• The Korea Journal of Herbology
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• v.24 no.2
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• pp.13-20
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• 2009

Objectives: To compare the contents of hazardous substances before/after a decoction. Methods : The heavy metal contents before/after a decoction were measured by Inductively Coupled Plasma Atomic Emission Spectrometer (ICP-AES) and mercury analyzer. In order to analyze pesticides in 6 samples we used simultaneous multi-residue analysis of pesticides by GC/ECD, which was followed by GC/MSD analysis to confirm the identity of the detected pesticide in each sample. In addition, the contents of sulfur dioxide (S02) were performed by Monier-Williams distillation method. Results : 1. The mean values of heavy metal contents (mg/kg) for the samples were as follows: Socheongryong-tang (before decoction - Pb; 1.115, Cd; 0.179, As; 0.069 and Hg; 0.028, after decoction - Pb; 0.110, Cd; 0.011, As; 0.005 and Hg; 0.002), Insampaedok-san (before decoction - Pb; 1.207, Cd; 0.148, As; 0.171 and Hg; 0.026, after decoction - Pb; 0.075, Cd; 0.006, As; not detected and Hg; O.OOD, Oryung-san (before decoction - Pb; 1.955, Cd; 0.430, As; 0.063 and Hg; 0.027, after decoction - Pb; 0.083, Cd; 0.013, As; 0.006 and Hg; 0.002), Hwangryunhaedok-tang (before decoction - Pb; 1.825, Cd; 0.210, As; 0.050 and Hg; 0.009, after decoction - Pb; 0.107, Cd; 0.010, As; 0.005 and Hg; O.OOD, Bangpungtongseong-san (before decoction - Pb; 1.740, Cd; 0.162, As; 0.585 and Hg; 0.018, after decoction - Pb; 0.041, Cd; 0.006, As; 0.022 and Hg; not detected) and Oyaksungi-san (before decoction - Pb; 1.199, Cd; 0.183, As; 0.321 and Hg; 0.031, after decoction - Pb; 0.096, Cd; 0.008, As; 0.021 and Hg; 0.0004). 2. Contents (mg/kg) of sulfur dioxide (S0$_2$) before a decoction in Socheongryong-tang, Insampaedok-san, Oryung-san, Hwangryunhaedok-tang, Bangpungtongseong-san and Oyaksungi-san exhibited 3.2, 5.7, 4.5, 49.8, 7.8 and 22.4, respectively. However, contents of sulfur dioxide after a decoction in all samples were not detected. 3. Contents (mg/kg) of residual pesticides before/after a decoction in all samples were not detected. Conclusions : These results will be used to establish a criterion of heavy metals, residual pesticides and sulfur dioxide.

• Journal of the Korean Chemical Society
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• v.12 no.2
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• pp.47-50
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• 1968

Two methods for separation of the impurities from bismuth metal have been found by the use of Dowex $1{\times}4,$ anion exchange resins. The first method is that Dowex $1{\times}4$ resins are packed into the two stage columns (height of under stage is 22cm and upper stage is 3cm, and diameter of columns are 1.5cm), and the impurities of Pb(II), Ag(I) and Cu(II) are separated by the eluent of 7.5M HCl soln, Zn(II), Fe(III) by 0.5M HCl solns, and Te(IV) in the upper stage by 2M NaOH soln. Remained Au(III) in the upper stage is determined by the ignition with resins. The 2nd method is that for the separation of all the impurities simultaneously the same resins are packed into single stage column(height is 10cm and diameter is 1.5cm), and all the impurities of Pb(II), Zn(II), Cu(II), Fe(III) and Ag(I) are eluted by the eluent of 0.5M HCl soln. Separated impurities are determined by the colorimetry.

• Journal of the Mineralogical Society of Korea
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• v.30 no.3
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• pp.127-136
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• 2017

High pressure has been applied to check the pressure effect on the powdered $TiO_2$-complex, which was synthesized for ultra-violet rays cutoff and antimicrobial applications. $TiO_2$-complex consists of anatase, rutile and silver chloride. Grain size was determined to be ~34 nm. Both anatase and rutile begin structural phase transitions to $ZrO_2$ (baddeleyite)-type crystal structures at 14~16 GPa, then sustain their phases up to 22.7 GPa. Under decompression to 0.0001 GPa (ambient pressure), rutile transforms to another phase with ${\alpha}-PbO_2$ structure, while anatase retains its high pressure structure upon complete decompression. Silver chloride peaks disappear at the low pressures.

• Journal of the Microelectronics and Packaging Society
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• v.17 no.3
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• pp.11-15
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• 2010

In this paper, we focused on the optimization of bonding conditions for the successful thermo-compression bonding of electrodes between the RPCB and FPCB with Sn-Pb solder. The peel strength was proportionally affected by the bonding conditions, such as pressure, temperature, and time. In order to figure out an optimized bonding condition, fracture energies were calculated through F-x (force-displacement) curves in the peel test. The optimum condition for the thermo-compression bonding of electrodes between the RPCB and FPCB was found to be temperature of $225^{\circ}C$ and time of 7 s, and its peel strength was 22 N/cm.

