in capsules were $40.2{\pm}54.5$ mg/kg (0.001%), and those in dried fruits and vegetables were $3.0{\pm}18.1$ mg/kg (0.0001%). No liquid paraffin was detected in fresh fruits and vegetables. We propose that our method can be used to monitor and detect liquid paraffin in foods for food safety management.

Chemical leaching of radioactive cement and paraffin waste form generated from NPPs (원전 발생 고화체 폐기물 핵종분석을 위한 침출 조건)

  • Lee Jeong-Jin;Ahn Hong-Joo;Pyo Hyung-Yeal;;;Jee Kwang-Young
    • Proceedings of the Korean Radioactive Waste Society Conference
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    • 2005.06a
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    • pp.278-283
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    • 2005
  • Cement and paraffin waste form were prepared with a acid extraction method for the analysis of radionuclides generated from nuclear power plants. The acid extraction method was carried out with $HNO_3-HCl$ acid. At first, we compared the method with the microwave acid digestion method using SRM. The solutions of decomposed SRM were then analyzed by AAS and ICP-AES. The acid extraction method had shown good results as microwave acid digestion method. This method provided recovery values greater than $80\%$ for metallic elements.

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Protease antigen recovery induces non-specific reaction in B-Cells (Protease antigen recovery의 B-Cell에 대한 비특이반응 유발)

  • Kim, Ok-Jin;Yi, Seong-Joon
    • Korean Journal of Veterinary Pathology
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    • v.7 no.1
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    • pp.11-15
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    • 2003
  • Antigen retrieval (AR) techniques were widely used to recover the antigenicity from the fixed tissues, which were guided by the philosophy of rendering immunohistochemistry (IHC) applicable to routine formalin-fixed, paraffin-embedded tissues for wide application of IHC in research and clinical filed for morphological observation like as anatomy, histology and pathology. Protease antigen recovery (PAR) is an AR technique, which is obtained the antigen retrieve by using enzyme digestion, and commonly used in IHC field. However, during the IHC for the detection of ovine herpesvirus 2 (OvHV-2) antigen, we noted lymphocyte-like cells-specific staining in the infiltrated cells into various organs like as liver and kidney, which was also shown in the IHC tissues with isotype control. However, those signals were not observed in the tissues conducted with in situ hybridization. Therefore, we analyzed the specificity of the IHC detection results. We found that PAR may induce false-positive result during IHC in lymphocyte-like cells, which were infiltrated mainly around vessels and in interstitial tissues. Through the Phenotyping, we realized that those false-positive cells were B-cell-related cells. These results suggest that PAR, a AR using protease, may induce non-specific false-positive reactions during IHC.

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ADMINISTRATION OF CROTON OIL EFFECTED IN THE INTESTINAL MUCOUS CELL OF MICE (파두유(巴豆油) 투여(投與)가 생쥐의 장관점액세포(腸管粘液細胞)에 미치는 영향(影響))

  • Han, Kyung-Taik
    • The Journal of Internal Korean Medicine
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    • v.1 no.1
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    • pp.98-106
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    • 1976
  • In order to study the effect of croton oil on the mucous cell in the mice intestin the experimental animals were injected with 0.1gm body weight of croton oil through intraperitoneally. They were sacrificed by ether anesthesia and obtained from distal small intestine and duodenum and colon, and fixed in 10% meutral formal. After embedded in paraffin, sectioned in 5 micro thickness, and stained with P.A.S (Periodic Acid Schiffis) reaction. The average number of the mucous cell was counted in each specimen over 20 fields under 450 magnification. The following results were obtained; 1) An average number of mucous cell began rapidly increase from 15 min and reached high average number after injection of croton oil of mucous cell from 30-60 min after injection. 2) An average number of mucous cell rapidly increase after injection of croton oil and were not reduced normal level by time lapsed 48 hrs. 3) The mucous cell showed with tape of time after injection of croton oil. A type and B type decrease and showed recovery C type decrease and recovery. 4) According to the above findings, it is presumed that croton oil accelerate secretion of mucin of the mucouse cell and production of mucin in growing mucous cell.

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