• 제목/요약/키워드: Pak1

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식육중 Chlorfluazuron의 잔류분석법 및 잔류량에 관한 연구 (Studies on the Analytical Methods and Quantity of Residual Chlorfluazuron in Meat)

  • 박건상;홍무기;백선영;정병곤;박종세
    • 한국식품위생안전성학회지
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    • 제12권4호
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    • pp.288-293
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    • 1997
  • Analytical method using capillary GC/ECD was developed to determine trace residues of chlofluazuron, 1-[3, 5-dichloro-5-trifluoromethyl-2-pyridyloxy)phenyl]-3-(2, 6-difiuorobenzoyl), in meat, and applied to analyze the residues in domestic and imported meats. The analytical scheme developed does not require column chromatographic cleanup; chlorfiuazuron was extracted with diethyl ether and petroleum ether (50: 50), partitioned against acetonitrile, cleaned up with silica Sep-Pak cartridge, identified GC/ECD, and comfirmed by GC/MS. The mean recoveries of the pesticide in meat fortified with standard solution 0.1, 0.5, 0.1 mg/kg were ranged from 82 to 95%. The limit of detection and limit of quantitation were 0.001 and 0.005 mg/kg, respectively. Chlorfluazuron residues were not found in domestic samples, but found in imported Australian beef ranging from 0.02 to 0.17 mg/kg, detected by 18% among the samples.

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TRANSVERSE HARMONIC FIELDS ON RIEMANNIAN MANIFOLDS

  • Pak, Jin-Suk;Yoo, Hwal-Lan
    • 대한수학회보
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    • 제29권1호
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    • pp.73-80
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    • 1992
  • We discuss transverse harmonic fields on compact foliated Riemannian manifolds, and give a necessary and sufficient condition for a transverse field to be a transverse harmonic one and the non-existence of transverse harmonic fields. 1. On a foliated Riemannian manifold, geometric transverse fields, that is, transverse Killing, affine, projective, conformal fields were discussed by Kamber and Tondeur([3]), Molino ([5], [6]), Pak and Yorozu ([7]) and others. If the foliation is one by points, then transverse fields are usual fields on Riemannian manifolds. Thus it is natural to extend well known results concerning those fields on Riemannian manifolds to foliated cases. On the other hand, the following theorem is well known ([1], [10]): If the Ricci operator in a compact Riemannian manifold M is non-negative everywhere, then a harmonic vector field in M has a vanishing covariant derivative. If the Ricci operator in M is positive-definite, then a harmonic vector field other than zero does not exist in M.

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반복된 후방 십자 인대 재건술 후 발생한 구획 증후군 및 심부 정맥 혈전증 (Compartment Syndrome and Deep Vein Thrombosis after Repetitive Posterior Cruciate Ligament Reconstruction)

  • 김진구;이수원;최홍준
    • 대한관절경학회지
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    • 제12권1호
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    • pp.58-62
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    • 2008
  • 후방 십자 인대 재건술은 신경혈관 합병증 발생 위험율이 높은 수술 방법이다. 하지만 후방 십자 인대 재건술 후 발생한 심부 정맥 혈전증 및 그와 관련된 구획증후군에 대한 보고는 없다. 본 교실에서는 후방 십자 인대 파열로 반복적인 수술을 시행 받은 환자에서 경골 inlay 방법을 이용한 후방 십자 인대 재재건술 후 발생한 신경혈관 합병증의 증례를 보고하고 이의 중요성에 대한 고찰을 하고자 한다.

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악관절음 환자의 하악 비틀림회전운동에 관한 연구 (A Study on Mandibular Rotational Torque Movement in Subjects with Temporomandibular Joint Sounds)

  • 소종섭;이경호;정성창
    • Journal of Oral Medicine and Pain
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    • 제24권4호
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    • pp.455-466
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    • 1999
  • The purpose of this study was to investigate the magnitude of mandibular rotational torque movements in subjects with TMJ sounds, and to analyse correlation between quantitative characteristics of TMJ sounds and mandibular rotational torque movement. Twenty dental college students with TMJ clicking and twenty students without any TMD signs and symptoms were examined by mean of SonoPak and Rotate program of BioPAK system(Bioresearch Inc. MilWaukee, wisconsin, USA) in this study. Mandibular rotational torque movements were recorded and analysed during maximum mouth opening, protrusion, and lateral excursion in frontal and horizontal planes. The obtained results were as follows: 1. On maximum mouth opening, mandibular rotational angle and distance of clicking group were significantly greater than those of control group in frontal plane. (P<0.05). 2. During maximum mouth opening closing, maximum mandibular rotational angle and distance of clicking group were significantly greater than those of control group in frontal plane. (P<0.01). 3. On protrusion, mandibular rotational angle and distance of clickin group were significantly greater than those of control group in horizontal plane. (P<0.05). 4. On lateral excursion, there was no significant difference in mandibular rotational angle and distance between clicking group and control group in frontal and horizontal planes. 5. There were significant correlations between peak amplitude of TMJ sounds and maximum mandibular rotational distance during maximum mouth opening (r=-.481) and mandibular rotational distance on maximum mouth opening (r=-.455) in horizontal plane. 6. There were significant correlations between Above 300/(0-300)Hz ratio of TMJ sounds and mandibular rotational angle (r=-.499) and distance (r=-.457) on maximum mouth opening in frontal plane.