• Journal of the Korea Organic Resources Recycling Association
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• v.22 no.3
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• pp.53-59
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• 2014

In this study, the sewage sludge dryer is installed before and after dehydration of the sludge and aqueous phase composition, the heavy metal content, and measurement and analysis were investigated. The removal efficiency of water content of sewage sludge was about 95.7% in the sewage sludge dryer. The removal efficiency of water content for primary dryer was designed for 35% of primary drying, secondary drying to remove the water content to 10%, but as the measurement revealed that 20.8% of primary drying, the second dryer 3.3% a better effect to the actual operation respectively. Before the installation of the sewage sludge dryer, the content of heavy metal was as follows, Cu:352~614 ppm, Hg: 1.3~1.44ppm, Cd : 1.1~1.86ppm, Pb : 17.25~ 28.93 ppm, As : 1ppm. And after the installation of the sewage sludge dryer, the content of heavy metal changed to as follows, Cu : 340~350 ppm, Hg : 0 ppm, Cd : 0~0.021 ppm, Pb : 0 ppm, As : 0~0.043 ppm which is Also below the legal limits. Also, the sewage sludge dryer produce 1/4 of the sewage sludge into dried sludge.

• Journal of the Korea Organic Resources Recycling Association
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• v.22 no.2
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• pp.17-26
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• 2014

In this study, the adsorption efficiency of mixed heavy metals from an aqueous solution was examined using bentonite. The physical and chemical properties of bentonite was analyzed via scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FT-IR), Further, heavy metal adsorption was characterized using Freundlich and Langmuir equations. Equilibrium adsorption data were fitted well to the Langmuir model for bentonite. The adsorption uptake of heavy metals was high and followed the order $Pb^{2+}$ > $Cu^{2+}$ > $Cd^{2+}$ > $$Zn^{2+}{\sim_=}Ni^{2+}$$. The results also showed that adsorption uptake slightly increased as increasing pH from 6 to 10. The bentonite surface was observed viay SEM and FT-IR; Si-O and Si-O-Al were found to be the main functional groups by FT-IR analysis. From these results, the adsorption mechanisms of heavy metal were not only surface adsorption and ion exchange, but also surface precipitation. Thus, bentonite could be a useful adsorbent for treating heavy metal in aqueous solution.

• Journal of Environmental Health Sciences
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• v.18 no.1
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• pp.22-33
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• 1992

In Iri industrial area, Heavy metals in ait of the factories, 10 metal and 8 non-metal factories, were examined for ten months(from Feb. to Nov, 1991). The methals in blood, urin and hair of 232 employees who have worked in the factories were also examined at the same time The results are summarized as follows 1. Heavy metals Pb, Cd and Mn in the metal factories were 0.031mg/m$^{3}$, 0.0065mg/m$^{3}$, and 0. 035mg/m$^{3}$ respectively, but 0.017mg/m$^{3}$, 0.021mg/m$^{3}$ and 0.014mg/m$^{3}$ in non-metal factories. 2. Heavy metals such as Pb, Cd and Mn in blood from employees in the metal factories were measured : 22.36$\mu$g/dl, 0.27$\mu$g/dl and 1.26$\mu$g/dl respectively, The values in the non-metal factories were 19.84$\mu$g/dl, 0.21$\mu$g/dl and 1.24$\mu$g/dl. 3. Heavy metals such as Pb, Cd and Mn in urine from employees in the metal factories were measured 32.94$\mu$g/l, 0.16$\mu$g/dl, and 1.60$\mu$g/dl respectively, whereas the values in the non-metal factories were 28.79$\mu$g/l, 0.13$\mu$g/dl and 1.35$\mu$g/l. 4. Heavy metals such as Pb, Cd and Mn in hair from employees in the metal factories were measured 8.92mg/kg, 0.33mg/kg and 3.71mg/kg respectively, but 8.14mg/kg, 0.31mg/kg and 3.26 rng/kg in the non-metal factories.

• Journal of environmental and Sanitary engineering
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• v.22 no.1 s.63
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• pp.29-35
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• 2007

This study was examined adsorption ability of heavy metal Hg(I), Pb(II), and U(Vl) ion use of fruit from schizandra chinensis, The fruits of schizandra chinensis sample used breaking into fragments $50{\sim}100$ mesh. The sample solution was mixed fruits of schizandra chinensis and heavy metal ion. Each heavy metal ion of into solution was quantum analysis with ICP-AES. As the result, each condition of maxium adsorption ability of heavy metal ion was high in the range of pH 5-7, adsorption time was about 15 minutes, and the optimum temperature was $100^{\circ}C$. The heavy metal ion was increased adsorption in order of increasing concentration and in ethanol solution better than in aqueous solution.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 1996.05a
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• pp.68-71
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• 1996

In the study, the thermal and optical properties of SiO$_2$-PbO-K$_2$O-Al$_2$O$_3$ g1asses were investigated. According to Ga$_2$O$_3$ addictions, the properties of bulk glass, transition temperature and softening temperature were increased, whereas thermal expansion coefficient was decreased; In the optical properties, refractive index was increased, and IR cut-off wavelength was enlarged from 4.64$\mu\textrm{m}$ to 5.22$\mu\textrm{m}$. But, the optical loss of fiber was decreased.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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• 2001.05c
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• pp.19-24
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• 2001

In this study, Pb(La Ce)$TiO_3$ composition ceramics were manufactured for 20 MHz resonator application. Electromechanical coupling factor, mechanical quality factor and dynamic range of thickness vibration mode were measured as the variations of L/T(length/thickness) ratio of ceramic substrats. Mechanical quality factor and dynamic range of third overtone thickness vibration mode showed the highest value of 2,773 and 52.22 dB at specimen S4(l/t=12), respectively. The excellent temperature stability of resonant frequency suitable for resonator application was shown, regardless of thermal shock.