• Title/Summary/Keyword: P-Y curves

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Preparation and Characteristics of Magnetite Ferrofluid (Magnetite 강자성유체의 제조와 그 특성)

  • 김태옥;김상문
    • Journal of the Korean Ceramic Society
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    • v.27 no.1
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    • pp.13-22
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    • 1990
  • The magnetite ferrofluids of which solvents are water or kerosene have been prepared by making surfactant absorbed on the surface of the magnetite which have been synthesized by air oxidation of Fe(OH)2 at pH 11 and 75$^{\circ}C$, and their basic properties have been measured by XRD, SEM, DTA, TG, viscometer, magnetometer and B-H tracer. The results are as follows ; 1) The shape of magnetite prepared by air oxidation is found to be sphere-like shape and its particle size is smaller than 200A. 2) The maximum amount of sodium oleate adsorbed on the surface of magnetite is about 20% in the weight of the magnetite including the adsorbed sodium oleate. And when magnetite is well dispersed into solvent, R(the weight ratio of the added sodium oleate to Fe3O4) is 0.40-0.48. 3) The dispersion ratio, the viscosity and the magnetization of magnetite ferrofluid are constant regardless of the added amount of sodium oleate above R=0.40-0.48. 4) The magnetic hysteresis curves of magnetite ferrofluid show superparamagnetism-like behavior.

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A Study on the Intrinsic Degradation Behavior of LaNi5 (LaNi5의 intrinsic degradation 거동에 관한 연구)

  • Ahn, Hyo-Jun;Lee, Jai-Young
    • Journal of Hydrogen and New Energy
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    • v.2 no.1
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    • pp.77-82
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    • 1990
  • To investigate the effect of strains heat effect and thermal energy on the intrinsic degradation of $LaNi_5$, the changes of P-C-Isotherm curves under the condition of mainly applied one of the above factors were investigated. The revesible hydrogen storage capacity decreased by means of the hydrogenation at high temperature without cyclings or pressure induced cyclings with low thermal energy. The degree of degradation was more severe as the heat of hydrogenation reaction increased. Thus the intrinsic degradation of $LaNi_5$ depended upon lattice strain as well as thermal energy.

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A Study on the Hydrogenation Properties of Mechanically Alloyed Ti0.7Mg0.3Ni (기계적합금화에 의해 제조된 Ti0.7Mg0.3Ni합금의 수소화학반응특성에 관한 연구)

  • Kim, Eul-Soo;Ahn, Hyo-Jun;Kim, Ki-Won
    • Journal of Hydrogen and New Energy
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    • v.8 no.4
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    • pp.173-180
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    • 1997
  • The Mechanically Alloyed $Ti_{0.7}Mg_{0.3}Ni$ was investigated as a function of milling time by X-ray diffraction, SEM(scanning electron microscope), EDS(energy dispersive spectrometer), P-C-Isotherm curves. After 10hrs milling, mixed $Ti_{0.7}Mg_{0.3}Ni$ powders were changed to amorphous phase. And amorphous $Ti_{0.7}Mg_{0.3}Ni$ alloys became TiNi phase crystalline after heat treatment at 873K in a vacuum for 1 hour. The hydrogen absorption capacity of the annealed $Ti_{0.7}Mg_{0.3}Ni$ alloy increased as a function of mechanical alloying time.

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Voltammetric Determination of Ag(I) ion using Carbon Paste Electrode Modified with $Ph_2O_2S_3$ ($Ph_2O_2S_3$로 변성된 탄소반죽전극에 의한 Ag(I) 이온의 전압-전류법적 정량)

  • Lee, Ihn Chong
    • Analytical Science and Technology
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    • v.12 no.2
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    • pp.171-175
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    • 1999
  • Carbon paste electrodes, modified with podands containing more than two sulfur atoms, have been employed for the voltammetric determination of Ag(I) ion from aqueous solution. The voltammetric response was characterized with respect to paste composition, preconcentration method, kind of anion, variation of pH, Ag(I) ion concentration, and possible interferences. Linear calibration curves were obtained for Ag(I) ion concentration ranging from $1.0{\times}10^{-6}$ to $9.0{\times}10^{-5}M$, and detection limit was $5.0{\times}10^{-7}M$.

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Studies on single electron-hole recombination in InAs/GaAs Quantum dots (InAs/GaAs 양자점의 단전자-정공 재결합 연구)

  • 이주인;임재영;서정철
    • Journal of the Korean Vacuum Society
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    • v.10 no.2
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    • pp.257-261
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    • 2001
  • InAs/GaAs quantum dots between InGaAs/GaAs superlattices were grown by MBE. The quantum dots size is shown to be very uniform by measuring photoluminescence spectra of quantum dots. Single photon structures based on self-consistent calculation were grown and single photon devices were fabricated by e-beam lithography. The electrical hystereses of I-V curves for single Photon devices would result from single electron-hole recombination, where the resonant-tunneling voltages of electron and hole are different.