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수경재배시 양액 조성 처리가 몇가지 엽채류의 내적 품질에 미치는 영향 (Effect of Nutrient Solution Composition Modification on the Internal Quality of Some Leaf Vegetables in Hydroponics)

  • 강호민;김일섭
    • 생물환경조절학회지
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    • 제16권4호
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    • pp.348-351
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    • 2007
  • 본 실험은 양액조성 및 단비 처리에 의한 엽채류의 질산염과 비타민 C와 같은 내적품질 변화를 알아보고자 하였다. 2주일간 정상적인 배양액에서 재배한 후 다시 2주일간 서로 다른조건의 양액에서 재배한 청경채, 청치마상추, 로메인상추는 단비처리구를 제외하고는 생육에 큰 차이를 보이지 않았다. 내적 품질로 질산염은 야마자키 상추 1배 양액 처리구에서 가장 높았으며 다음으로 $+NH_4$ 처리구 순서였고 $-NO_3$와 단비 처리구에서 가장 낮았다. 비타민 C 함량은 대체로 질산염과 반대의 결과를 나타내어 청치마, 로메인상추에서는 단비처리구에서 청경채는 $-NO_3$처리구에서 가장 높았다. 이들 질산염과 비타민 C 함량간의 상관계수는 청경채는 -0.614, 로메인상추는 -0.651이었으며 특히 청치마상추는 -0.804를 나타내었다.

Selection of appropriate nutrient solution for simultaneous hydroponics of three leafy vegetables (Brassicaceae)

  • Young Hwi, Ahn;Seung Won, Noh;Sung Jin, Kim;Jong Seok, Park
    • 농업과학연구
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    • 제49권3호
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    • pp.643-653
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    • 2022
  • This study investigated which nutrient solution is suitable for growth and secondary metabolite contents when three different vegetable plants are grown simultaneously in one hydroponic cultivation bed. Seeds of pak choi (Brassica compestris L. ssp chinsensis), red mustard (Brassica juncea L.), and arugula (Eruca sativa Mill.) were sown in the shape of a triangle in three places on rockwool cubes. The rockwool cubes were placed in semi deepflow technique (semi-DFT) hydroponic systems in a rooftop greenhouse after three weeks of growth as seedlings then cultivated with four different nutrient solutions, Korea Horticultural Experiment Station (KHE), Hoagland, Otsuka-A, and Yamazaki, at the rooftop greenhouse for two weeks. The leaf area of pak choi cultivated in Otsuka-A was the largest but SPAD values, leaf area, and fresh weight of arugula were highest with KHE treatment. The total glucosinolate (GSL) content of pak choi was 151.7% higher in KHE than in Hoagland, and there was no significant difference in Yamazaki and Otsuka-A treatments. The total GSL content of red mustard was 34.6 μmol·g-1 in Hoagland, and it was 32.6% higher in Hoagland than in Yamazaki. Total GSL content of arugula was 57.5% higher in Yamazaki and Hoagland nutrients than in KHE and Otsuka-A nutrients solutions. The total GSL content of three plants grown with KHE was 40.7% higher than with Yamazaki, and the other nutrient solutions did not show significant differences. Therefore, KHE nutrient solution is considered suitable for nutrient solution composition for the cultivation of three different Brassicaceae crops in a single hydroponic cultivation system.

목재(木材) 세포벽중(細胞壁中)의 탄수화합물(炭水化合物) 간(間)의 결합(結合) 양식(樣式)(I) -탄수화합물(炭水化合物)의 단리(單離)- (The Types of Linkage of Carbohydrates in Wood Cell Wall (I) - The Isolation of Carbohydrates -)

  • 이상필;이종윤
    • Journal of the Korean Wood Science and Technology
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    • 제15권3호
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    • pp.34-43
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    • 1987
  • This study was performed to find out the types of linkage of carbohydrates in wood cell walls. To study the structure of linkage of carbohydrates in wood cell walls, we have attempted to find out the method holocellulose preparation and optimum condition of enzyme hydrolysis in holocellulose, and fractionate oligosaccharide with products that hydrolized partly by acetolysis and deacetylation in holocellulose. We have achieved four results. These results as follow; 1. At first. we reacted in wood meal $NaClO_2$ 1g per lignin lg for one hour and then the same of quantity $NaClO_2$ for four hours. Through these experiments, we have developed new holocellulose preparation method which had low loss of carbohydrates and high effect of the delignification. 2. The optimum condition of enzyme hydrolysis of holocellulose which had lignin was 0.005M sodium acetate buffer (pH 5.0). We have achieved 7.2% reducing sugar through the procedure that reactioned 0.01g holocellulose putting enzyme 0.03g for 72 hours. It may be supposed that 5.5% of lignin contained in holocellulose prevented enzyme contaction from holocellulose and so this lignin has resulted in the low efficiency of enzyme hydrolysis. 3. We did not fractionated from oligosaccharides which were preparated by the method of acetolysis and deacetylation in holocellulose. The reason is that holocellulose having a lot of lignin prevented prefectly partial hydrolysis from the method of acetolysis and deacetylation. 4. We attempted analysis of six standard substances through HPLC apparatus having sugar pak 1 column which we have changed flow rate and the column temperature variably. These six standard substances were D-glucose, D-mannose, D-xylose, D-galactose and L-rhamnose, L-arabinose, But sugar pak 1 column was not fitted analysis of four substances because D-galactose, D-mannose, D-xylose, L-rhamnose were agreement with elution time. And so, we could not analize four standard substances with sugar pak 1 column.

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