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A Small Ultra-Wideband (UWB) Antenna with Combination of Electric-Magnetic Radiators (전기-자기계 방사체 결합형 소형 초광대역 안테나)

  • Kim, Yong-Jin;Jung, Chang-Won;Kim, Young-Bong;Kwon, Do-Hoon
    • The Transactions of the Korean Institute of Electrical Engineers P
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    • v.58 no.1
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    • pp.33-37
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    • 2009
  • In this paper, a printed small Ultra-Wideband (UWB) antenna with directive radiation characteristics based on combination of electric-magnetic radiators is presented. The combinations of the electric and magnetic type antennas result in the directive radiation patterns for all observed UWB frequency band. Simple combination of dipole antenna and loop antenna is also presented to show that proper configuration of electric radiator and magnetic radiator can produces directive radiation characteristics. The target frequency is from 3.1 GHz to 10.6 GHz with size of $15\;mm{\times}31\;mm$. A proto-type of the combined antenna is simulated, fabricated and measured. Simulation and experimental results of input impedance and gain characteristics of the proposed antenna are presented. There are good agreements between the simulated and measured VSWR curves. Also, the results show the directive radiation characteristics with small antenna form factor over the target frequency range.

Quantitation and Validation of Atorvastatin using HPLC-UV

  • Heine, Daniel;Yong, Chul-Soon;Kim, Jung-Sun
    • Journal of Pharmaceutical Investigation
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    • v.37 no.3
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    • pp.187-192
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    • 2007
  • A reversed phase HPLC analysis of atorvastatin (AS) standard solution was performed using diclofenac (DF) as internal standard. Column oven temperature, flow rate and the composition of the mobile phase were varied in order to determine a practical system setup using a C18 column and UV detector. Two C18 columns of different length were compared regarding their influence on the AS peak shape. Based on these preliminary experiments a validation study was performed utilizing a C18 column at $62^{\circ}C$ with a mobile phase consisting of sodium phosphate buffer (0.05 M, pH 4.0), methanol and acetonitrile (40:50:10, v/v/v). The detection limit for AS was $0.1{\mu}g/ml$ and inter- and intra-day calibration curves were linear over a concentration range of $0.2-50{\mu}g/ml$. Accuracy and precision were satisfactory in the AS concentration range of $0.5-50{\mu}g/ml$.

Voltammetric Determination of Ag(I) ion with Carbon Paste Electrode Modified with Macrocyclic Ligand Containing Oxygen and Nitrogen as Ligating Atoms (주게원자로 산소와 질소를 포함하는 거대고리 리간드로 변성된 탄소반죽전극에 의한 Ag(I) 이온의 전압-전류법적 정량)

  • Lee, Ihn Chong
    • Analytical Science and Technology
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    • v.15 no.1
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    • pp.91-95
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    • 2002
  • Carbon paste electrodes, modified with 5,6,14,15-dibenzo-1,4-dioxa-8,12-diazacyclopentadeca-5,14-diene containing different ligating atoms of oxygen and nitrogen, have been employed for the voltammetric determination of Ag(I) ion from aqueous solution. The voltammetric response was characterized with respect to paste composition, preconcentration method, kind of anion, variation of pH, Ag(I) ion concentration, and possible interferences. Linear calibration curves were obtained for Ag(I) ion concentration ranging from $3.0{\times}10^{-6}M$ to $8.0{\times}10^{-5}M$, and detection limit was $8.5{\times}10^{-7}M$.

Photometric Study on the Spot-Double Star XY Ursae Majoris(I)

  • Lee, Woo-Baik
    • Journal of Astronomy and Space Sciences
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    • v.5 no.1
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    • pp.57-72
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    • 1988
  • The long-term observational properties of the photometric behaviors of the short period(p=0.48 day) eclipsing binary system XY UMa are discussed. They are based on the UBV observatins, which were carried out by Geyer in the yaers 1955-1961, 1968, 1975-1984. Light curves of XY UMa revealed very large changes not only between consecutive observing nights, but also from season to season. Between 1955 and 1984, the mean system brightness increased about 30% during this time interfvals, meanwhile, the orbital period of this system was constant whithin 1.6% of its period. The colour index curve shows similar variations like the light curve but with a phase offset oscillation around the time instants of the primary minama. Observational evidence for photospheric and chromospheric activities on the XY Uma are also discussed.

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Fragility curves and loss functions for RC structural components with smooth rebars

  • Cardone, Donatello
    • Earthquakes and Structures
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    • v.10 no.5
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    • pp.1181-1212
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    • 2016
  • Fragility and loss functions are developed to predict damage and economic losses due to earthquake loading in Reinforced Concrete (RC) structural components with smooth rebars. The attention is focused on external/internal beam-column joints and ductile/brittle weak columns, designed for gravity loads only, using low-strength concrete and plain steel reinforcing bars. First, a number of damage states are proposed and linked deterministically with commonly employed methods of repair and related activities. Results from previous experimental studies are used to develop empirical relationships between damage states and engineering demand parameters, such as interstory and column drift ratios. Probability distributions are fit to the empirical data and the associated statistical parameters are evaluated using statistical methods. Repair costs for damaged RC components are then estimated based on detailed quantity survey of a number of pre-70 RC buildings, using Italian costing manuals. Finally, loss functions are derived to predict the level of monetary losses to individual RC components as a function of the experienced response demand.